Patent US4645533A successfully refreshed from Google Patents.
US4645533A
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Tantalum powder and method of making
Assignee: Cabot Supermetals KK
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Filing: 1985-01-17
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Granted: 1987-02-24
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Expires: 2005-01-17
Abstract
Abstract The dielectric characteristic and resistance against the dielectric characteristic deterioration of tantalum powder for use in a solid electrolyte capacitor are improved by incorporating phosphorus and boron dopant sources into tantalum material at the reducing step of K2TaF7 or by incorporating one of the two dopant sources at the reducing step and the other dopant source at the heat-treating step.
Inventors
- 👤 Tomoo Izumi
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-05 01:30
CPC Classifications
H; H01; H01G; H01G9/00; H01G9/004; H01G9/04; H01G9/048; H01G9/052; H01G9/0525; B; B22; B22F; B22F9/00; B22F9/16; B22F9/18; B22F9/24; C; C22; C22B; C22B34/00; C22B34/20; C22B34/24
Claims Analysis
Total Claims: 7
Claim 1
Independent Claim
123 words
A method for producing tantalum powder, comprising the successive steps of: (1) reducing potassium fluorotantalate with metallic sodium in the presence of a diluent to yield unrefined tantalum powder; (2) washing the unrefined tantalum powder to yield tantalum powder; (3) heat-treating the tantalum powder; and (4) fine crushing the tantalum powder, wherein at least one boron component and at least one phosphorus component are used as doping sources; and wherein the reducing of the poatassium fluorotantalate (1) is conducted in the presence of both of said dopant sources, or the reducing of the potassium fluorotantalate is conducted in the presence of one of the dopant sources and the other of the dopant sources is brought into inseparable contact with the heat-treated tantalum powder.
Claim 2
Independent Claim
123 words
A method for producing tantalum powder, comprising the successive steps of: (1) reducing potassium fluorotantalate with metallic sodium in the presence of a diluent to yield unrefined tantalum powder; (2) washing the unrefined tantalum powder to yield tantalum powder; (3) heat-treating the tantalum powder; and (4) fine crushing the tantalum powder, wherein at least one boron component and at least one phosphorus component are used as doping sources; and wherein the reducing of the poatassium fluorotantalate (1) is conducted in the presence of both of said dopant sources, or the reducing of the potassium fluorotantalate is conducted in the presence of one of the dopant sources and the other of the dopant sources is brought into inseparable contact with the heat-treated tantalum powder.
Claim 3
Dependent Claim
52 words
A method according to claim 1, wherein said at least one boron component is selected from the group consisting of H 3 BO 3 , KBF 4 , NH 3 BO 3 , Na 3 BO 3 , B 2 O 3 , NH 4 BF 4 , and NaBF 4 .
Claim 4
Dependent Claim
35 words
A method according to claim 1, wherein said phosphorus component is selected from the group consisting of P 2 O 5 , Ca 3 (PO 4 ) 2 , and H 3 PO 4 .
Claim 5
Dependent Claim
43 words
A method according to claim 1, wherein the process comprises conducting the reducing of the potassium fluorotantalate in the presence of one of the dopant sources, and said process comprises adding the other dopant source to the tantalum powder before the heat treatment.
Claim 6
Dependent Claim
21 words
A method according to claim 1, wherein said at least other dopant source is added to the tantalum powder as heated-treated.
Claim 7
Dependent Claim
61 words
A powder for a solid electrolyte capacitor consisting of powder produced by the method according to claim 1, 2, 3, 4, or 5, having a specific electrostatic capacity of 10,000 μFV/g or more and short circuits of approximately 3% or less, when tested under a life test of a direct current of 32.5 V applied for 1000 hours at 85° C.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1990-02-23 | 1990-08-25 | 1991-02-24 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1994-02-23 | 1994-08-25 | 1995-02-24 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1998-02-23 | 1998-08-25 | 1999-02-24 | $7700.00 | Window Closed / Lapsed |