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US4622267A Expired / Lapsed US ⏱️ 0.0 years remaining

Microcapsules having capsule walls formed of aliphatic diisocyanate and diamine

Assignee: Feldmuehle AG
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Filing: 1984-12-12
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Granted: 1986-11-11
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Expires: 2004-12-12
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Abstract

Abstract In microcapsules of the type used for pressure-sensitive, carbonless copy papers, having walls formed from aliphatic diisocyanate and diamine and containing a solvent mixture with a dye precursor dissolved therein, the solvent mixture containing a component which easily dissolves the dye precursor and the capsule wall material and a component which only poorly dissolves the dye precursor and the capsule wall, the improvement comprising the poorly disolving solvent component is an alkylbenzene having from 8 up to 14 C-atoms in the alkyl moiety; and the easily dissolving solvent component is selected from the group consisting of diisopropyl naphthaline, a hydrogenated terphenyl, an alkylated diphenyl, a diphenyl alkane, a chloroparaffin and a mixture thereof, the ratio of easily to poorly dissolving components ranging from 15:85 to 75:25 vol %, and being adjusted within this range so that a solution of the wall-forming aliphatic diisocyanate is just at the turbidity point in the mixture of easily dissolving and poorly dissolving components.

Inventors

  • 👤 Kurt Riecke

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-26 20:07
CPC Classifications
B; B01; B01J; B01J13/00; B01J13/02; B01J13/06; B01J13/14; B01J13/16; B41; B41M; B41M5/00; B41M5/124; B41M5/165; B41M5/1655; Y; Y10; Y10T; Y10T428/00; Y10T428/29; Y10T428/2982; Y10T428/2984; Y10T428/2985

Claims Analysis

Total Claims: 5
Claim 1
Independent Claim 137 words
In microcapsules of the type used for pressure-sensitive, carbonless copy papers, having walls formed from aliphatic diisocyanate and diamine and containing a solvent mixture with a die precursor dissolved therein, the solvent mixture containing a component which easily dissolves the dye precursor and the capsule wall material and a component which only poorly dissolves the dye precursor and the capsule wall, the improvement comprising the poorly dissolving solvent component is an alkylbenzene having from 8 to 14 C-atoms in the alkyl moiety; and the easily dissolving solvent component is a chloroparaffin, the ratio of easily to poorly dissolving components ranging from 15:85 to 75:25 vol %, and being adjusted within this range so that a solution of the wall-forming aliphatic diisocyanate is just at the turbidity point in the mixture of easily dissolving and poorly dissolving components.
Claim 2
Dependent Claim 137 words
In microcapsules of the type used for pressure-sensitive, carbonless copy papers, having walls formed from aliphatic diisocyanate and diamine and containing a solvent mixture with a die precursor dissolved therein, the solvent mixture containing a component which easily dissolves the dye precursor and the capsule wall material and a component which only poorly dissolves the dye precursor and the capsule wall, the improvement comprising the poorly dissolving solvent component is an alkylbenzene having from 8 to 14 C-atoms in the alkyl moiety; and the easily dissolving solvent component is a chloroparaffin, the ratio of easily to poorly dissolving components ranging from 15:85 to 75:25 vol %, and being adjusted within this range so that a solution of the wall-forming aliphatic diisocyanate is just at the turbidity point in the mixture of easily dissolving and poorly dissolving components.
Claim 3
Dependent Claim 25 words
The microcapsules of claim 1 wherein the easily dissolving solvent component is n-C 14 to n-C 17 chloroparaffins with a chlorine content of about 45%.
Claim 4
Dependent Claim 13 words
The microcapsules of claim 2 wherein the poorly dissolving solvent component is dodecylbenzene.
Claim 5
Dependent Claim 14 words
The microcapsules of claim 1 wherein the easily dissolving solvent component is stabilized chloroparaffin.

References Cited (Backward Citations)

US3886085A Cited
US3968301A Cited
US4275905A Cited
US4299723A Cited
US4406816A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1989-11-10 1990-05-12 1990-11-11 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1993-11-10 1994-05-12 1994-11-11 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1997-11-10 1998-05-12 1998-11-11 $7700.00 Window Closed / Lapsed

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