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US4597858A Expired / Lapsed US ⏱️ 0.0 years remaining

Multistream, multiproduct beneficiation arrangement

Assignee: SOHIO ALTERNATE ENERGY DEVELOPMENT COMPANY A DE CORP
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Filing: 1984-09-14
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Granted: 1986-07-01
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Expires: 2004-09-14
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Abstract

Abstract An improved method and apparatus for froth flotation separation of the components of a slurry, having particular utility for the beneficiation of coal by the flotation separation of coal particles from impurities associated therewith such as ash and sulfur. In this arrangement, a forward product stream is formed in which a first quantity of chemical reagents is mixed with the particulate matter slurry. The treated particulate matter slurry is then sprayed through a nozzle onto the surface of water in a forward stream flotation tank to create a floating froth phase containing therein a first quantity of the particulate matter. The remainder of the particulate matter slurry separates from the froth phase by sinking in the water, and the froth phase is separated as a first product. The remainder of the particulate matter slurry is then directed to a scavenger product stream in which an additional quantity of chemical reagents is mixed with the remainder of the separated particulate matter slurry. The mixture is then sprayed through a second nozzle onto the surface of water in a second scavenger stream flotation tank to create a floating froth phase containing therein a second quantity of the particulate matter. The remainder of the particulate matter slurry separates from the second froth phase by sinking in the water, and the second froth phase is then separated as a second product. The amounts of the products recovered in the first and second product streams are substantially independently adjustable by controlling the amounts and types of chemical reagents added in each stream.

Inventors

  • 👤 Lester E. Burgess
  • 👤 Phillip E. McGarry
  • 👤 David E. Herman

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 18:50
CPC Classifications
B; B03; B03D; B03D1/00; B03D1/02; B03D1/14; B03D1/1406; B03D1/1443; B03D1/1456; B03D1/1462; B03D1/1475

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 333 words
A multiple stream, multiple product method for froth flotation separation of the components of an input slurry having particulate coal therein, said method comprising: (a) in a first forward product stream, mixing a first quantity of chemical reagents with the particulate coal slurry, said chemical reagents comprising a monomer, a catalyst and a fluid hydrocarbon, spraying the particulate coal slurry with said chemical reagents mixed therein onto the surface of a liquid to create a floating froth phase on the liquid surface having a first quantity of the particulate coal therein, and allowing the remainder of the particulate coal slurry to separate from the froth phase by sinking in the liquid, and separating the froth phase as a first product; and (b) in a second scavenger product stream, mixing an additional quantity of said chemical reagents with said remainder of the separated particulate coal slurry, spraying said remainder particulate coal slurry with the additional chemical reagents onto the surface of a liquid to create a floating froth phase on the liquid surface having a second quantity of the particulate coal therein, and allowing the remainder of the particulate coal slurry to separate from the froth phase by sinking in the liquid, and separating the second froth phase as a second product, whereby first and second separate product streams are separated from the input slurry, wherein said fluid hydrocarbon in said first quantity of chemical reagents mixed with said forward product stream is restricted to a quantity which yields a lower recovery of said first product than said second product but which yields a first product which is cleaner than said second product and wherein said additional quantity of said chemical reagents mixed with said second scavenger product stream contains a sufficient quantity of fluid hydrocarbon to yield a higher recovery of said second product than first product and sufficient to yield a less clean second product than said first product but a cleaner second product than the particulate coal in said input slurry.
Claim 2
Dependent Claim 333 words
A multiple stream, multiple product method for froth flotation separation of the components of an input slurry having particulate coal therein, said method comprising: (a) in a first forward product stream, mixing a first quantity of chemical reagents with the particulate coal slurry, said chemical reagents comprising a monomer, a catalyst and a fluid hydrocarbon, spraying the particulate coal slurry with said chemical reagents mixed therein onto the surface of a liquid to create a floating froth phase on the liquid surface having a first quantity of the particulate coal therein, and allowing the remainder of the particulate coal slurry to separate from the froth phase by sinking in the liquid, and separating the froth phase as a first product; and (b) in a second scavenger product stream, mixing an additional quantity of said chemical reagents with said remainder of the separated particulate coal slurry, spraying said remainder particulate coal slurry with the additional chemical reagents onto the surface of a liquid to create a floating froth phase on the liquid surface having a second quantity of the particulate coal therein, and allowing the remainder of the particulate coal slurry to separate from the froth phase by sinking in the liquid, and separating the second froth phase as a second product, whereby first and second separate product streams are separated from the input slurry, wherein said fluid hydrocarbon in said first quantity of chemical reagents mixed with said forward product stream is restricted to a quantity which yields a lower recovery of said first product than said second product but which yields a first product which is cleaner than said second product and wherein said additional quantity of said chemical reagents mixed with said second scavenger product stream contains a sufficient quantity of fluid hydrocarbon to yield a higher recovery of said second product than first product and sufficient to yield a less clean second product than said first product but a cleaner second product than the particulate coal in said input slurry.
Claim 3
Dependent Claim 24 words
A multiple stage, multiple product froth flotation separation method as claimed in claim 1, each spraying step utilizing a spiral, open flow spray nozzle.
Claim 4
Dependent Claim 21 words
A multiple stage, multiple product froth flotation separation method as claimed in claim 1 wherein said fluid hydrocarbon is fuel oil.
Claim 5
Dependent Claim 31 words
A multiple stage, multiple product froth flotation separation method as claimed in claim 1, including conducting a series of spraying and separating steps in each of said forward and scavenger streams.
Claim 6
Dependent Claim 24 words
A multiple stage, multiple product froth flotation separation method as claimed in claim 4, each spraying step utilizing a spiral, open flow spray nozzle.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1989-06-30 1989-12-30 1990-07-01 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1993-06-30 1993-12-30 1994-07-01 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1997-06-30 1997-12-30 1998-07-01 $7700.00 Window Closed / Lapsed

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