Patent US4595520A successfully refreshed from Google Patents.
US4595520A
Expired / Lapsed
US
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Method for forming solid detergent compositions
Assignee: Ecolab USA Inc
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Filing: 1984-10-18
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Granted: 1986-06-17
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Expires: 2004-10-18
Abstract
Abstract Methods are disclosed for preparing solid alkaline detergent compositions from aqueous emulsions comprising water, a source of alkalinity, a condensed phosphate hardness sequestering agent and a solidifying agent such as anhydrous sodium carbonate, comprising heating said emulsion to hydrate and melt the solidifying agent and then cooling the mixture.
Inventors
- 👤 Bernard J. Heile
- 👤 Terry J. Klos
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 23:31
CPC Classifications
C; C11; C11D; C11D3/00; C11D3/02; C11D3/04; C11D3/06; C11D17/00; C11D17/0047; C11D17/0052; C11D17/0065; C11D3/10
Claims Analysis
Total Claims: 27
Claim 1
Independent Claim
87 words
A method for forming a solid alkaline detergent composition comprising forming an emulsion comprising water, a source of alkalinity comprising about 5-25% of an alkali metal hydroxide, a condensed phosphate hardness sequestering agent and a solidifying agent selected from the group consisting of anhydrous sodium carbonate, anhydrous sodium sulfate and mixtures thereof, said solidifying agent being being incorporated into said emulsion at about 35°-50° C., the amount of said agent being effective to solidify said emulsion to a homogeneous solid when it is cooled to ambient temperatures.
Claim 2
Independent Claim
87 words
A method for forming a solid alkaline detergent composition comprising forming an emulsion comprising water, a source of alkalinity comprising about 5-25% of an alkali metal hydroxide, a condensed phosphate hardness sequestering agent and a solidifying agent selected from the group consisting of anhydrous sodium carbonate, anhydrous sodium sulfate and mixtures thereof, said solidifying agent being being incorporated into said emulsion at about 35°-50° C., the amount of said agent being effective to solidify said emulsion to a homogeneous solid when it is cooled to ambient temperatures.
Claim 3
Dependent Claim
16 words
The method of claim 1 wherein said emulsion comprises about 25-55% water and about 45-75% solids.
Claim 4
Dependent Claim
17 words
The method of claim 1 wherein the condensed phosphate hardness sequestering agent comprises an alkali metal tripolyphosphate.
Claim 5
Dependent Claim
21 words
The method of claim 3 wherein the weight ratio of alkali metal tripolyphosphate to the alkali metal hydroxide is about 3-4:1.
Claim 6
Dependent Claim
16 words
The method of claim 3 wherein said emulsion further comprises a synthetic hectorite clay suspending agent.
Claim 7
Dependent Claim
15 words
The method of claim 1 wherein said emulsion further comprises a source of active halogen.
Claim 8
Dependent Claim
13 words
The method of claim 6 wherein the active halogen source comprises sodium hypochlorite.
Claim 9
Dependent Claim
14 words
The method of claim 1 wherein the source of alkalinity comprises anhydrous sodium metasilicate.
Claim 10
Dependent Claim
14 words
The method of claim 1 wherein the emulsion further comprises a synthetic organic surfactant.
Claim 11
Dependent Claim
24 words
The method of claim 9 wherein the surfactant is selected from the group consisting of an anionic surfactant, a nonionic surfactant and mixtures thereof.
Claim 12
Independent Claim
93 words
A method for forming a solid detergent product comprising: (a) forming a stirred dispersion of a synthetic hectorite clay suspending agent in water; (b) adding sufficient sodium or potassium hydroxide to said dispersion to raise the temperature of said dispersion to about 40°-45° C.; (c) adding sodium tripolyphosphate and a solidifying agent comprising anhydrous sodium carbonate, anhydrous sodium sulfate or mixtures thereof to said dispersion while maintaining the temperature at about 40°-45° C. to form a detergent emulsion; and (d) cooling said dispersion to ambient temperatures to form a homogeneous solid detergent product.
Claim 13
Independent Claim
93 words
A method for forming a solid detergent product comprising: (a) forming a stirred dispersion of a synthetic hectorite clay suspending agent in water; (b) adding sufficient sodium or potassium hydroxide to said dispersion to raise the temperature of said dispersion to about 40°-45° C.; (c) adding sodium tripolyphosphate and a solidifying agent comprising anhydrous sodium carbonate, anhydrous sodium sulfate or mixtures thereof to said dispersion while maintaining the temperature at about 40°-45° C. to form a detergent emulsion; and (d) cooling said dispersion to ambient temperatures to form a homogeneous solid detergent product.
Claim 14
Dependent Claim
18 words
The method of claim 11 further comprising adding an active chlorine source to the dispersion in step (c).
Claim 15
Dependent Claim
16 words
The method of claim 11 wherein the active chlorine source comprises an aqueous alkali metal hypochlorite.
Claim 16
Dependent Claim
18 words
The method of claim 11 further comprising adding a synthetic organic surfactant to the dispersion in step (c).
Claim 17
Dependent Claim
17 words
The method of claim 11 wherein the detergent emulsion comprises about 30-45% water and about 55-70% solids.
Claim 18
Dependent Claim
21 words
The method of claim 11 wherein an aqueous solution of sodium or potassium hydroxide is added to the stirred clay-water dispersion.
Claim 19
Dependent Claim
29 words
The method of claim 11 wherein the detergent emulsion comprises water, about 0.1-2.5% synthetic hectorite clay, about 5-15% sodium hydroxide, about 10-30% solidifying agent and about 20-40% sodium tripolyphosphate.
Claim 20
Dependent Claim
15 words
The method of claim 17 wherein the detergent emulsion comprises about 1-5% of sodium hypochlorite.
Claim 21
Dependent Claim
16 words
The method of claim 18 wherein the sodium hypochlorite is encapsulated in a chlorine resistant coating.
Claim 22
Dependent Claim
19 words
The method of claim 11 further comprising adding a quaternary ammonium softening agent to the dispersion in step (c).
Claim 23
Dependent Claim
12 words
A solid alkaline detergent composition formed by the method of claim 1.
Claim 24
Dependent Claim
12 words
A solid alkaline detergent composition formed by the method of claim 1.
Claim 25
Dependent Claim
12 words
A solid alkaline detergent composition formed by the method of claim 11.
Claim 26
Dependent Claim
24 words
The method of claim 1 further comprising forming a cast detergent composition by introducing said emulsion into a mold prior to cooling said emulsion.
Claim 27
Dependent Claim
19 words
The method of claim 11 wherein said dispersion is cooled in a mold to form a cast detergent product.
References Cited (Backward Citations)
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| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
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| 3.5 Years (Year 4) | 1989-06-16 | 1989-12-16 | 1990-06-17 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1993-06-16 | 1993-12-16 | 1994-06-17 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1997-06-16 | 1997-12-16 | 1998-06-17 | $7700.00 | Window Closed / Lapsed |