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Ultrafiltration membrane of polyamide

Assignee: Membrana GmbH
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Filing: 1984-10-10
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Granted: 1986-06-17
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Expires: 2004-10-10
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Abstract

Abstract A membrane is disclosed of polyamide, a copolyamide or a mixture of polyamides, suitable for ultrafiltration and composed of an ultrafiltration skin and a backing layer. The pore size in the backing layer increases with distance from the ultrafiltration skin. The membrane is prepared by dissolving a polyamide in at least 75% formic acid, applying a casting solution, containing about 12-22% by weight polyamide and about 1-7% by weight polyethylene glycol in formic acid which has been brought to a temperature of below about 18 DEG C., as a thin layer onto a carrier foil resistant to the components of the solution, introducing the casting solution on the carrier foil into a precipitation and washing bath, withdrawing the casting solution as a coagulated and washed membrane from the carrier foil, stretching in at least one direction and subsequently drying this coagulated and washed membrane.

Inventors

  • 👤 Erich Schindler
  • 👤 Franz Maier

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-25 11:37
CPC Classifications
B; B01; B01D; B01D71/00; B01D71/06; B01D71/56

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 148 words
Flat membranes of a polyamide, a copolyamide or a mixture of polyamides, suitable for ultrafiltration and comprising an ultrafiltration skin and a porous backing layer, the pore size in said backing layer increasing with distance from said ultrafiltration skin, produced by dissolving the polyamide in at least 75% concentration formic acid, applying said casting solution, containing about 12-22% by weight polyamide and 1-7% by weight polyethylene glycol in formic acid and brought to a temperature of below about 18° C., as a thin layer onto a carrier foil resistant to the solution components, introducing said casting solution on said casting foil into a precipitation and washing bath, withdrawing said casting solution as a coagulated and washed membrane from said carrier foil, stretching said coagulated and washed membrane in at least one direction to a ratio from 1.5:1 up to 2.5:1 and subsequently drying said coagulated and washed membrane.
Claim 2
Dependent Claim 148 words
Flat membranes of a polyamide, a copolyamide or a mixture of polyamides, suitable for ultrafiltration and comprising an ultrafiltration skin and a porous backing layer, the pore size in said backing layer increasing with distance from said ultrafiltration skin, produced by dissolving the polyamide in at least 75% concentration formic acid, applying said casting solution, containing about 12-22% by weight polyamide and 1-7% by weight polyethylene glycol in formic acid and brought to a temperature of below about 18° C., as a thin layer onto a carrier foil resistant to the solution components, introducing said casting solution on said casting foil into a precipitation and washing bath, withdrawing said casting solution as a coagulated and washed membrane from said carrier foil, stretching said coagulated and washed membrane in at least one direction to a ratio from 1.5:1 up to 2.5:1 and subsequently drying said coagulated and washed membrane.
Claim 3
Dependent Claim 30 words
The membrane according to claim 1, produced with said drying effected by initially heating the membrane to about 130° C. and then finish-drying at temperatures between 60° and 80° C.
Claim 4
Dependent Claim 19 words
The membrane according to claim 1, having an ultrafiltration efficiency from about 50 up to 20,000 l/m 2 hbar.

References Cited (Backward Citations)

US3615024A Cited
US3876738A Cited
US4340481A Cited
US4203847A Cited
DE2845797A1 Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1989-06-16 1989-12-16 1990-06-17 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1993-06-16 1993-12-16 1994-06-17 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1997-06-16 1997-12-16 1998-06-17 $7700.00 Window Closed / Lapsed

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