Patent US4589428A successfully refreshed from Google Patents.
US4589428A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Tobacco treatment
Assignee: Philip Morris USA Inc
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Filing: 1980-02-21
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Granted: 1986-05-20
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Expires: 2000-02-21
Abstract
Abstract A process for maximizing reduction of gas phase components during combustion of tobacco products is disclosed. The process comprises contacting tobacco material with an aqueous solution to form a tobacco extract. After separating the extract from the fibrous tobacco portion, the extract is treated to remove potassium nitrate by ion exchange, electrodialysis, crystallization techniques or the like. Thereafter, potassium ions in the form of a potassium salt other than potassium nitrate are restored to the potassium depleted tobacco and/or extract to a level approximating that originally present in the tobacco prior to extractions.
Inventors
- 👤 Gus D. Keritsis
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 15:39
CPC Classifications
A; A24; A24B; A24B15/00; A24B15/18; A24B15/24
Claims Analysis
Total Claims: 11
Claim 1
Independent Claim
130 words
In the preparation of a smoking tobacco product including the steps of forming an aqueous extract of tobacco, separating the aqueous extract from the fibrous tobacco residue, the improved method of treating the tobacco to obtain a product which exhibits reduced delivery of gas phase components during combustion thereof, which methhod comprises subjecting tobacco to the following treatments: (a) measuring the potassium content of the aqueous extract; (b) treating the aqueous extract to remove potassium nitrate therefrom; (c) remeasuring the potassium content of the denitrated extract obtained in step (b) and thereafter adding a potassium salt other than potassium nitrate to the denitrated extract to achieve a potassium content approximating that originally present in the unextracted tobacco; and (d) recombining the denitrated potassium containing extract and the fibrous tobacco residue.
Claim 2
Dependent Claim
130 words
In the preparation of a smoking tobacco product including the steps of forming an aqueous extract of tobacco, separating the aqueous extract from the fibrous tobacco residue, the improved method of treating the tobacco to obtain a product which exhibits reduced delivery of gas phase components during combustion thereof, which methhod comprises subjecting tobacco to the following treatments: (a) measuring the potassium content of the aqueous extract; (b) treating the aqueous extract to remove potassium nitrate therefrom; (c) remeasuring the potassium content of the denitrated extract obtained in step (b) and thereafter adding a potassium salt other than potassium nitrate to the denitrated extract to achieve a potassium content approximating that originally present in the unextracted tobacco; and (d) recombining the denitrated potassium containing extract and the fibrous tobacco residue.
Claim 3
Independent Claim
66 words
A method of treating tobacco to reduce the delivery of gas phase components during combustion thereof which comprises: (a) forming an aqueous extract of tobacco and a separated fibrous tobacco residue and treating the extract to remove potassium nitrate therefrom; (b) adding a potassium salt other than potassium nitrate to the denitrated extract; and (c) recombining the denitrated potassium containing extract with the fibrous tobacco residue.
Claim 4
Independent Claim
66 words
A method of treating tobacco to reduce the delivery of gas phase components during combustion thereof which comprises: (a) forming an aqueous extract of tobacco and a separated fibrous tobacco residue and treating the extract to remove potassium nitrate therefrom; (b) adding a potassium salt other than potassium nitrate to the denitrated extract; and (c) recombining the denitrated potassium containing extract with the fibrous tobacco residue.
Claim 5
Dependent Claim
19 words
The method of claim 2 wherein the potassium content of the aqueous extract is determined prior to step (b).
Claim 6
Dependent Claim
18 words
The method of claim 2 wherein the tobacco is extracted with a denitrated aqueous solution of tobacco solubles.
Claim 7
Dependent Claim
21 words
The method of claim 2 wherein the removal of potassium nitrate in step (a) is effected by means of membrane electrodialysis.
Claim 8
Dependent Claim
24 words
The method of claim 2 wherein the tobacco extract is treated to remove potassium nitrate by crystallization and then further denitrated by membrane electrodialysis.
Claim 9
Dependent Claim
26 words
The method of claim 2 wherein the removal of potassium nitrate in step (a) is effected by means of a mixed bed of anion-cation exchange resins.
Claim 10
Dependent Claim
34 words
The method of claim 2 wherein the potassium salt added to the denitrated extract in step (b) has an anion portion selected from the group consisting of citrate, acetate, phosphate, carbonate, bicarbonate and malate.
Claim 11
Dependent Claim
23 words
The method of claim 2 wherein the potassium salt is added after the denitrated extract has been recombined with the fibrous tobacco residue.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1989-05-19 | 1989-11-18 | 1990-05-20 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1993-05-19 | 1993-11-18 | 1994-05-20 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1997-05-19 | 1997-11-18 | 1998-05-20 | $7700.00 | Window Closed / Lapsed |