US4585499A
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Method of producing ceramics
Assignee: NGK Insulators Ltd
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Filing: 1984-07-31
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Granted: 1986-04-29
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Expires: 2004-07-31
Abstract
Abstract Zirconia powder is formed by dry grinding, and slurry of the zirconia powder with nonaqueous solvent is shaped and fired.
Inventors
- 👤 Syunzo Mase
- 👤 Shigeo Soejima
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-02 12:26
CPC Classifications
G; G01; G01N; G01N27/00; G01N27/26; G01N27/403; G01N27/406; G01N27/407; G01N27/4073; C; C04; C04B; C04B35/00; C04B35/01; C04B35/48; C04B35/486; C04B41/00; C04B41/009; C04B41/45; C04B41/50; C04B41/51; C04B41/80; C04B41/81; C04B41/85; C04B41/88
Claims Analysis
Total Claims: 22
Claim 1
Independent Claim
62 words
A method of producing ceramics comprising the steps of: preparing a powder consisting essentially of zirconia; calcining said powder at a temperature of 200°-1,200° C. for at least one hour; dry grinding said powder forming a non-aqueous slurry of the dry ground powder; shaping said non-aqueous slurry into a body; and firing the shaped body at a temperature greater than 1,100° C.
Claim 2
Independent Claim
62 words
A method of producing ceramics comprising the steps of: preparing a powder consisting essentially of zirconia; calcining said powder at a temperature of 200°-1,200° C. for at least one hour; dry grinding said powder forming a non-aqueous slurry of the dry ground powder; shaping said non-aqueous slurry into a body; and firing the shaped body at a temperature greater than 1,100° C.
Claim 3
Dependent Claim
32 words
The method of claim 1, wherein a layer of paste containing metallic powder is overlaid on at least one side surface of said shaped body and the shaped body is then fired.
Claim 4
Dependent Claim
38 words
The method of claim 1, wherein a layer of paste containing a compound capable of forming metal upon heating is overlaid on at least one side surface of said shaped body and the shaped body is then fired.
Claim 5
Dependent Claim
56 words
The method of claim 1, wherein a layer of paste containing metallic powder is overlaid on at least one side surface of said shaped body, and said shaped body is overlaid on a green layer consisting essentially of a ceramic material, thereby forming a laminated body, and the laminated body is fired into a unitary body.
Claim 6
Dependent Claim
56 words
The method of claim 1, wherein a layer of paste containing metallic powder is overlaid on at least one side surface of said shaped body, and the shaped body is overlaid on a fired layer consisting essentially of a ceramic material, thereby forming a laminated body, and the laminated body is fired into a unitary body.
Claim 7
Dependent Claim
61 words
The method of claim 1, wherein a layer of paste containing a compound capable of forming metal upon heating is overlaid on at least one side surface of said shaped body, the shaped body is overlaid on a green layer consisting essentially of a ceramic material, thereby forming a laminated body, and the laminated body is fired into a unitary body.
Claim 8
Dependent Claim
67 words
The method of claim 1, wherein a layer of paste containing a compound capable of producing metal upon heating is overlaid on at least one side surface of said shaped body, and the shaped body having the layer of paste is overlaid on a fired layer consisting essentially of a ceramic material, thereby forming a laminated body, and the laminated body is fired into a unitary body.
Claim 9
Dependent Claim
25 words
The method of producing ceramics of claim 1, wherein said dry ground powder has a specific surface area of greater than 5 m 2 /g.
Claim 10
Independent Claim
167 words
A method of producing an oxygen sensor element comprising the steps of: preparing a substrate consisting essentially of a ceramic material; overlaying a first electrode layer on said substrate, said first electrode layer consisting essentially of at least one material selected from the group of materials consisting of metallic powder and a compound capable of forming metal upon heating; heating said substrate with the first electrode layer thereon to form a first electrode; overlaying said heated substrate on a shaped body to form a laminated body, said shaped body being formed by: preparing a powder consisting essentially of zirconia; calcining said powder at a temperature of 200-1,200° C. for at least one hour; dry grinding said powder; forming a non-aqueous slurry of the dry ground powder; and shaping said non-aqueous slurry into a body; firing said laminated body at a temperature greater than 1,100° C. to produce a zirconia ceramic body; and forming a second electrode on said zirconia ceramic body to form an oxygen sensor element.
Claim 11
Independent Claim
167 words
A method of producing an oxygen sensor element comprising the steps of: preparing a substrate consisting essentially of a ceramic material; overlaying a first electrode layer on said substrate, said first electrode layer consisting essentially of at least one material selected from the group of materials consisting of metallic powder and a compound capable of forming metal upon heating; heating said substrate with the first electrode layer thereon to form a first electrode; overlaying said heated substrate on a shaped body to form a laminated body, said shaped body being formed by: preparing a powder consisting essentially of zirconia; calcining said powder at a temperature of 200-1,200° C. for at least one hour; dry grinding said powder; forming a non-aqueous slurry of the dry ground powder; and shaping said non-aqueous slurry into a body; firing said laminated body at a temperature greater than 1,100° C. to produce a zirconia ceramic body; and forming a second electrode on said zirconia ceramic body to form an oxygen sensor element.
Claim 12
Dependent Claim
28 words
The method of producing an oxygen sensor element of claim 9, wherein said dry ground powder has a specific surface area of greater than 5 m 2 /g.
Claim 13
Independent Claim
168 words
A method of producing an oxygen sensor element comprising the steps of: preparing a substrate consisting essentially of a zirconia ceramic material; overlaying a first electrode layer on said substrate, said first electrode layer consisting essentially of at least one material selected from the group of materials consisting of metallic powder and a compound capable of forming metal upon heating; heating said substrate with the first electrode layer thereon to form a first electrode; overlaying said heated substrate on a shaped body to form a laminated body, said shaped body being formed by: preparing a powder consisting essentially of zirconia; calcining said powder at a temperature of 200°-1,200° C. for at least one hour; dry grinding said powder; forming a non-aqueous slurry of the dry ground powder; and shaping said non-aqueous slurry into a body; firing said laminated body at a temperature greater than 1,100° C. to produce a zirconia ceramic body; and forming a second electrode on said zirconia ceramic body to form an oxygen sensor element.
Claim 14
Independent Claim
168 words
A method of producing an oxygen sensor element comprising the steps of: preparing a substrate consisting essentially of a zirconia ceramic material; overlaying a first electrode layer on said substrate, said first electrode layer consisting essentially of at least one material selected from the group of materials consisting of metallic powder and a compound capable of forming metal upon heating; heating said substrate with the first electrode layer thereon to form a first electrode; overlaying said heated substrate on a shaped body to form a laminated body, said shaped body being formed by: preparing a powder consisting essentially of zirconia; calcining said powder at a temperature of 200°-1,200° C. for at least one hour; dry grinding said powder; forming a non-aqueous slurry of the dry ground powder; and shaping said non-aqueous slurry into a body; firing said laminated body at a temperature greater than 1,100° C. to produce a zirconia ceramic body; and forming a second electrode on said zirconia ceramic body to form an oxygen sensor element.
Claim 15
Independent Claim
162 words
A method of producing an oxygen sensor element comprising the steps of: preparing a substrate consisting essentially of a ceramic material; preparing a first electrode layer on said substrate, said first electrode layer consisting essentially of at least one material selected from the group of materials consisting of metallic powder and a compound capable of forming metal upon heating; overlaying said substrate and said first electrode layer on a shaped body to form a laminated body, said shaped body being formed by: preparing a powder consisting essentially of zirconia; calcining said powder at a temperature of 200°-1,200° C. for at least one hour; dry grinding said powder; forming a non-aqueous slurry of the dry ground powder; and shaping said non-aqueous slurry into a body; firing said laminated body at a temperature greater than 1,100° C. to produce a zirconia ceramic body with a first electrode therein; and forming a second electrode on said zirconia ceramic body to form an oxygen sensor element.
Claim 16
Independent Claim
162 words
A method of producing an oxygen sensor element comprising the steps of: preparing a substrate consisting essentially of a ceramic material; preparing a first electrode layer on said substrate, said first electrode layer consisting essentially of at least one material selected from the group of materials consisting of metallic powder and a compound capable of forming metal upon heating; overlaying said substrate and said first electrode layer on a shaped body to form a laminated body, said shaped body being formed by: preparing a powder consisting essentially of zirconia; calcining said powder at a temperature of 200°-1,200° C. for at least one hour; dry grinding said powder; forming a non-aqueous slurry of the dry ground powder; and shaping said non-aqueous slurry into a body; firing said laminated body at a temperature greater than 1,100° C. to produce a zirconia ceramic body with a first electrode therein; and forming a second electrode on said zirconia ceramic body to form an oxygen sensor element.
Claim 17
Independent Claim
163 words
A method of producing an oxygen sensor element comprising the steps of: preparing a substrate consisting essentially of a zirconia ceramic material; preparing a first electrode layer on said substrate, said first electrode layer consisting essentially of at least one material selected from the group of materials consisting of metallic powder and a compound capable of forming metal upon heating; overlaying said substrate and said first electrode layer on a shaped body to form a laminated body, said shaped body being formed by: preparing a powder consisting essentially of zirconia; calcining said powder at a temperature of 200°-1,200° C. for at least one hour; dry grinding said powder; forming a non-aqueous slurry of the dry ground powder; and shaping said non-aqueous slurry into a body; firing said laminated body at a temperature greater than 1,100° C. to produce a zirconia ceramic body with a first electrode therein; and forming a second electrode on said zirconia ceramic body to form an oxygen sensor element.
Claim 18
Independent Claim
163 words
A method of producing an oxygen sensor element comprising the steps of: preparing a substrate consisting essentially of a zirconia ceramic material; preparing a first electrode layer on said substrate, said first electrode layer consisting essentially of at least one material selected from the group of materials consisting of metallic powder and a compound capable of forming metal upon heating; overlaying said substrate and said first electrode layer on a shaped body to form a laminated body, said shaped body being formed by: preparing a powder consisting essentially of zirconia; calcining said powder at a temperature of 200°-1,200° C. for at least one hour; dry grinding said powder; forming a non-aqueous slurry of the dry ground powder; and shaping said non-aqueous slurry into a body; firing said laminated body at a temperature greater than 1,100° C. to produce a zirconia ceramic body with a first electrode therein; and forming a second electrode on said zirconia ceramic body to form an oxygen sensor element.
Claim 19
Independent Claim
158 words
A method of producing an oxygen sensor element comprising the steps of: preparing a substrate consisting essentially of a ceramic material; preparing a first eletrode layer and a second electrode layer, said electrode layers consisting essentially of at least one material selected from the group of materials consisting of metallic powder and a compound capable of forming metal upon heating; preparing a green zirconia layer by: preparing a powder consisting essentially of zirconia; calcining said powder at a temperature of 200°-1,200° C. for at least one hour; dry grinding said powder; forming a non-aqueous slurry of the dry ground powder; and shaping said non-aqueous slurry into a green zirconia layer; overlaying said substrate, said first and second electrode layer and said green zirconia layer to form a laminated body with said zirconia layer being between said first and second electrodes; and firing said laminated body at a temperature greater than 1,100° C. to produce an oxygen sensor element.
Claim 20
Independent Claim
158 words
A method of producing an oxygen sensor element comprising the steps of: preparing a substrate consisting essentially of a ceramic material; preparing a first eletrode layer and a second electrode layer, said electrode layers consisting essentially of at least one material selected from the group of materials consisting of metallic powder and a compound capable of forming metal upon heating; preparing a green zirconia layer by: preparing a powder consisting essentially of zirconia; calcining said powder at a temperature of 200°-1,200° C. for at least one hour; dry grinding said powder; forming a non-aqueous slurry of the dry ground powder; and shaping said non-aqueous slurry into a green zirconia layer; overlaying said substrate, said first and second electrode layer and said green zirconia layer to form a laminated body with said zirconia layer being between said first and second electrodes; and firing said laminated body at a temperature greater than 1,100° C. to produce an oxygen sensor element.
Claim 21
Independent Claim
159 words
A method of producing an oxygen sensor element comprising the steps of: preparing a substrate consisting essentially of a zirconia ceramic material; preparing a first electrode layer and a second electrode layer, said electrode layers consisting essentially of at least one material selected from the group of materials consisting of metallic powder and a compound capable of forming metal upon heating; preparing a green zirconia layer by: preparing a powder consisting essentially of zirconia; calcining said powder at a temperature of 200°-1,200° C. for at least one hour; dry grinding said powder; forming a non-aqueous slurry of the dry ground powder; and shaping said non-aqueous slurry into a green zirconia layer; overlaying said substrate, said first and second electrode layers and said green zirconia layer to form a laminated body with said zirconia layer being between said first and second electrodes; and firing said laminated body at a temperature greater than 1,100° C. to form an oxygen sensor element.
Claim 22
Independent Claim
159 words
A method of producing an oxygen sensor element comprising the steps of: preparing a substrate consisting essentially of a zirconia ceramic material; preparing a first electrode layer and a second electrode layer, said electrode layers consisting essentially of at least one material selected from the group of materials consisting of metallic powder and a compound capable of forming metal upon heating; preparing a green zirconia layer by: preparing a powder consisting essentially of zirconia; calcining said powder at a temperature of 200°-1,200° C. for at least one hour; dry grinding said powder; forming a non-aqueous slurry of the dry ground powder; and shaping said non-aqueous slurry into a green zirconia layer; overlaying said substrate, said first and second electrode layers and said green zirconia layer to form a laminated body with said zirconia layer being between said first and second electrodes; and firing said laminated body at a temperature greater than 1,100° C. to form an oxygen sensor element.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1989-04-28 | 1989-10-28 | 1990-04-29 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1993-04-28 | 1993-10-28 | 1994-04-29 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1997-04-28 | 1997-10-28 | 1998-04-29 | $7700.00 | Window Closed / Lapsed |