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US4576890A Expired / Lapsed US ⏱️ 0.0 years remaining

Preparation of encapsulated electrostatographic toner material

Assignee: Fujifilm Holdings Corp
•
Filing: 1984-03-14
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Granted: 1986-03-18
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Expires: 2004-03-14
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Abstract

Abstract A process for the preparation of an encapsulated electrostatographic toner material comprising a stage of forming shells around micro-droplets of core material containing colorant dispersed in an aqueous medium to produce microcapsules therein, and a stage of separating the microcapsules from the aqueous medium, which is characterized in that methylcellulose is employed for stabilizing the micro-droplets of core material in the aqueous medium.

Inventors

  • 👤 Noriyuki Hosoi

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 15:46
CPC Classifications
G; G03; G03G; G03G9/00; G03G9/08; G03G9/093; G03G9/09392; G03G9/0935; G03G9/09357; G03G9/09371

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 64 words
A process for the preparation of an encapsulated electrostatographic toner material comprising a stage of forming shells around micro-droplets of hydrophobic core material containing colorant dispersed in an aqueous medium to produce microcapsules therein, and a stage of separating the microcapsules from the aqueous medium, which is characterized in that methylcellulose is employed for stabilizing the micro-droplets of core material in the aqueous medium.
Claim 2
Dependent Claim 64 words
A process for the preparation of an encapsulated electrostatographic toner material comprising a stage of forming shells around micro-droplets of hydrophobic core material containing colorant dispersed in an aqueous medium to produce microcapsules therein, and a stage of separating the microcapsules from the aqueous medium, which is characterized in that methylcellulose is employed for stabilizing the micro-droplets of core material in the aqueous medium.
Claim 3
Dependent Claim 30 words
The process for the preparation of an encapsulated electrostatographic toner material as claimed in claim 1, in which said methylcellulose has an average molecular weight ranging from 10,000 to 50,000.
Claim 4
Dependent Claim 32 words
The process for the preparation of an encapsulated electrostatographic toner material as claimed in claim 1, in which the methylcellulose has a methoxy substitution degree in the range of 1.2 to 2.0.
Claim 5
Dependent Claim 32 words
The process for the preparation of an encapsulated electrostatographic toner material as claimed in claim 3 in which the methylcellulose is substituted with hydrooxypropoxy groups in a portion of its methoxy groups.
Claim 6
Dependent Claim 34 words
The process for the preparation of an encapsulated electrostatographic toner material as claimed in claim 4, in which 20 to 60% of the methoxy groups attached to the methylcellulose are substituted with hydroxypropoxy groups.
Claim 7
Dependent Claim 36 words
The process for the preparation of an encapsulated electrostatographic toner material as claimed in claim 1 in which said the stage of forming shells around micro-droplets of core material is performed by an interfacial polymerization method.
Claim 8
Dependent Claim 27 words
The process for the preparation of an encapsulated electrostatographic toner material as claimed in claim 1, in which said methylcellulose is made hydrophobic by treatment with methylolmelamine.
Claim 9
Dependent Claim 42 words
The process for the preparation of an encapsulated electrostatographic toner material as claimed in claim 1, in which said methylcellulose is employed in an amount of not higher than 10% by weight based on the total amount of materials constituting the microcapsules.
Claim 10
Dependent Claim 41 words
The process for the preparation of an encapsulated electrostatographic toner material as claimed in claim 6 in which said shell comprises at least one resin selected from the group consisting of a polyurethane resin, a polyurea resin and a polyamide resin.
Claim 11
Dependent Claim 47 words
The process for the preparation of an encapsulated electrostatographic toner material as claimed in claim 6 in which said shell is composed of a complex layer comprising at least two resins selected from the group consisting of a polyurethane resin, a polyurea resin and a polyamide resin.

References Cited (Backward Citations)

US3523906A Cited
US3645911A Cited
DE2809659A1 Cited
US4439510A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1989-03-17 1989-09-16 1990-03-18 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1993-03-17 1993-09-16 1994-03-18 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1997-03-17 1997-09-16 1998-03-18 $7700.00 Window Closed / Lapsed

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