Patent US4544032A successfully refreshed from Google Patents.
US4544032A
Expired / Lapsed
US
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Method and apparatus for production of perfect well treatment fluid solutions
Assignee: Mid-Continent Equipment Group Pte Ltd
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Filing: 1984-04-02
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Granted: 1985-10-01
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Expires: 2004-04-02
Abstract
Abstract A method and apparatus for providing and treating a well with a viscosity-enhanced treatment liquid which will not clog perforations, gravel packs, filters and the like. A selected viscosity-enhancing agent in particle size is mixed in a selected well treatment liquid to produce a dispersion and the mixing continued at least until hydration is initiated to form an interface between the particles and the liquid. The liquid containing the interface is then subjected to a simultaneous mechanical and hydraulic shearing action by passage through axial apertures in a relatively rotatable rotor and stator units which are disposed in axial juxtaposition with a spacing between the adjacent rotor and stator surfaces selected to be less than the minor dimensions of the interface produced by the dispersion of the selected well treatment liquid and viscosity-enhancing agent. Such treatment results in a substantially complete dissolution of the viscosity enhancing particles in the well treatment liquid, thereby producing a "perfect" solution, and eliminates clogging of well perforations, gravel packs, filters, and the like.
Inventors
- 👤 John B. Echols
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 21:40
CPC Classifications
C; C09; C09K; C09K8/00; C09K8/60; C09K8/92; C09K8/02; C09K8/03; C09K8/035; E; E21; E21B; E21B43/00; E21B43/02; E21B43/04; Y; Y10; Y10S; Y10S507/00; Y10S507/904; Y10S507/922; Y10S507/925; Y10S507/926; Y10S507/935
Claims Analysis
Total Claims: 19
Claim 1
Independent Claim
122 words
The method of treating a subterranean well with an increased viscosity liquid solution and reducing clogging of formations or gravel packs, with such solution, comprising the steps of: (1) mixing dry viscosity-enhancing particles into a liquid phase to produce a dispersion of the dry particles in the liquid phase; (2) mixing the dispersion until at least hydration of the viscosity-enhancing particles is initiated, thereby forming an interface between the particles and the liquid phase; (3) subjecting the dispersion to concurrent mechanical and hydraulic shearing forces sufficient to break down the interface and perfecting the dissolution of the viscosity-enhancing particles into the liquid phase; and (4) introducing the resultant perfect solution into a subterranean well for treatment of at least a portion thereof.
Claim 2
Independent Claim
122 words
The method of treating a subterranean well with an increased viscosity liquid solution and reducing clogging of formations or gravel packs, with such solution, comprising the steps of: (1) mixing dry viscosity-enhancing particles into a liquid phase to produce a dispersion of the dry particles in the liquid phase; (2) mixing the dispersion until at least hydration of the viscosity-enhancing particles is initiated, thereby forming an interface between the particles and the liquid phase; (3) subjecting the dispersion to concurrent mechanical and hydraulic shearing forces sufficient to break down the interface and perfecting the dissolution of the viscosity-enhancing particles into the liquid phase; and (4) introducing the resultant perfect solution into a subterranean well for treatment of at least a portion thereof.
Claim 3
Independent Claim
147 words
The method of treating a subterranean well with an increased viscosity liquid solution and reducing clogging of formations or gravel packs, with such solution, comprising the steps of: (1) mixing dry viscosity-enhancing particles into a liquid phase to produce a dispersion of the dry particles in the liquid phase; (2) mixing the dispersion until at least hydration of the viscosity-enhancing particles is initiated, thereby forming an interface between the particles and the liquid phase; (3) subjecting the dispersion to concurrent mechanical and hydraulic shearing forces sufficient to break down the interface and perfecting the dissolution of the viscosity-enhancing particles in the liquid phase; (4) introducing the resultant perfect solution into a subterranean well for treatment of at least a portion thereof; and (5) removing the perfect solution from the well and filtering entrained contaminate particulates therefrom to permit re-introduction of the perfect solution into a subterranean well.
Claim 4
Independent Claim
147 words
The method of treating a subterranean well with an increased viscosity liquid solution and reducing clogging of formations or gravel packs, with such solution, comprising the steps of: (1) mixing dry viscosity-enhancing particles into a liquid phase to produce a dispersion of the dry particles in the liquid phase; (2) mixing the dispersion until at least hydration of the viscosity-enhancing particles is initiated, thereby forming an interface between the particles and the liquid phase; (3) subjecting the dispersion to concurrent mechanical and hydraulic shearing forces sufficient to break down the interface and perfecting the dissolution of the viscosity-enhancing particles in the liquid phase; (4) introducing the resultant perfect solution into a subterranean well for treatment of at least a portion thereof; and (5) removing the perfect solution from the well and filtering entrained contaminate particulates therefrom to permit re-introduction of the perfect solution into a subterranean well.
Claim 5
Dependent Claim
29 words
The process of claim 1 or 2 wherein said viscosity-enhancing particles comprise at least one of the class of hydroxyethylcellulose, a polysaccharide, a polyester, a polyacrylate; and quar gum.
Claim 6
Dependent Claim
32 words
The process of claim 1 or 2 wherein the liquid phase comprises an aqueous solution of at least one of the class of sodium chloride, calcium chloride, calcium bromide and zinc bromide.
Claim 7
Dependent Claim
58 words
The process of claim 1 or 2 wherein step 3 is performed by passing the dispersion axially through apertures formed in two relatively rotating discs, said discs being axially separated by a distance less than the minor dimensions of the interface thereby imposing a mechanical and hydraulic shear on the interface passing axially through the relatively rotating apertures.
Claim 8
Dependent Claim
29 words
The process of claim 5 wherein the axial clearance between the relatively rotating discs is selectively adjustable to fall in the range of about forty to about 2 microns.
Claim 9
Dependent Claim
26 words
The process of claim 5 wherein the relative rotation speed of the apertured discs is varied as a function of the apparent viscosity of the dispersion.
Claim 10
Independent Claim
87 words
The method of preparing a well treatment fluid comprising a perfect solution of viscosity-enhancing particles in a liquid phase, comprising the steps of: (1) dispersing the viscosity-enhancing particles in the liquid phase; (2) mixing the dispersion until at least hydration of the viscosity-enhancing particles is initiated, thereby forming an interface between the particles and the liquid phase; and (3) subjecting the dispersion to concurrent mechanical and hydraulic shearing forces sufficient to break down the interface and completing the dissolution of the viscosity-enhancing particles in the liquid phase.
Claim 11
Independent Claim
87 words
The method of preparing a well treatment fluid comprising a perfect solution of viscosity-enhancing particles in a liquid phase, comprising the steps of: (1) dispersing the viscosity-enhancing particles in the liquid phase; (2) mixing the dispersion until at least hydration of the viscosity-enhancing particles is initiated, thereby forming an interface between the particles and the liquid phase; and (3) subjecting the dispersion to concurrent mechanical and hydraulic shearing forces sufficient to break down the interface and completing the dissolution of the viscosity-enhancing particles in the liquid phase.
Claim 12
Dependent Claim
27 words
The process of claim 8 wherein said viscosity-enhancing particles comprise at least one of the class of hydroxyethylcellulose, a polysaccharide, a polyester, a polyacrylate and quar gum.
Claim 13
Dependent Claim
30 words
The process of claim 9 wherein the liquid phase comprises an aqueous solution of at least one of the class of sodium chloride, calcium chloride, calcium bromide and zinc bromide.
Claim 14
Dependent Claim
54 words
The process of claim 8 wherein step 3 is performed by passing the dispersion axially through apertures formed in two relatively rotating discs, said discs being axially separated by a distance less than the minor dimensions of the interface to impose a mechanical shear on the interface passing axially through the relatively rotating apertures.
Claim 15
Dependent Claim
28 words
The process of claim 11 wherein the axial clearance between the relatively rotating discs is adjusted to fall in the range of about 40 to about 2 microns.
Claim 16
Dependent Claim
26 words
The process of claim 11 wherein the relative rotational speed of the apertured discs is varied as a function of the apparent viscosity of the dispersion.
Claim 17
Independent Claim
91 words
The method of preparing a well treatment fluid comprising a perfect solution of water soluble polymer particles in an aqueous fluid comprising the steps of: (1) dispersing the polymer particles in the aqueous fluid; (2) mixing the dispersion until at least hydration of the soluble polymer particles is initiated, thereby forming an interface between the polymer particles and the aqueous fluid; and (3) subjecting the dispersion to concurrent mechanical and hydraulic shearing forces sufficicent to break down the interface and perfecting the dissolution of the polymer particles into the aqueous solution.
Claim 18
Independent Claim
91 words
The method of preparing a well treatment fluid comprising a perfect solution of water soluble polymer particles in an aqueous fluid comprising the steps of: (1) dispersing the polymer particles in the aqueous fluid; (2) mixing the dispersion until at least hydration of the soluble polymer particles is initiated, thereby forming an interface between the polymer particles and the aqueous fluid; and (3) subjecting the dispersion to concurrent mechanical and hydraulic shearing forces sufficicent to break down the interface and perfecting the dissolution of the polymer particles into the aqueous solution.
Claim 19
Dependent Claim
28 words
The process of claim 1 wherein said soluble polymer particles comprises at least one of the class of hydroxyethylcellulose, a polysaccharide, a polyester, a polyacrylate and quar gum.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1988-09-30 | 1989-04-01 | 1989-10-01 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1992-09-30 | 1993-04-01 | 1993-10-01 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1996-09-30 | 1997-04-01 | 1997-10-01 | $7700.00 | Window Closed / Lapsed |