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US4537820A Expired / Lapsed US ⏱️ 0.0 years remaining

Insulation board and process of making

Assignee: Praxair Technology Inc
•
Filing: 1983-11-01
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Granted: 1985-08-27
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Expires: 2003-11-01
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Abstract

Abstract Insulation board capable of bearing a load without significant loss of insulating capacity due to compression, produced by a method wherein the board is made in compliance with specified conditions of time, temperature and pressure.

Inventors

  • 👤 Jeffert J. Nowobilski
  • 👤 William J. Owens

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 20:26
CPC Classifications
C; C03; C03B; C03B37/00; C03B37/10; C03B37/14; C03B37/15; H; H01; H01M; H01M10/00; H01M10/60; H01M10/65; H01M10/658; Y; Y02; Y02E; Y02E60/00; Y02E60/10; Y10; Y10S; Y10S428/00; Y10S428/902; Y10S428/903; Y10S428/92; Y10T; Y10T156/00; Y10T156/10; Y10T156/1089; Y10T156/1092; Y10T442/00; Y10T442/60; Y10T442/643; Y10T442/644

Claims Analysis

Total Claims: 24
Claim 1
Independent Claim 163 words
Insulation board having a density less than 30 pounds per cubic foot and capable of bearing a load, produced by a process comprising: (a) providing a stack of substantially binderless glass fiber sheets in an amount sufficient to achieve insulation board of desired density less than 30 pounds per cubic foot; (b) providing a press to compress the stack; (c) heating the stack and the press to a temperature in the range of from the glass strain temperature to less than the glass softening temperature for a time period sufficient to achieve thermal equilibration of the stack and the press surface; (d) thereafter compressing the stack by applying a light vertically compressive force of from 0.2 to 5.0 pounds per square inch to the stack with the press, at said thermal equilibrium for a time period sufficient to produce insulation board of desired density and to substantially relieve stress within the board; and (e) cooling the compressed glass fiber stack to ambient temperature.
Claim 2
Dependent Claim 163 words
Insulation board having a density less than 30 pounds per cubic foot and capable of bearing a load, produced by a process comprising: (a) providing a stack of substantially binderless glass fiber sheets in an amount sufficient to achieve insulation board of desired density less than 30 pounds per cubic foot; (b) providing a press to compress the stack; (c) heating the stack and the press to a temperature in the range of from the glass strain temperature to less than the glass softening temperature for a time period sufficient to achieve thermal equilibration of the stack and the press surface; (d) thereafter compressing the stack by applying a light vertically compressive force of from 0.2 to 5.0 pounds per square inch to the stack with the press, at said thermal equilibrium for a time period sufficient to produce insulation board of desired density and to substantially relieve stress within the board; and (e) cooling the compressed glass fiber stack to ambient temperature.
Claim 3
Dependent Claim 205 words
Insulation board having a density less than 30 pounds per cubic foot and capable of bearing a load, produced by a process comprising: (a) heating binder-containing glass fiber sheets at a temperature in the range of from equal to, to 400° F. below, the glass strain temperature for a time period sufficient to remove essentially all of the binder material in the glass fiber sheets and providing a stack of said binderless glass fiber sheets in an amount sufficient to achieve insulation board of desired density less than 30 pounds per cubic foot; (b) providing a press to compress the stack; (c) heating the stack and the press to a temperature in the range of from the glass strain temperature to less than the glass softening temperature for a time period sufficient to achieve thermal equilibration of the stack and the press surface; (d) thereafter compressing the stack by applying a light vertically compressive force of from 0.2 to 5.0 pounds per square inch to the stack with the press, at said thermal equilibrium for a time period sufficient to produce insulation board of desired density and to substantially relieve stress within the board; and (e) cooling the compressed glass fiber stack to ambient temperature.
Claim 4
Dependent Claim 205 words
Insulation board having a density less than 30 pounds per cubic foot and capable of bearing a load, produced by a process comprising: (a) heating binder-containing glass fiber sheets at a temperature in the range of from equal to, to 400° F. below, the glass strain temperature for a time period sufficient to remove essentially all of the binder material in the glass fiber sheets and providing a stack of said binderless glass fiber sheets in an amount sufficient to achieve insulation board of desired density less than 30 pounds per cubic foot; (b) providing a press to compress the stack; (c) heating the stack and the press to a temperature in the range of from the glass strain temperature to less than the glass softening temperature for a time period sufficient to achieve thermal equilibration of the stack and the press surface; (d) thereafter compressing the stack by applying a light vertically compressive force of from 0.2 to 5.0 pounds per square inch to the stack with the press, at said thermal equilibrium for a time period sufficient to produce insulation board of desired density and to substantially relieve stress within the board; and (e) cooling the compressed glass fiber stack to ambient temperature.
Claim 5
Dependent Claim 22 words
The insulation board of claims 1 or 2 having a density of from 14 to less than 30 pounds per cubic foot.
Claim 6
Dependent Claim 21 words
The insulation board of claims 1 or 2 wherein step (c) is accomplished by heating the stack and the press together.
Claim 7
Dependent Claim 24 words
The insulation board of claims 1 or 2 wherein a part of step (c) is accomplished by heating the stack and the press separately.
Claim 8
Dependent Claim 32 words
The insulation board of claims 1 or 2 wherein the temperature range of step (c) is from 100° F. greater than the strain temperature to 200° F. below the glass softening temperature.
Claim 9
Dependent Claim 23 words
The insulation board of claims 1 or 2 wherein the light vertically compressive force is from 0.5 to 1.5 pounds per square inch.
Claim 10
Dependent Claim 21 words
The insulation board of claims 1 or 2 wherein the time period of step (d) is from 2 to 16 hours.
Claim 11
Dependent Claim 27 words
The insulation board of claims 1 or 2 wherein the glass fiber sheets are comprised of glass fibers having a diameter of from 0.2 to 13 microns.
Claim 12
Dependent Claim 164 words
A process for producing insulation board having a density of less than 30 pounds per cubic foot and capable of bearing a load comprising: (a) providing a stack of substantially binderless glass fiber sheets in an amount sufficient to achieve insulation board of desired density less than 30 pounds per cubic foot; (b) providing a press to compress the stack; (c) heating the stack and the press to a temperature in the range of from the glass strain temperature to less than the glass softening temperature for a time period sufficient to achieve thermal equilibration of the stack and the press surface; (d) thereafter compressing the stack by applying a light vertically compressive force of from 0.2 to 5.0 pounds per square inch to the stack with the press, at said thermal equilibrium for a time period sufficient to produce insulation board of desired density and to substantially relieve stress within the board; and (e) cooling the compressed glass fiber stack to ambient temperature.
Claim 13
Dependent Claim 164 words
A process for producing insulation board having a density of less than 30 pounds per cubic foot and capable of bearing a load comprising: (a) providing a stack of substantially binderless glass fiber sheets in an amount sufficient to achieve insulation board of desired density less than 30 pounds per cubic foot; (b) providing a press to compress the stack; (c) heating the stack and the press to a temperature in the range of from the glass strain temperature to less than the glass softening temperature for a time period sufficient to achieve thermal equilibration of the stack and the press surface; (d) thereafter compressing the stack by applying a light vertically compressive force of from 0.2 to 5.0 pounds per square inch to the stack with the press, at said thermal equilibrium for a time period sufficient to produce insulation board of desired density and to substantially relieve stress within the board; and (e) cooling the compressed glass fiber stack to ambient temperature.
Claim 14
Dependent Claim 206 words
A process for producing insulation board having a density of less than 30 pounds per cubic foot and capable of bearing a load comprising: (a) heat binder-containing glass fiber sheets at a temperature in the range of from equal to, to 400° F. below, the glass strain temperature for a time period sufficient to remove essentially all of the binder material in the glass fiber sheets and providing a stack of said binderless glass fiber sheets in an amount sufficient to achieve insulation board of desired density less than 30 pounds per cubic foot; (b) providing a press to compress the stack; (c) heating the stack and the press to a temperature in the range of from the glass strain temperature to less than the glass softening temperature for a time period sufficient to achieve thermal equilibration of the stack and the press surface; (d) thereafter compressing the stack by applying a light vertically compressive force of from 0.2 to 5.0 pounds per square inch to the stack with the press, at said thermal equilibrium for a time period sufficient to produce insulation board of desired density and to substantially relieve stress within the board; and (e) cooling the compressed glass fiber stack to ambient temperature.
Claim 15
Dependent Claim 206 words
A process for producing insulation board having a density of less than 30 pounds per cubic foot and capable of bearing a load comprising: (a) heat binder-containing glass fiber sheets at a temperature in the range of from equal to, to 400° F. below, the glass strain temperature for a time period sufficient to remove essentially all of the binder material in the glass fiber sheets and providing a stack of said binderless glass fiber sheets in an amount sufficient to achieve insulation board of desired density less than 30 pounds per cubic foot; (b) providing a press to compress the stack; (c) heating the stack and the press to a temperature in the range of from the glass strain temperature to less than the glass softening temperature for a time period sufficient to achieve thermal equilibration of the stack and the press surface; (d) thereafter compressing the stack by applying a light vertically compressive force of from 0.2 to 5.0 pounds per square inch to the stack with the press, at said thermal equilibrium for a time period sufficient to produce insulation board of desired density and to substantially relieve stress within the board; and (e) cooling the compressed glass fiber stack to ambient temperature.
Claim 16
Dependent Claim 21 words
The process of claims 10 or 11 wherein the density is from 14 to less than 30 pounds per cubic foot.
Claim 17
Dependent Claim 20 words
The process of claims 10 or 11 wherein step (c) is accomplished by heating the stack and the press together.
Claim 18
Dependent Claim 23 words
The process of claims 10 or 11 wherein a part of step (c) is accomplished by heating the stack and the press separately.
Claim 19
Dependent Claim 31 words
The process of claims 10 or 11 wherein the temperature range of step (c) is from 100° F. greater than the strain temperature to 200° F. below the glass softening temperature.
Claim 20
Dependent Claim 22 words
The process of claims 10 or 11 wherein the light vertically compressive force is from 0.5 to 1.5 pounds per square inch.
Claim 21
Dependent Claim 20 words
The process of claims 10 or 11 wherein the time period of step (d) is from 2 to 16 hours.
Claim 22
Dependent Claim 26 words
The process of claims 10 or 11 wherein the glass fiber sheets are comprised of glass fibers having a diameter of from 0.2 to 13 microns.
Claim 23
Dependent Claim 45 words
Insulation board essentially free of binder, capable of bearing a load and having a density less than 30 pounds per cubic foot comprised of compressed glass fibers oriented essentially in planes parallel to one another so as to have substantially only point contact between fibers.
Claim 24
Dependent Claim 45 words
Insulation board essentially free of binder, capable of bearing a load and having a density less than 30 pounds per cubic foot comprised of compressed glass fibers oriented essentially in planes parallel to one another so as to have substantially only point contact between fibers.

References Cited (Backward Citations)

US2745173A Cited
US2765587A Cited
US3199715A Cited
US3289423A Cited
US4447490A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1988-08-26 1989-02-25 1989-08-27 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1992-08-26 1993-02-25 1993-08-27 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1996-08-26 1997-02-25 1997-08-27 $7700.00 Window Closed / Lapsed

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