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Ceramic-glass-metal seal by microwave heating

Assignee: United States, DOE THE, Secretary of
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Filing: 1983-10-04
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Granted: 1985-07-16
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Expires: 2003-10-04
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Abstract

Abstract A method for producing a ceramic-glass-metal seal by microwaving mixes a slurry of glass sealing material and coupling agent and applies same to ceramic and metal workpieces. The slurry and workpieces are then insulated and microwaved at a power, time and frequency sufficient to cause a liquid phase reaction in the slurry. The reaction of the glass sealing material forms a chemically different seal than that which would be formed by conventional heating because it is formed by diffusion rather than by wetting of the reactants.

Inventors

  • 👤 Thomas T. Meek
  • 👤 Rodger D. Blake

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 16:14
CPC Classifications
H; H05; H05B; H05B6/00; H05B6/64; C; C04; C04B; C04B37/00; C04B37/02; C04B37/023; C04B37/025; C04B2235/00; C04B2235/65; C04B2235/66; C04B2235/667; C04B2237/00; C04B2237/02; C04B2237/10; C04B2237/30; C04B2237/32; C04B2237/34; C04B2237/343; C04B2237/40; C04B2237/405; C04B2237/406

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 87 words
A method of producing a ceramic-glass-metal seal comprising the steps of: a. mixing a slurry of glass sealing material and coupling agent, applying said slurry to ceramic and metal workpieces for sealing, b. surrounding said slurry and ceramic and metal workpieces with an insulative material, c. microwaving said slurry and ceramic and metal workpieces at a power, time and frequency sufficient to cause a liquid phase reaction in said slurry, and d. allowing said slurry and ceramic and metal workpieces to cool, thereby securing a ceramic-glass-metal seal.
Claim 2
Independent Claim 87 words
A method of producing a ceramic-glass-metal seal comprising the steps of: a. mixing a slurry of glass sealing material and coupling agent, applying said slurry to ceramic and metal workpieces for sealing, b. surrounding said slurry and ceramic and metal workpieces with an insulative material, c. microwaving said slurry and ceramic and metal workpieces at a power, time and frequency sufficient to cause a liquid phase reaction in said slurry, and d. allowing said slurry and ceramic and metal workpieces to cool, thereby securing a ceramic-glass-metal seal.
Claim 3
Dependent Claim 22 words
The method of claim 1 wherein said step of mixing comprises mixing a slurry of glass sealing material and organic coupling agent.
Claim 4
Dependent Claim 20 words
The method of claim 2 wherein said step of mixing comprises mixing a slurry of glass sealing material and water.
Claim 5
Dependent Claim 20 words
The method of claim 2 wherein said step of mixing comprises mixing a slurry of glass sealing material and oil.
Claim 6
Dependent Claim 21 words
The method of claim 4 wherein said step of mixing comprises mixing a slurry of glass sealing material and watch oil.
Claim 7
Dependent Claim 19 words
The method of claim 1 wherein said step of microwaving comprises microwaving at a frequency of about 2.5 gHz.

References Cited (Backward Citations)

US3585258A Cited
US3732048A Cited
US4003368A Cited
US3953703A Cited
US4147911A Cited
US4179596A Cited
US4219361A Cited
US4307277A Cited
US4273950A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1988-07-15 1989-01-14 1989-07-16 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1992-07-15 1993-01-14 1993-07-16 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1996-07-15 1997-01-14 1997-07-16 $7700.00 Window Closed / Lapsed

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