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US4529427A Expired / Lapsed US ⏱️ 0.0 years remaining

Method for making low-loss optical waveguides on an industrial scale

Assignee: Furukawa Electric North America Inc
•
Filing: 1979-01-05
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Granted: 1985-07-16
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Expires: 1999-01-05
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Abstract

Abstract A method is disclosed for making an optical fiber by drawing a preform whose fabrication involves deposition of a glass on a substrate by means of a chemical reaction between gaseous reagents. According to the disclosed method, accurately controlled amounts of a gaseous reagent are produced by flash evaporating a metered flow of a liquid reagent. The disclosed method is of particular interest for the industrial production of optical fibers.

Inventors

  • 👤 William G. French

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-31 19:22
CPC Classifications
C; C03; C03B; C03B37/00; C03B37/01; C03B37/012; C03B37/014; C03B37/018; C03B37/01807; C23; C23C; C23C16/00; C23C16/44; C23C16/448; C23C16/4481; C23C16/52; C03B2201/00; C03B2201/06; C03B2201/08; C03B2201/10; C03B2201/30; C03B2201/40; C03B2201/42; C03B2207/00; C03B2207/80; C03B2207/85; C03B2207/87

Claims Analysis

Total Claims: 16
Claim 1
Independent Claim 88 words
A method for fabricating an optical fiber by drawing a preform whose manufacture comprises depositing a glass on a substrate by means of a chemical reaction between at least two reagents forming a gaseous mixture, characterized in that the preparation of said gaseous mixture comprises the steps of (1) supplying at least a first of said reagents in liquid form, (2) supplying a precisely metered flow of said first of said reagents to a flash evaporation chamber, and (3) flash evaporating said flow in said flash evaporation chamber.
Claim 2
Independent Claim 88 words
A method for fabricating an optical fiber by drawing a preform whose manufacture comprises depositing a glass on a substrate by means of a chemical reaction between at least two reagents forming a gaseous mixture, characterized in that the preparation of said gaseous mixture comprises the steps of (1) supplying at least a first of said reagents in liquid form, (2) supplying a precisely metered flow of said first of said reagents to a flash evaporation chamber, and (3) flash evaporating said flow in said flash evaporation chamber.
Claim 3
Dependent Claim 14 words
Method of claim 1 in which said flow is produced by a metering pump.
Claim 4
Dependent Claim 14 words
Method of claim 1 in which said flow is produced by a gravity feed.
Claim 5
Dependent Claim 49 words
Method of claim 1 in which said first of said reagents is selected from the group consisting of BBr 3 , BCl 3 , GeBr 4 , GeCl 4 , PBr 3 , PCl 3 , POCl 3 , SiBr 4 , SiCl 4 , and TiCl 4 .
Claim 6
Dependent Claim 17 words
Method of claim 1 in which at least two of said reagents are supplied in liquid form.
Claim 7
Dependent Claim 16 words
Method of claim 5 in which said two of said reagents are mixed in liquid form.
Claim 8
Dependent Claim 14 words
Method of claim 1 in which said chemical reaction is caused by flame hydrolysis.
Claim 9
Dependent Claim 22 words
Method of claim 1 in which said substrate is a tube which is externally heated and into which said mixture is fed.
Claim 10
Dependent Claim 13 words
Method of claim 1 in which said glass is deposited by plasma deposition.
Claim 11
Dependent Claim 13 words
Method of claim 1 in which said fiber is a graded index fiber.
Claim 12
Independent Claim 111 words
A method for fabricating an optical fiber by drawing a preform whose manufacture comprises depositing a glass on a substrate by means of a chemical reaction between at least two reagents forming a gaseous mixture, characterized in that the preparation of said gaseous mixture comprises the steps of (1) liquifying at least a first of said reagents by refrigeration to a temperature which is less than the boiling temperature and which is greater than the freezing temperature of said first of said reagents, (2) supplying a precisely metered flow of said first of said reagents to a flash evaporation chamber, and (3) flash evaporating said flow in said flash evaporation chamber.
Claim 13
Independent Claim 111 words
A method for fabricating an optical fiber by drawing a preform whose manufacture comprises depositing a glass on a substrate by means of a chemical reaction between at least two reagents forming a gaseous mixture, characterized in that the preparation of said gaseous mixture comprises the steps of (1) liquifying at least a first of said reagents by refrigeration to a temperature which is less than the boiling temperature and which is greater than the freezing temperature of said first of said reagents, (2) supplying a precisely metered flow of said first of said reagents to a flash evaporation chamber, and (3) flash evaporating said flow in said flash evaporation chamber.
Claim 14
Dependent Claim 14 words
Method of claim 11 in which said flow is produced by a metering pump.
Claim 15
Dependent Claim 14 words
Method of claim 11 in which said flow is produced by a gravity feed.
Claim 16
Dependent Claim 15 words
Method of claim 11 in which said first of said reagents is BCl 3 .

References Cited (Backward Citations)

US1879551A Cited
US2377607A Cited
US2406913A Cited
US3854881A Cited
US3904449A Cited
US3980459A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1988-07-15 1989-01-14 1989-07-16 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1992-07-15 1993-01-14 1993-07-16 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1996-07-15 1997-01-14 1997-07-16 $7700.00 Window Closed / Lapsed

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