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US4519959A Expired / Lapsed US ⏱️ 0.0 years remaining

Gas-liquid contacting apparatus

Assignee: Takeda Pharmaceutical Co Ltd
•
Filing: 1983-04-13
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Granted: 1985-05-28
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Expires: 2003-04-13
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Abstract

Abstract A gas-liquid contacting apparatus is constituted by an upright vessel, at least one perforated gas distributor for supplying a gaseous medium into a liquid medium within the vessel, a plate-like rotary disintegrator positioned within the vessel and above the gas distributor for disintegrating bubbles of the gaseous medium into fine bubbles, and a drive shaft concentrically extending through the vessel for the support of the rotary disintegrator.

Inventors

  • 👤 Tatsuro Takeuchi
  • 👤 Shohei Yoshida
  • 👤 Kazuhiro Kawai

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-05 19:56
CPC Classifications
B; B01; B01J; B01J19/00; B01J19/18; B01J19/1868; B01J19/1875; B01D; B01D19/00; B01D19/02; B01F; B01F23/00; B01F23/20; B01F23/23; B01F23/233; B01F23/2336; B01F23/23362; B01F23/23364; B01F23/2366; B01F23/2368; B01F27/00; B01F27/80; B01F27/93; B01F33/00; B01F33/40; B01F33/402; B01J19/0053; B01J19/006; C; C12; C12M; C12M27/00; C12M27/02; C12M27/18; C12M27/20; C12M27/24; C12M29/00; C12M29/06; C12M29/08; B01F23/237; B01F23/2376; B01F23/23761; B01F27/05; B01F27/11; B01F27/113; B01F27/115; B01F27/1151

Claims Analysis

Total Claims: 22
Claim 1
Independent Claim 317 words
A gas-liquid contacting apparatus which comprises, in combination: a generally cylindrical upright vessel for accommodating a quantity of liquid medium to be agitated by the action of bubbles of gaseous medium moving upwards within the vessel; at least one perforated distributor in said vessel for supplying the gaseous medium under pressure into the vessel so as to disperse it into the liquid medium in the form of bubbles; at least one generally disc-shaped rotary disintegrator rotatably mounted in said vessel immediately above said distributor for rotation in a plane perpendicular to the longitudinal axis of said vessel and concentric with the inner peripheral surface of said vessel and having a diameter for defining an annular clearance between the periphery of said disintegrator and the inner peripheral surface of said vessel, said disintegrator having a flat under surface facing the bottom of said vessel for, during the rotation of said disintegrator, causing bubbles of the gaseous medium emerging from said distributor to form a vortex below the flat under surface of said disintegrator, said distributor having a plurality of apertures therein in an annular area around the outer peripheral part of said disintegrator, the radial dimension of said annular area being less than half the radius of said disintegrator, and each of said apertures extending completely through the thickness of said disintegrator from said flat under surface to the upper surface thereof and being defined by peripheral edges of said disintegrator around said apertures, whereby all the bubbles from said vortex pass upwards through the apertures and are sheared by the peripheral edges of said disintegrator for disintegrating the bubbles into fine bubbles; a drive shaft extending coaxially into said vessel and having one end positioned exteriorly of said vessel and having said disintegrator mounted on the other end for rotation together with said shaft; and a drive mechanism connected to said one end of said drive shaft.
Claim 2
Dependent Claim 317 words
A gas-liquid contacting apparatus which comprises, in combination: a generally cylindrical upright vessel for accommodating a quantity of liquid medium to be agitated by the action of bubbles of gaseous medium moving upwards within the vessel; at least one perforated distributor in said vessel for supplying the gaseous medium under pressure into the vessel so as to disperse it into the liquid medium in the form of bubbles; at least one generally disc-shaped rotary disintegrator rotatably mounted in said vessel immediately above said distributor for rotation in a plane perpendicular to the longitudinal axis of said vessel and concentric with the inner peripheral surface of said vessel and having a diameter for defining an annular clearance between the periphery of said disintegrator and the inner peripheral surface of said vessel, said disintegrator having a flat under surface facing the bottom of said vessel for, during the rotation of said disintegrator, causing bubbles of the gaseous medium emerging from said distributor to form a vortex below the flat under surface of said disintegrator, said distributor having a plurality of apertures therein in an annular area around the outer peripheral part of said disintegrator, the radial dimension of said annular area being less than half the radius of said disintegrator, and each of said apertures extending completely through the thickness of said disintegrator from said flat under surface to the upper surface thereof and being defined by peripheral edges of said disintegrator around said apertures, whereby all the bubbles from said vortex pass upwards through the apertures and are sheared by the peripheral edges of said disintegrator for disintegrating the bubbles into fine bubbles; a drive shaft extending coaxially into said vessel and having one end positioned exteriorly of said vessel and having said disintegrator mounted on the other end for rotation together with said shaft; and a drive mechanism connected to said one end of said drive shaft.
Claim 3
Dependent Claim 55 words
An apparatus as claimed in claim 1 further comprising baffle means disposed along the inner peripheral surface of said vessel parallel to said longitudinal axis and above said disintegrator for providing resistance to the whirling flow of the liquid medium with the disintegrated bubbles therein which occur as a result of rotation of said disintegrator.
Claim 4
Dependent Claim 24 words
An apparatus as claimed in claim 1 wherein each of said apertures is a slit opening out of the peripheral edge of said disintegrator.
Claim 5
Dependent Claim 17 words
An apparatus as claimed in claim 1 wherein said each of said apertures is a through hole.
Claim 6
Dependent Claim 37 words
An apparatus as claimed in claim 1 wherein the ratio of the total surface area of said disintegrator to the sum of the cross-sectional areas of the respective apertures is in the range of 0.05 to 0.35.
Claim 7
Dependent Claim 20 words
An apparatus as claimed in claim 1 wherein each of said apertures is no larger than 20 mm in size.
Claim 8
Dependent Claim 29 words
An apparatus as claimed in claim 1 wherein said drive mechanism comprises an electric motor mounted above said vessel and said drive shaft extends downward therefrom into said vessel.
Claim 9
Dependent Claim 36 words
An apparatus as claimed in claim 1 further comprising at least one further distributor and disintegrator are mounted in said vessel above said firstmentioned distributor and disintegrator to form a second stage for disintegration of bubbles.
Claim 10
Dependent Claim 24 words
An apparatus as claimed in claim 1 further comprising means for journalling said drive shaft at the top and the bottom of said vessel.
Claim 11
Dependent Claim 383 words
A gas-liquid contacting apparatus which comprises, in combination: a generally cylindrical upright vessel for accomodating a quantity of liquid medium to be agitated by the action of bubbles of gaseous medium moving upwards within the vessel; at least one perforated distributor in said vessel for supplying the gaseous medium under pressure into the vessel so as to disperse it into the liquid medium in the form of bubbles; at least one generally disc-shaped rotary disintegrator rotatably mounted in said vessel immediately above said distributor for rotation in a plane perpendicular to the longitudinal axis of said vessel and concentric with the inner peripheral surface of said vessel and having a diameter for defining an annular clearance between the periphery of said disintegrator and the inner peripheral surface of said vessel, said disintegrator having a flat under surface facing the bottom of said vessel for, during the rotation of said disintegrator, causing bubbles of the gaseous medium emerging from said distributor to form a vortex below the flat under surface of said disintegrator, said distributor having a plurality of apertures therein in an annular area around the outer peripheral part of said disintegrator, the radial dimension of said annular area being less than half the radius of said disintegrator, and each of said apertures extending completely through the thickness of said disintegrator from said flat under surface to the upper surface thereof and being defined by peripheral edges of said disintegrator around said apertures, whereby all the bubbles from said vortex pass upwards through the apertures and are sheared by the peripheral edges of said disintegrator for disintegrating the bubbles into fine bubbles; a drive shaft extending coaxially into said vessel and having one end positioned exteriorly of said vessel and having said disintegrator mounted on the other end for rotation together with said shaft; a drive mechanism connected to said one end of said drive shaft; a draft tube mounted in said vessel coaxially thereof and above said disintegrator; and at least one rotary stirrer cooperable with said draft tube for producing a circulation of the flow of liquid medium within said vessel through the interior of said draft tube and then through the space between said draft tube and the inner peripheral surface of said vessel by the rotation of said stirrer.
Claim 12
Dependent Claim 383 words
A gas-liquid contacting apparatus which comprises, in combination: a generally cylindrical upright vessel for accomodating a quantity of liquid medium to be agitated by the action of bubbles of gaseous medium moving upwards within the vessel; at least one perforated distributor in said vessel for supplying the gaseous medium under pressure into the vessel so as to disperse it into the liquid medium in the form of bubbles; at least one generally disc-shaped rotary disintegrator rotatably mounted in said vessel immediately above said distributor for rotation in a plane perpendicular to the longitudinal axis of said vessel and concentric with the inner peripheral surface of said vessel and having a diameter for defining an annular clearance between the periphery of said disintegrator and the inner peripheral surface of said vessel, said disintegrator having a flat under surface facing the bottom of said vessel for, during the rotation of said disintegrator, causing bubbles of the gaseous medium emerging from said distributor to form a vortex below the flat under surface of said disintegrator, said distributor having a plurality of apertures therein in an annular area around the outer peripheral part of said disintegrator, the radial dimension of said annular area being less than half the radius of said disintegrator, and each of said apertures extending completely through the thickness of said disintegrator from said flat under surface to the upper surface thereof and being defined by peripheral edges of said disintegrator around said apertures, whereby all the bubbles from said vortex pass upwards through the apertures and are sheared by the peripheral edges of said disintegrator for disintegrating the bubbles into fine bubbles; a drive shaft extending coaxially into said vessel and having one end positioned exteriorly of said vessel and having said disintegrator mounted on the other end for rotation together with said shaft; a drive mechanism connected to said one end of said drive shaft; a draft tube mounted in said vessel coaxially thereof and above said disintegrator; and at least one rotary stirrer cooperable with said draft tube for producing a circulation of the flow of liquid medium within said vessel through the interior of said draft tube and then through the space between said draft tube and the inner peripheral surface of said vessel by the rotation of said stirrer.
Claim 13
Dependent Claim 20 words
An apparatus as claimed in claim 10 in which said stirrer is mounted on said drive shaft for rotation therewith.
Claim 14
Dependent Claim 54 words
An apparatus as claimed in claim 10 further comprising baffle means disposed along the inner peripheral surface of said vessel parallel to said longitudinal axis and above said disintegrator for providing resistance to the whirling flow of the liquid medium with the disintegrated bubbles therein which occur as a result of rotating said disintegrator.
Claim 15
Dependent Claim 24 words
An apparatus as claimed in claim 10 wherein each of said apertures is a slit opening out of the peripheral edge of said disintegrator.
Claim 16
Dependent Claim 16 words
An apparatus as claimed in claim 10 wherein each of said apertures is a through hole.
Claim 17
Dependent Claim 19 words
An apparatus as claimed in claim 10 further comprising means for reversing the direction of drive to said stirrer.
Claim 18
Dependent Claim 19 words
An apparatus as claimed in claim 10 wherein said draft tube is tapered downwardly and inwardly of said vessel.
Claim 19
Dependent Claim 25 words
An apparatus as claimed in claim 10 further comprising an additional drive shaft connected to said stirrer by means of which said stirrer is driven.
Claim 20
Dependent Claim 21 words
An apparatus as claimed in claim 10 further comprising a further drive mechanism connected to said stirrer for driving said stirrer.
Claim 21
Dependent Claim 39 words
An apparatus as claimed in claim 10 further comprising at least one further distributor and disintegrator and at least one further draft tube and stirrer, all mounted in said vessel above said firstmentioned distributor, disintegrator, draft tube and stirrer.
Claim 22
Dependent Claim 23 words
An apparatus as claimed in claim 10 further comprising a generally annular foam suppressing element positioned within said vessel above said draft tube.

References Cited (Backward Citations)

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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1988-05-27 1988-11-26 1989-05-28 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1992-05-27 1992-11-26 1993-05-28 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1996-05-27 1996-11-26 1997-05-28 $7700.00 Window Closed / Lapsed

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