Patent US4512951A successfully refreshed from Google Patents.
US4512951A
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Hydrogen peroxide liquid film sterilization method
Assignee: American Sterilizer Co
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Filing: 1983-08-04
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Granted: 1985-04-23
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Expires: 2003-08-04
Abstract
Abstract A method is provided of hydrogen peroxide sterilization of medical articles whereby there are obtained the advantages of both vapor penetration, especially for such articles as surgical packs, and direct liquid-sterilant article contact, in which a vapor mixture comprising hydrogen peroxide is brought into contact with the article to be sterilized, the article being at a temperature below the dew point or condensation temperature of the vapor mixture, is caused thus to condense as a liquid film on the article, and is revaporized and hence removed from the so-sterilized article.
Inventors
- 👤 Edward Koubek
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-24 19:10
CPC Classifications
A; A61; A61L; A61L2/00; A61L2/16; A61L2/20; A01; A01N; A01N59/00; A61L2/02; A61L2/04; A61L2/06
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
104 words
A method of liquid-contact sterilization which comprises: vaporizing from an aqueous solution of hydrogen peroxide a gaseous vapor consisting of hydrogen peroxide and water vapor; passing the said gaseous vapor into an evacuated sterilization zone and into contact therein with an article to be sterilized; maintaining the article at a temperature below the dew point of the entering vapor so that aqueous hydrogen peroxide solution is condensed out of that said vapor in contact with the said article as a layer of liquid thereon; and maintaining the said film of liquid on the article for a predetermined period to effect sterilization of the article.
Claim 2
Independent Claim
104 words
A method of liquid-contact sterilization which comprises: vaporizing from an aqueous solution of hydrogen peroxide a gaseous vapor consisting of hydrogen peroxide and water vapor; passing the said gaseous vapor into an evacuated sterilization zone and into contact therein with an article to be sterilized; maintaining the article at a temperature below the dew point of the entering vapor so that aqueous hydrogen peroxide solution is condensed out of that said vapor in contact with the said article as a layer of liquid thereon; and maintaining the said film of liquid on the article for a predetermined period to effect sterilization of the article.
Claim 3
Independent Claim
140 words
A method of liquid sterilization which comprises: vaporizing from an aqueous solution of hydrogen peroxide a mixed gaseous vapor consisting of hydrogen peroxide and water vapor free of solid contaminates which may exist in the said solution and passing the said vapor into an evacuated sterilization zone and therein into contact with an article to be sterilized whereby the vapor penetrates the interstices of the said article; maintaining the article at a temperature below the dew point of the entering vapor so that hydrogen peroxide solution is condensed out of said vapor as a layer of liquid on the said article; maintaining the said film of liquid on the article for a predetermined period to effect sterilization of the article; and vaporizing the hydrogen peroxide solution from the surface of the article and removing the so-sterilized-article from the sterilization zone.
Claim 4
Independent Claim
140 words
A method of liquid sterilization which comprises: vaporizing from an aqueous solution of hydrogen peroxide a mixed gaseous vapor consisting of hydrogen peroxide and water vapor free of solid contaminates which may exist in the said solution and passing the said vapor into an evacuated sterilization zone and therein into contact with an article to be sterilized whereby the vapor penetrates the interstices of the said article; maintaining the article at a temperature below the dew point of the entering vapor so that hydrogen peroxide solution is condensed out of said vapor as a layer of liquid on the said article; maintaining the said film of liquid on the article for a predetermined period to effect sterilization of the article; and vaporizing the hydrogen peroxide solution from the surface of the article and removing the so-sterilized-article from the sterilization zone.
Claim 5
Dependent Claim
55 words
The method of claim 2 in which the mixed vapor of hydrogen peroxide and water is passed into the sterilization zone and into contact with the article to be sterilized until the heat of condensation of the vapor raises the temperature of the surface of said article to equilibrium temperature with that of the vapor.
Claim 6
Dependent Claim
26 words
The method of claim 1 in which there is employed an aqueous solution of hydrogen peroxide in concentration between 6% and 70% by weight of solution.
Claim 7
Dependent Claim
20 words
The method of claim 1 in which the hydrogen peroxide is vaporized at a temperature between 100° and 300° F.
Claim 8
Dependent Claim
39 words
The method of claim 5 in which the temperature in the sterilization zone is upon introduction of the said hydrogen peroxide vapor mixture at a temperature between 50° and 200° F. but is lower than the vaporization temperature utilized.
Claim 9
Dependent Claim
71 words
The method of claim 1 in which so-formed vapor of hydrogen peroxide and water is introduced into the sterilization zone, articles to be sterilized are placed in the sterilization zone, thereafter closed to ambient air, at a temperature substantially below the temperature of the introduced said vapor, and the sterilization zone is warmed to a temperature above the temperature of the said article but below the temperature of the introduced vapor.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1988-04-22 | 1988-10-22 | 1989-04-23 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1992-04-22 | 1992-10-22 | 1993-04-23 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1996-04-22 | 1996-10-22 | 1997-04-23 | $7700.00 | Window Closed / Lapsed |