US4487198A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for producing a high-purity maltose
Assignee: Hayashibara Seibutsu Kagaku Kenkyujo KK
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Filing: 1982-07-28
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Granted: 1984-12-11
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Expires: 2002-07-28
Abstract
Abstract High-purity maltose is produced by applying a feed starch sugar solution with a maltose content of at least 70% to a column packed with a strongly-acidic cation exchange resin of alkali metal- or alkaline earth metal-form; fractionating the feed solution by charging water thereto into a high-dextrin fraction, a high-dextrin.maltose fraction, a high-maltose fraction, a high-maltose.glucose fraction, and a high-glucose fraction, in the given order; and recovering the high-maltose fraction. This process constantly provides a fraction with a maltose content of 93% or higher, and enables industrial-scale production of a high-purity maltose much easier and at lower-cost than conventional processes.
Inventors
- 👤 Toshio Miyake
- 👤 Shuzo Sakai
- 👤 Takashi Shibuya
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-04 13:30
CPC Classifications
C; C13; C13B; C13B20/00; C13B20/14; C13B20/144; C13K; C13K7/00
Claims Analysis
Total Claims: 8
Claim 1
Independent Claim
205 words
A process for the separation of maltose from a feed solution by the utilization of an ion exchange resin, comprising: (a) providing a feed solution containing at least 70% maltose based on the weight of the dry solid, the remainder consisting essentially of glucose and dextrins; (b) sequentially admitting predetermined volumes of the feed solution and water to a column of a strongly acidic cation exchange resin having sulphonyl groups of an alkali metal or alkaline earth metal form; (c) sequentially separating the effluents from the column into the following fractions: a first fraction rich in dextrins, a second fraction rich in dextrins, but highly contaminated with maltose, a third fraction of substantially pure maltose, a fourth fraction rich in maltose, but highly contaminated with glucose, and a fifth fraction rich in glucose; (d) recovering the third fraction of substantially pure maltose; (e) sequentially admitting into the column: the second fraction obtained in the step (c), a feed solution having a maltose content of at least 70% based on the weight of dry solid, and the remainder consisting essentially of glucose and dextrin, the fourth fraction obtained in the step (c), and water; and (f) repeating steps (c), (d) and (e) in a cyclic manner.
Claim 2
Dependent Claim
205 words
A process for the separation of maltose from a feed solution by the utilization of an ion exchange resin, comprising: (a) providing a feed solution containing at least 70% maltose based on the weight of the dry solid, the remainder consisting essentially of glucose and dextrins; (b) sequentially admitting predetermined volumes of the feed solution and water to a column of a strongly acidic cation exchange resin having sulphonyl groups of an alkali metal or alkaline earth metal form; (c) sequentially separating the effluents from the column into the following fractions: a first fraction rich in dextrins, a second fraction rich in dextrins, but highly contaminated with maltose, a third fraction of substantially pure maltose, a fourth fraction rich in maltose, but highly contaminated with glucose, and a fifth fraction rich in glucose; (d) recovering the third fraction of substantially pure maltose; (e) sequentially admitting into the column: the second fraction obtained in the step (c), a feed solution having a maltose content of at least 70% based on the weight of dry solid, and the remainder consisting essentially of glucose and dextrin, the fourth fraction obtained in the step (c), and water; and (f) repeating steps (c), (d) and (e) in a cyclic manner.
Claim 3
Dependent Claim
27 words
A process in accordance with claim 1, wherein the maltose content in the third fraction is 93% or higher, based on the weight of the dry solid.
Claim 4
Dependent Claim
19 words
A process in accordance with claim 1, wherein the bed depth of the column is at least 7 m.
Claim 5
Dependent Claim
21 words
A process in accordance with claim 1, wherein the temperature of the column of the resin is kept at 45°-85° C.
Claim 6
Dependent Claim
30 words
A process in accordance with claim 1, wherein the cation exchange resin is in the form of N + , K + , Ca 2+ , or Mg 2+ .
Claim 7
Dependent Claim
26 words
A process in accordance with claim 1, wherein the concentration of the dry solid solute in the feed solution is in the range of 10-70 w/w%.
Claim 8
Dependent Claim
22 words
A process in accordance with claim 1, wherein the water is admitted to the column at a flow rate of SV 0.1-2.0.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1987-12-11 | 1988-06-11 | 1988-12-11 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1991-12-11 | 1992-06-11 | 1992-12-11 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1995-12-11 | 1996-06-11 | 1996-12-11 | $7700.00 | Window Closed / Lapsed |