Patent US5832104A successfully refreshed from Google Patents.
Patent US4482418A successfully refreshed from Google Patents.
US4482418A
Expired / Lapsed
US
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Bonding method for producing very thin bond lines
Assignee: International Business Machines Corp
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Filing: 1983-08-17
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Granted: 1984-11-13
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Expires: 2003-08-17
Abstract
Abstract A bonding method which uses two solutions, one being anionic and the other being cationic, to lay down alternating layers of particles of accurate dimension onto members which are to be bonded. Thereafter, the layers are placed in contact, and the members are bonded together by diffusion bonding techniques.
Inventors
- 👤 Eugene B. Rigby
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-07 09:04
CPC Classifications
C; C09; C09J; C09J5/00; G; G11; G11B; G11B5/00; G11B5/127; G11B5/187; G11B5/23; G11B5/232; Y; Y10; Y10S; Y10S428/00; Y10S428/90; Y10T; Y10T29/00; Y10T29/49; Y10T29/49002; Y10T29/4902; Y10T29/49021; Y10T29/49032; Y10T29/49055; Y10T428/00; Y10T428/25; Y10T428/256; Y10T428/257; Y10T428/259; Y10T428/31504; Y10T428/31536
Claims Analysis
Total Claims: 13
Claim 1
Independent Claim
133 words
A method of diffusion bonding one member to another, to form a very thin bond line therebetween, comprising: a. providing a first colloid solution having a polarity; b. providing a second colloid solution having an opposite polarity; c. dipping at least one of said surfaces in said first solution; d. removing said one surface, and thereafter washing, to leave a monolayer of said first colloid; e. dipping said one surface in said second solution; f. removing said one surface, and thereafter washing, to leave a monolayer of said second colloid; and g. placing the two surfaces to be in contact in a high-heat/high-pressure environment in order to effect a diffusion bond therebetween, the bond-line thickness being determined by the thickness of at least one of the layers of said first and second colloid.
Claim 2
Independent Claim
133 words
A method of diffusion bonding one member to another, to form a very thin bond line therebetween, comprising: a. providing a first colloid solution having a polarity; b. providing a second colloid solution having an opposite polarity; c. dipping at least one of said surfaces in said first solution; d. removing said one surface, and thereafter washing, to leave a monolayer of said first colloid; e. dipping said one surface in said second solution; f. removing said one surface, and thereafter washing, to leave a monolayer of said second colloid; and g. placing the two surfaces to be in contact in a high-heat/high-pressure environment in order to effect a diffusion bond therebetween, the bond-line thickness being determined by the thickness of at least one of the layers of said first and second colloid.
Claim 3
Dependent Claim
16 words
The method of claim 1 including an initial step of cleaning the surfaces to be bonded.
Claim 4
Dependent Claim
21 words
The method of claim 2 including the steps of drying said one surface after each of said steps d and f.
Claim 5
Dependent Claim
62 words
The method of claim 3 wherein said first solution is a solution of one of colloidal silica or colloidal alumina, said second solution is a solution of the colloid not selected for the first solution, both solutions are of about 1% concentration, and said bond-line thickness is determined by the sum of the thickness of layers of said first and second colloid.
Claim 6
Dependent Claim
40 words
The method of claim 4 including the step, performed intermediate steps f and g, of repeating steps c through f, in order to increase the bond-line thickness by increasing the thickness of alternate layers of said first and second colloid.
Claim 7
Dependent Claim
34 words
The method of claim 1 wherein said members to be bonded are ceramic, and wherein said first colloid solution is of a negative polarity, and said second colloid solution is of a positive polarity.
Claim 8
Dependent Claim
52 words
The method of claim 6 wherein said first solution is an anionic solution of colloidal alumina (Al 2 O 3 ), said second solution is a cationic solution of colloidal silica (SiO 2 ), and said bond-line thickness is determined by the sum of the size of said first and second colloid.
Claim 9
Dependent Claim
36 words
The method of claim 7 wherein said solutions are of a concentration about 1% and a pH about 4, and including the steps of air-drying said one surface after each of said steps d and f.
Claim 10
Dependent Claim
40 words
The method of claim 8 including the step, performed intermediate steps f and g, of repeating steps c through f, in order to increase the bond-line thickness by increasing the thickness of alternate layers of said first and second colloid.
Claim 11
Dependent Claim
72 words
The method of claim 6 wherein said members are magnetic ferrite, with said bond-line thickness defining the gap width of a magnetic recording head, and wherein said first solution is an anionic solution of colloidal alumina (Al 2 O 3 ), said second solution is a cationic solution of colloidal silica (SiO 2 ), and said bond-line thickness is determined by the sum of the layers of said first and second colloid.
Claim 12
Dependent Claim
16 words
The method of claim 9 wherein the solution concentrations are about 1% and pH about 4.
Claim 13
Dependent Claim
93 words
The method of claim 1 wherein said one of said surfaces is electrically conductive and exhibits a positive electrical charge in the presence of water, wherein said first colloidal solution is an anionic solution of alumina particles about 0.3 microns in size, wherein said one surface is bonded to one side of an alumina shim, and including the additional step of providing a second electrically conductive surface of positive electrical charge which has been coated by operation of steps a through f and is bonded to the opposite surface of said alumina shim.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1987-11-13 | 1988-05-14 | 1988-11-13 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1991-11-13 | 1992-05-14 | 1992-11-13 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1995-11-13 | 1996-05-14 | 1996-11-13 | $7700.00 | Window Closed / Lapsed |