Patent US4477286A successfully refreshed from Google Patents.
US4477286A
Expired / Lapsed
US
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Breaking oil-in-water emulsions
Assignee: Henkel AG and Co KGaA
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Filing: 1982-07-19
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Granted: 1984-10-16
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Expires: 2002-07-19
Abstract
Abstract The invention relates to the use of 2,4,7,9-tetramethyl-5-decyne-4,7-diol for breaking oil-in-water emulsions and in regenerating used cleaning compositions by making it possible to remove emulsified oils therefrom.
Inventors
- 👤 Christian Rossmann
- 👤 Wolfgang Riedel
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 22:58
CPC Classifications
B; B01; B01D; B01D17/00; B01D17/02; B01D17/04; B01D17/047; C; C23; C23G; C23G1/00; C23G1/36
Claims Analysis
Total Claims: 12
Claim 1
Independent Claim
21 words
A process for breaking oil-in-water emulsions which comprises adding an emulsion breaking effective amount of 2,4,7,9-tetramethyl-5-decyne-4,7-diol to an emulsion containing composition.
Claim 2
Dependent Claim
21 words
A process for breaking oil-in-water emulsions which comprises adding an emulsion breaking effective amount of 2,4,7,9-tetramethyl-5-decyne-4,7-diol to an emulsion containing composition.
Claim 3
Dependent Claim
16 words
A process as set forth in claim 1, wherein the 2,4,7,9-tetramethyl-5-decyne-4,7,-diol is added at room temperature.
Claim 4
Dependent Claim
17 words
A process as set forth in claim 1 wherein the process is carried out at elevated temperatures.
Claim 5
Dependent Claim
31 words
A process as set forth in claim 1 or 2 or 3 wherein the 2,4,7,9-tetramethyl-5-decyne-4,7-diol is added in an amount of about 0.5 to 50 g/l of the emulsion containing composition.
Claim 6
Dependent Claim
22 words
A process as set forth in claim 4, wherein the 2,4,7,9-tetramethyl-5-decyne-4,7-diol is added in an amount of about 0.5 to 5 g/l.
Claim 7
Dependent Claim
49 words
A process as set forth in claim 1 or 2 or 3 wherein the emulsion containing composition includes neutral to strongly alkaline cleaning solutions, emulsified petroleum oils or fixed oils or both and fats, the emulsion is broken, the oil 2,4,7,9-tetramethyl-5-decyne-4,7-diol layer is separated and the cleaning solution reused.
Claim 8
Dependent Claim
21 words
A process as set forth in claim 6 wherein the separated, regenerated cleaning solution has its depleted components replenished before reuse.
Claim 9
Dependent Claim
30 words
A process for causing an oil-in-water emulsion to form separate, aqueous and oily phases which comprises adding from about 0.5 to 50 g/l of 2,4,7,9-tetramethyl-5-decyne-4,7-diol to an oil-in-water emulsion-containing composition.
Claim 10
Dependent Claim
30 words
A process for causing an oil-in-water emulsion to form separate, aqueous and oily phases which comprises adding from about 0.5 to 50 g/l of 2,4,7,9-tetramethyl-5-decyne-4,7-diol to an oil-in-water emulsion-containing composition.
Claim 11
Dependent Claim
79 words
A process for regenerating an oil-in-water emulsion-containing cleaning composition which comprises the steps of: (a) adding from 0.5 to 50 g/l of 2,4,7,9-tetramethyl-5-decyne-4,7-diol to an emulsion-containing composition comprising (i) neutral to strongly alkaline cleaning solution, (ii) emulsified petroleum oils, fixed oils, or both, and (iii) fats to form separate, aqueous and oily phases, said oily phase containing the 2,4,7,9-tetramethyl-5-decyne-4,7-diol; (b) separating the oily phase from the aqueous phase; and (c) replenishing depleted cleaning solution components in the aqueous phase.
Claim 12
Dependent Claim
79 words
A process for regenerating an oil-in-water emulsion-containing cleaning composition which comprises the steps of: (a) adding from 0.5 to 50 g/l of 2,4,7,9-tetramethyl-5-decyne-4,7-diol to an emulsion-containing composition comprising (i) neutral to strongly alkaline cleaning solution, (ii) emulsified petroleum oils, fixed oils, or both, and (iii) fats to form separate, aqueous and oily phases, said oily phase containing the 2,4,7,9-tetramethyl-5-decyne-4,7-diol; (b) separating the oily phase from the aqueous phase; and (c) replenishing depleted cleaning solution components in the aqueous phase.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1987-10-16 | 1988-04-16 | 1988-10-16 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1991-10-16 | 1992-04-16 | 1992-10-16 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1995-10-16 | 1996-04-16 | 1996-10-16 | $7700.00 | Window Closed / Lapsed |