Patent US4469282A successfully refreshed from Google Patents.
US4469282A
Expired / Lapsed
US
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Metal flake production
Assignee: Alcoa Corp
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Filing: 1983-05-11
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Granted: 1984-09-04
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Expires: 2003-05-11
Abstract
Abstract A method of forming metal flake from metal particles comprises charging metal particles, liquid and milling material to a mill and operating the mill to form the metal flake. A portion of the metal flake, liquid and milling material is removed from the mill at a rate substantially commensurate with the charging thereto and milling material is separated from the liquid and metal flake.
Inventors
- 👤 A. David Booz
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-05 22:45
CPC Classifications
B; B02; B02C; B02C17/00; B02C17/18; B22; B22F; B22F1/00; B22F1/06; B22F1/068; B22F9/00; B22F9/02; B22F9/04; B22F2009/043; B22F2998/00
Claims Analysis
Total Claims: 16
Claim 1
Independent Claim
215 words
A method of forming aluminum flake having a predetermined size from aluminum particles in a ball mill wherein backmixing is minimized, said method comprising: (a) charging the ball mill with milling media to be recirculated at a predetermined constant flow rate and with feed materials at a predetermined flow rate to provide a mix therein comprising approximately 30 to 70 wt.% aluminum particles, the remainder liquid; (b) operating the mill to form said aluminum flake; (c) removing the aluminum flake, liquid and milling media from the mill at a rate commensurate with said charging thereto; (d) separating the milling media from the liquid and aluminum flake by addition of solvent to provide a mix having a aluminum flake content in the range of 5 to 20 wt.%; (e) recirculating the milling media to the mill; and (f) maintaining the predetermined flow rates at which said feed materials and the recirculating milling media are charged to the mill to produce aluminum flake having a predetermined size and to minimize backmixing in the mill, said predetermined milling media flow rate being maintained by varying the rate at which said milling media is removed from the mill so as to correct any deviations in the recirculating milling media flow rate from the predetermined recirculating milling media flow rate.
Claim 2
Independent Claim
215 words
A method of forming aluminum flake having a predetermined size from aluminum particles in a ball mill wherein backmixing is minimized, said method comprising: (a) charging the ball mill with milling media to be recirculated at a predetermined constant flow rate and with feed materials at a predetermined flow rate to provide a mix therein comprising approximately 30 to 70 wt.% aluminum particles, the remainder liquid; (b) operating the mill to form said aluminum flake; (c) removing the aluminum flake, liquid and milling media from the mill at a rate commensurate with said charging thereto; (d) separating the milling media from the liquid and aluminum flake by addition of solvent to provide a mix having a aluminum flake content in the range of 5 to 20 wt.%; (e) recirculating the milling media to the mill; and (f) maintaining the predetermined flow rates at which said feed materials and the recirculating milling media are charged to the mill to produce aluminum flake having a predetermined size and to minimize backmixing in the mill, said predetermined milling media flow rate being maintained by varying the rate at which said milling media is removed from the mill so as to correct any deviations in the recirculating milling media flow rate from the predetermined recirculating milling media flow rate.
Claim 3
Dependent Claim
46 words
A method according to claim 1 wherein the step of removing includes projecting a discharge scoop into the ball mill such that on rotation of said mill a portion of the metal flake, liquid and milling media can be removed by being directed into said scoop.
Claim 4
Independent Claim
206 words
A method of forming metal flake having a predetermined size from metal particles in a ball mill wherein backmixing is minimized, said method comprising: (a) charging the ball mill with milling media to be recirculated at a predetermined flow rate and with feed materials at a predetermined constant flow rate to provide a mix therein comprising approximately 30 to 85 wt.% metal particles, the remainder liquid; (b) operating the mill to form said metal flake; (c) removing the metal flake, liquid and milling media from the mill at a rate commensurate with said charging thereto; (d) separating the milling media from the liquid and metal flake by washing the milling media substantially free of said metal flake; (e) recirculating the milling media to the mill; and (f) maintaining the predetermined flow rates at which said feed materials and the recirculating milling media are charged to the mill to produce metal flake having a predetermined size and to minimize backmixing in the mill, said predetermined recirculating milling media flow rate being maintained by varying the rate at which said milling media is removed from the mill so as to correct any deviations in the recirculating milling media flow rate from the predetermined recirculating milling media flow rate.
Claim 5
Independent Claim
206 words
A method of forming metal flake having a predetermined size from metal particles in a ball mill wherein backmixing is minimized, said method comprising: (a) charging the ball mill with milling media to be recirculated at a predetermined flow rate and with feed materials at a predetermined constant flow rate to provide a mix therein comprising approximately 30 to 85 wt.% metal particles, the remainder liquid; (b) operating the mill to form said metal flake; (c) removing the metal flake, liquid and milling media from the mill at a rate commensurate with said charging thereto; (d) separating the milling media from the liquid and metal flake by washing the milling media substantially free of said metal flake; (e) recirculating the milling media to the mill; and (f) maintaining the predetermined flow rates at which said feed materials and the recirculating milling media are charged to the mill to produce metal flake having a predetermined size and to minimize backmixing in the mill, said predetermined recirculating milling media flow rate being maintained by varying the rate at which said milling media is removed from the mill so as to correct any deviations in the recirculating milling media flow rate from the predetermined recirculating milling media flow rate.
Claim 6
Dependent Claim
13 words
The method according to claim 3 wherein the metal particles comprise aluminum particles.
Claim 7
Dependent Claim
12 words
The method according to claim 3 wherein the liquid comprises mineral spirits.
Claim 8
Dependent Claim
24 words
The method according to claim 4 wherein the weight ratio of milling media to metal particles is in the range of 18:1 to 60:1.
Claim 9
Dependent Claim
37 words
The method according to claim 3 wherein the metal particles comprise a metal selected from the group consisting of nickel, copper, zinc, brass, bronze, iron and stainless steel, the mix contains 50 to 83 wt.% metal particles.
Claim 10
Dependent Claim
24 words
The method according to claim 7 wherein the weight ratio of milling media to metal particles is in the range of 5:1 to 20:1.
Claim 11
Dependent Claim
31 words
The method according to claim 7 wherein in the separating step liquid is added to provide a mix having a metal flake content in the range of 20 to 65 wt.%.
Claim 12
Dependent Claim
28 words
The method according to claim 3 wherein the space between the flight and the trough is adapted to be less than one-half the diameter of the milling material.
Claim 13
Dependent Claim
46 words
A method according to claim 3 wherein the step of removing includes projecting a discharge scoop into the ball mill such that on rotation of said mill a portion of the metal flake, liquid and milling media can be removed by being directed into said scoop.
Claim 14
Dependent Claim
32 words
The method according to claim 3 wherein the changes in the milling media flow rate are detected by sensing changes in the weight of the milling media being recirculated to the mill.
Claim 15
Dependent Claim
59 words
The method according to claim 12 wherein the milling media is recirculated employing a conveyor and trough, the conveyor having a flight at least a portion thereof located in the trough for purposes of said recirculating, the conveyor adapted to provide a space between the flight and trough of not greater than two-thirds the diameter of the milling media.
Claim 16
Dependent Claim
13 words
The method according to claim 13 wherein a screw type conveyor is employed.
References Cited (Backward Citations)
US3181800A
Cited
US3369761A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1987-09-04 | 1988-03-05 | 1988-09-04 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1991-09-04 | 1992-03-05 | 1992-09-04 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1995-09-04 | 1996-03-05 | 1996-09-04 | $7700.00 | Window Closed / Lapsed |