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US4465702A Expired / Lapsed US ⏱️ 0.0 years remaining

Cold-water-soluble granular starch for gelled food compositions

Assignee: Staley Continental Inc
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Filing: 1982-11-01
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Granted: 1984-08-14
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Expires: 2002-11-01
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Abstract

Abstract A cold-water-swelling granular starch material derived from ungelatinized corn starch and characterized by a cold-water solubility of at least 50% is prepared by subjecting granular corn starch, slurried in selected aqueous alcohols, to conditions of high temperature and pressure. The cold-water-swelling granular starch material derived from chemically unmodified (or minimally modified) ungelatinized corn starch has an ability to set to a sliceable gel without cooking or chilling when blended with an aqueous sugar syrup. That granular starch material is particularly useful in food systems of the type which set or gel upon standing such as pie fillings, jellies, demouldable desserts and puddings.

Inventors

  • 👤 James E. Eastman
  • 👤 Carl O. Moore

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-03 20:34
CPC Classifications
C; C08; C08B; C08B30/00; C08B30/12; C08B30/14; A; A23; A23L; A23L29/00; A23L29/20; A23L29/206; A23L29/212

Claims Analysis

Total Claims: 31
Claim 1
Independent Claim 48 words
An improved cold-water-swelling granular starch material derived from ungelatinized corn starch consisting essentially of substantially intact, partially swollen granules which appear nonbirefringent when viewed under a polarizing microscope and which have a cold-water-solubility of at least 50% and a reduced native fat content of about 0.25% or less.
Claim 2
Dependent Claim 48 words
An improved cold-water-swelling granular starch material derived from ungelatinized corn starch consisting essentially of substantially intact, partially swollen granules which appear nonbirefringent when viewed under a polarizing microscope and which have a cold-water-solubility of at least 50% and a reduced native fat content of about 0.25% or less.
Claim 3
Dependent Claim 18 words
The improved cold-water-swelling granular starch material of claim 1 characterized by a cold-water solubility of at least 70%.
Claim 4
Dependent Claim 20 words
The improved cold-water-swelling granular starch of claim 2 characterized by a reduced native fat content of about 0.15% or less.
Claim 5
Dependent Claim 31 words
The improved cold-water-swelling granular starch of claim 1 characterized further by an ability to set, without cooking or chilling, to a resilient, sliceable gel when blended with an aqueous sugar syrup.
Claim 6
Dependent Claim 19 words
The improved cold-water-swelling granular starch of claim 4 derived from ungelatinized corn starch which has not been chemically modified.
Claim 7
Dependent Claim 18 words
The improved cold-water-swelling granular starch material of claim 4 characterized by a cold-water solubility of at least 70%.
Claim 8
Dependent Claim 37 words
The improved cold-water-swelling granular starch of claim 4 which has not been chemically modified and which has a cold-water solubility of about 80 to about 95% and a reduced native fat content of about 0.15% or less.
Claim 9
Dependent Claim 196 words
A process for preparing the improved cold-water-swelling granular starch material of claim 4 which comprises: (1) preparing a starch slurry comprised of about 10 to about 25 parts by weight (dsb) of ungelatinized corn starch in a liquid medium comprised of about 50 to about 75 parts by weight of an alcohol selected from ethanol, denatured ethanol, propanol and isopropanol and about 13 to about 30 parts per weight of water provided that the liquid medium contains about 15 to about 35% by weight of water inclusive of the water in the starch, said ungelatinized corn starch being characterized by little or no chemical modification; (2) (a) heating said starch slurry in a closed vessel to a temperature of about 300° to about 360° F. for about 1 to about 30 minutes; or (b) passing said slurry through a heated confined zone in which the slurry is heated from about 300° to about 360° F., the rate of flow of the slurry through said confined zone being such that the residence time for said slurry in the confined zone is about 1 to about 30 minutes; and (3) recovering the cold-water-swelling granular starch from the slurry.
Claim 10
Dependent Claim 13 words
The process of claim 8 wherein the alcohol is ethanol or denatured ethanol.
Claim 11
Dependent Claim 10 words
The process of claim 8 wherein the alcohol is isopropanol.
Claim 12
Dependent Claim 19 words
The process of claim 8 wherein the starch slurry contains about 12 to about 20% by weight of starch.
Claim 13
Dependent Claim 21 words
The process of claim 11 wherein the liquid medium for the slurry contains about 18 to about 26% by weight water.
Claim 14
Dependent Claim 31 words
The process of claim 12 wherein the starch slurry is heated to a temperature of about 315° to about 350° F. for a period of about 1 to about 10 minutes.
Claim 15
Dependent Claim 19 words
The process of claim 13 wherein the alcohol used in forming the starch slurry is ethanol or denatured ethanol.
Claim 16
Dependent Claim 48 words
The process of claim 14 wherein the slurry is heated to a temperature of about 325° to about 340° F. for a period of about 2 to about 5 minutes and then cooled to below about 120° F. prior to recovering the cold-water-swelling granular starch from the slurry.
Claim 17
Dependent Claim 227 words
A process for converting an ungelatinized corn starch characterized by little or no cold-water solubility to a cold-water-swelling granular material consisting essentially of substantially intact, partially swollen granules which appear nonbirefringent when viewed under a polarizing microscope said cold-water-swelling granular starch material being further characterized by a cold-water solubility of at least 50%, which process comprises: (1) preparing a starch slurry comprised of about 10 to about 25 parts by weight (dsb) of an ungelatinized corn starch in a liquid medium comprised of about 50 to about 75 parts by weight of an alcohol selected from ethanol, denatured ethanol, propanol and isopropanol and about 13 to about 30 parts by weight of water provided that the liquid medium contains about 15 to about 35% by weight of water inclusive of the water in the starch; (2) (a) heating said starch slurry in a closed vessel to a temperature of about 300° to about 360° F. for about 1 to about 30 minutes; or (b) passing said slurry through a heated confined zone in which the slurry is heated from about 300° to about 360° F., the rate of flow of the slurry through said confined zone being such that the residence time for said slurry in the heated confined zone is about 1 to about 30 minutes; and (3) recovering the cold-water-swelling granular starch from the slurry.
Claim 18
Dependent Claim 227 words
A process for converting an ungelatinized corn starch characterized by little or no cold-water solubility to a cold-water-swelling granular material consisting essentially of substantially intact, partially swollen granules which appear nonbirefringent when viewed under a polarizing microscope said cold-water-swelling granular starch material being further characterized by a cold-water solubility of at least 50%, which process comprises: (1) preparing a starch slurry comprised of about 10 to about 25 parts by weight (dsb) of an ungelatinized corn starch in a liquid medium comprised of about 50 to about 75 parts by weight of an alcohol selected from ethanol, denatured ethanol, propanol and isopropanol and about 13 to about 30 parts by weight of water provided that the liquid medium contains about 15 to about 35% by weight of water inclusive of the water in the starch; (2) (a) heating said starch slurry in a closed vessel to a temperature of about 300° to about 360° F. for about 1 to about 30 minutes; or (b) passing said slurry through a heated confined zone in which the slurry is heated from about 300° to about 360° F., the rate of flow of the slurry through said confined zone being such that the residence time for said slurry in the heated confined zone is about 1 to about 30 minutes; and (3) recovering the cold-water-swelling granular starch from the slurry.
Claim 19
Dependent Claim 13 words
The process of claim 16 wherein the alcohol is ethanol or denatured ethanol.
Claim 20
Dependent Claim 10 words
The process of claim 16 wherein the alcohol is isopropanol.
Claim 21
Dependent Claim 35 words
The process of claim 16 wherein the starch slurry contains about 12 to about 20% by weight of starch and the liquid medium for the slurry contains about 18 to about 26% by weight water.
Claim 22
Dependent Claim 31 words
The process of claim 19 wherein the starch slurry is heated to a temperature of about 315° to about 350° F. for a period of about 1 to about 10 minutes.
Claim 23
Dependent Claim 20 words
The process of claim 20 wherein the alcohol is used in forming the starch slurry is ethanol or denatured ethanol.
Claim 24
Dependent Claim 30 words
The process of claim 21 wherein the slurry is heated to a temperature of about 325° to about 340° F. for a period of about 2 to about 5 minutes.
Claim 25
Dependent Claim 28 words
In an instant no-cook food composition wherein a starch material is used as the thickening agent, the improvement comprising the cold-water-swelling granular corn starch material of claim 1.
Claim 26
Dependent Claim 30 words
In an instant no-cook food composition wherein a starch material is used as the gelling or thickening agent, the improvement comprising the cold-water-swelling granular corn starch material of claim 4.
Claim 27
Dependent Claim 33 words
The improved instant food composition of claim 24 wherein the starch gelling or thickening agent is a cold-water-swelling granular corn starch material derived from ungelatinized corn starch which has not been chemically modified.
Claim 28
Dependent Claim 23 words
The improved instant food composition of claim 24 wherein the starch gelling or thickening agent exhibits a cold-water solubility of at least 70%.
Claim 29
Dependent Claim 54 words
A dessert formulation which will set to a resilient cleanly sliceable gel without cooking or chilling comprising a blended mixture of water or milk or a combination thereof, sweetening material, flavoring material, coloring material and the cold-water-swelling granular starch material of claim 4 in an amount effective to cause gelation of the dessert formulation.
Claim 30
Dependent Claim 52 words
The dessert formulation of claim 27 wherein the cold-water-swelling granular starch is (1) derived from ungelatinized corn starch which has not been reacted with chemical modifiers; (2) characterized by a cold-water solubility of at least about 70%, and (3) characterized further by a reduced native fat content of about 0.15% or less.
Claim 31
Dependent Claim 24 words
A dessert formulation of claim 27 wherein the cold-water-swelling granular starch material constitutes about 5 to about 8% by weight of the dessert formulation.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1987-08-14 1988-02-13 1988-08-14 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1991-08-14 1992-02-13 1992-08-14 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1995-08-14 1996-02-13 1996-08-14 $7700.00 Window Closed / Lapsed

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