Patent US4460491A successfully refreshed from Google Patents.
US4460491A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for preparing low silicate detergent compositions
Assignee: Lever Brothers Co
•
Filing: 1983-06-02
•
Granted: 1984-07-17
•
Expires: 2003-06-02
Abstract
Abstract The structure and hence the powder properties of spray-dried detergent powders are improved by the incorporation of a small amount of a succinate salt. In particular the invention is applicable to powders which are low in inherent structurants, especially to powders low in sodium silicate and in phosphate builder salts. Buccinic acid partially neutralized with sodium hydroxide is especially effective as a structuring aid.
Inventors
- 👤 Seeng D. Liem
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-06 15:17
CPC Classifications
C; C11; C11D; C11D3/00; C11D3/16; C11D3/20; C11D3/2075; C11D3/2082; C11D11/00; C11D11/02
Claims Analysis
Total Claims: 6
Claim 1
Independent Claim
103 words
A process for the preparation of a crisp, free-flowing detergent powder which contains each in an effective amount for structuring the powder, a phosphate salt up to 6% by weight calculated as phosphorus, and up to 4% by weight sodium silicate, which process comprises the steps of (a) forming an aqueous crutcher slurry comprising from about 2% to 25% anionic and from about 3% to 20% nonionic surfactant, (b) conducting pressurized slurry to spray nozzles, and (c) spray-drying the slurry to detergent powder, wherein the slurry comprises from 1 to 5% by weight, based on the spray-dried powder, of a water-soluble succinate salt.
Claim 2
Dependent Claim
103 words
A process for the preparation of a crisp, free-flowing detergent powder which contains each in an effective amount for structuring the powder, a phosphate salt up to 6% by weight calculated as phosphorus, and up to 4% by weight sodium silicate, which process comprises the steps of (a) forming an aqueous crutcher slurry comprising from about 2% to 25% anionic and from about 3% to 20% nonionic surfactant, (b) conducting pressurized slurry to spray nozzles, and (c) spray-drying the slurry to detergent powder, wherein the slurry comprises from 1 to 5% by weight, based on the spray-dried powder, of a water-soluble succinate salt.
Claim 3
Dependent Claim
19 words
A process according to claim 1, wherein the water-soluble succinate salt is incorporated into the slurry prior to pressurizing.
Claim 4
Dependent Claim
20 words
A process according to claim 1, wherein the water-soluble succinate salt is incorporated into the pressurized slurry prior to spray-drying.
Claim 5
Dependent Claim
18 words
A process according to claim 1, wherein the water-soluble succinate salt comprises completely or partially neutralized sodium succinate.
Claim 6
Dependent Claim
19 words
A process according to claim 1 wherein the nonionic surfactant is present from about 3% to 10% by weight.
References Cited (Backward Citations)
US3428690A
Cited
US3328314A
Cited
GB1365674A
Cited
US3962149A
Cited
US3985669A
Cited
US4000094A
Cited
US4072621A
Cited
US3998762A
Cited
US4140650A
Cited
US4180485A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1987-07-17 | 1988-01-16 | 1988-07-17 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1991-07-17 | 1992-01-16 | 1992-07-17 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1995-07-17 | 1996-01-16 | 1996-07-17 | $7700.00 | Window Closed / Lapsed |