Process for the manufacture of low D.E. maltodextrins

Claim 2

A process for producing a low D.E. starch hydrolyzate which comprises (1) liquefying non-waxy corn starch in the presence of an alpha amylase by heating at a temperature within the range of from about 104°-107° C., (2) maintaining the liquefied starch hydrolyzate of step (1) at a temperature above about 93° C. in the presence of alpha-amylase so as to dextrinize the hydrolyzate to a D.E. level within the range of from about 10-13, (3) terminating the reaction of step (2) by the addition of sufficient mineral acid to lower the pH of the dextrinized hydrolyzate to a level at which residual alpha-amylase is inactivated within the period of from about thirty to about sixty minutes while maintaining the hydrolyzate temperature at least above about 93° C., (4) refining the resulting hydrolyzate from step (3) while maintaining the hydrolyzate at a temperature of at least above about 76° C. during the refining operations, and (5) spray drying the refined hydrolyzate of step (4) so as to produce a dry free-flowing starch hydrolyzate.

Claim 3

The process of claim 1, wherein the pH of the starch hydrolyzate during step (2) is maintained within the range of from about pH 5 to about pH 6 and the temperature of the hydrolyzate is maitained in a range of from about 95° C. to about 98° C.

Claim 4

A process for producing a low D.E. starch hydrolyzate which comprises (1) liquefying non-waxy corn starch in the presence of an alpha-amylase by heating at a temperature within the range of from about 104°-107° C., (2) maintaining the liquefied starch hydrolyzate of step (1) at a temperature above about 93° C. in the presence of alpha-amylase so as to dextrinize the hydrolyzate to a D.E. level within the range of from about 10-13, (3) terminating the reaction of step (2) by the addition of sufficient mineral acid to lower the pH of the dextrinized hydrolyzate to a level at which residual alpha-amylase is inactivated within the period of from about thirty to about sixty minutes while maintaining the hydrolyzate temperature at least above about 93° C., (4) refining the resulting hydrolyzate from step (3) by treatment with activated carbon while maintaining the hydrolyzate at a temperature of at least above about 76° C., (5) removing the activated carbon by filtration while maintaining the hydrolyzate at a temperature of at least above about 76° C., (6) evaporating the hydrolyzate filtrate of step (5) while maintaining the hydrolyzate at a temperature of at least above about 76° C. to a dry solids content such that permits the hydrolyzate to be spray dried, and (7) spray drying the hydrolyzate so as to produce a dry free-flowing starch hydrolyzate.

Claim 5

A process for producing a low D.E. starch hydrolyzate which comprises (1) liquefying non-waxy corn starch in the presence of an alpha-amylase by heating at a temperature within the range of from about 104°-107° C., (2) maintaining the liquefied starch hydrolyzate of step (1) at a temperature above about 93° C. in the presence of alpha-amylase so as to dextrinize the hydrolyzate to a D.E. level within the range of from about 10-13, (3) terminating the reaction of step (2) by the addition of sufficient mineral acid to lower the pH of the dextrinized hydrolyzate to a level at which residual alpha-amylase is inactivated within the period of from about thirty to about sixty minutes while maintaining the hydrolyzate temperature at least above about 93° C., (4) refining the resulting hydrolyzate from step (3) by treatment with activated carbon while maintaining the hydrolyzate at a temperature of at least above about 76° C., (5) removing the activated carbon by filtration while maintaining the hydrolyzate at a temperature of at least above about 76° C., (6) evaporating the hydrolyzate filtrate of step (5) while maintaining the hydrolyzate at a temperature of at least above about 76° C. to a dry solids content such that permits the hydrolyzate to be spray dried, and (7) spray drying the hydrolyzate so as to produce a dry free-flowing starch hydrolyzate.