Patent US4418025A successfully refreshed from Google Patents.
← Back to Patent Explorer
US4418025A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for producing optically translucent mullite ceramic

Assignee: General Electric Co
•
Filing: 1982-05-25
•
Granted: 1983-11-29
•
Expires: 2002-05-25
📄 Original PDF 🌐 Google Patents 🔄 Sync Now

Abstract

Abstract Amorphous mixed oxide powder composed of from about 74 weight % to about 76.5 weight % Al 2 O 3 balance SiO 2 is pressed into a compact with a density of at least 1 g/cc and sintered in oxygen producing an optically translucent theoretically dense body of mullite.

Inventors

  • 👤 Svante Prochazka
  • 👤 Frederic J. Klug

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 15:22
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/01; C04B35/16; C04B35/18

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 228 words
A process for producing a polycrystalline mullite body optically translucent in the visible wave length which comprises providing an amorphous shapeless mixed oxide powder consisting essentially of from about 74 weight % to about 76.5 weight % Al 2 O 3 balance SiO 2 with a surface area ranging from about 100 square meters per gram to about 400 square meters per gram and a bulk density ranging from about 0.2 g/cc to about 0.3 g/cc containing a significant amount of water, calcining said powder at a temperature ranging from about 490° C. to about 1100° C. to remove water and any organic material therefrom leaving no significant amount thereof producing an amorphous shapeless mixed oxide powder consisting essentially of from about 74 weight % to about 76.5 weight % Al 2 O 3 balance SiO 2 , said calcining having no significant effect on the oxide composition or morphology of said powder, said calcined powder being pressable at about room temperature into a compact having a minimum density of 1.0 g/cc, pressing said calcined powder into a compact having a minimum density of 1.0 g/cc, and sintering said compact in an atmosphere of oxygen at a temperature ranging from about 1700° C. to about 1850° C. producing a sintered body of theoretical density based on the density of 3.16 g/cc±0.01 or 3.17 g/cc±0.01 for said mullite body.
Claim 2
Dependent Claim 228 words
A process for producing a polycrystalline mullite body optically translucent in the visible wave length which comprises providing an amorphous shapeless mixed oxide powder consisting essentially of from about 74 weight % to about 76.5 weight % Al 2 O 3 balance SiO 2 with a surface area ranging from about 100 square meters per gram to about 400 square meters per gram and a bulk density ranging from about 0.2 g/cc to about 0.3 g/cc containing a significant amount of water, calcining said powder at a temperature ranging from about 490° C. to about 1100° C. to remove water and any organic material therefrom leaving no significant amount thereof producing an amorphous shapeless mixed oxide powder consisting essentially of from about 74 weight % to about 76.5 weight % Al 2 O 3 balance SiO 2 , said calcining having no significant effect on the oxide composition or morphology of said powder, said calcined powder being pressable at about room temperature into a compact having a minimum density of 1.0 g/cc, pressing said calcined powder into a compact having a minimum density of 1.0 g/cc, and sintering said compact in an atmosphere of oxygen at a temperature ranging from about 1700° C. to about 1850° C. producing a sintered body of theoretical density based on the density of 3.16 g/cc±0.01 or 3.17 g/cc±0.01 for said mullite body.
Claim 3
Dependent Claim 35 words
A process according to claim 1 wherein said compact is prefired in oxygen or in a vacuum ranging from about 0.05 torr to about 1.0 torr at a temperature ranging up to about 1650° C.
Claim 4
Dependent Claim 22 words
A process to claim 1 wherein said Al 2 O 3 ranges from about 74.5 weight % to about 75.5 weight %.
Claim 5
Dependent Claim 49 words
A process according to claim 1 wherein said compact is prefired to impart strength thereto in air, argon, helium, nitrogen, oxygen and mixtures thereof as well as a partial vacuum at a temperature ranging up to about 1500° C., said prefiring having no significant deleterious effect on said compact.
Claim 6
Dependent Claim 222 words
A process for producing a polycrystalline mullite body optically translucent in the visible wave length which comprises providing an amorphous shapeless mixed oxide powder consisting esssentially of from about 74.5 weight % to about 75.5 weight % Al 2 O 3 balance SiO 2 with a surface area ranging from about 200 square meters per gram to about 300 square meters per gram and a bulk density ranging from about 0.2 g/cc to about 0.3 g/cc containing a significant amount of water, calcining said powder at a temperature ranging from about 500° C. to 700° C. to remove water and any organic material therefrom producing an amorphous shapeless mixed oxide powder consisting essentially of from about 74.5 weight % to about 75.5 weight % Al 2 O 3 balance SiO 2 , said calcining having no significant effect on the oxide composition or morphology of said powder, said calcined powder being pressable at about room temperature into a compact having a minimum density of 1.0 g/cc, pressing said calcined powder into a compact having a minimum density of 1.0 g/cc, and sintering said compact in an atmosphere of oxygen at a temperature ranging from about 1700° C. to about 1850° C. producing a sintered body of theoretical density based on the density of 3.16 g/cc±0.01 or 3.17 g/cc±0.01 for said mullite body.
Claim 7
Dependent Claim 222 words
A process for producing a polycrystalline mullite body optically translucent in the visible wave length which comprises providing an amorphous shapeless mixed oxide powder consisting esssentially of from about 74.5 weight % to about 75.5 weight % Al 2 O 3 balance SiO 2 with a surface area ranging from about 200 square meters per gram to about 300 square meters per gram and a bulk density ranging from about 0.2 g/cc to about 0.3 g/cc containing a significant amount of water, calcining said powder at a temperature ranging from about 500° C. to 700° C. to remove water and any organic material therefrom producing an amorphous shapeless mixed oxide powder consisting essentially of from about 74.5 weight % to about 75.5 weight % Al 2 O 3 balance SiO 2 , said calcining having no significant effect on the oxide composition or morphology of said powder, said calcined powder being pressable at about room temperature into a compact having a minimum density of 1.0 g/cc, pressing said calcined powder into a compact having a minimum density of 1.0 g/cc, and sintering said compact in an atmosphere of oxygen at a temperature ranging from about 1700° C. to about 1850° C. producing a sintered body of theoretical density based on the density of 3.16 g/cc±0.01 or 3.17 g/cc±0.01 for said mullite body.

References Cited (Backward Citations)

US4101615A Cited
US3989783A Cited
US4266978A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-11-28 1987-05-30 1987-11-29 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-11-28 1991-05-30 1991-11-29 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-11-28 1995-05-30 1995-11-29 $7700.00 Window Closed / Lapsed

Assigned Categories & Tags

No categories assigned to this patent yet.

Assign Category Tag