US4418025A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Process for producing optically translucent mullite ceramic
Assignee: General Electric Co
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Filing: 1982-05-25
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Granted: 1983-11-29
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Expires: 2002-05-25
Abstract
Abstract Amorphous mixed oxide powder composed of from about 74 weight % to about 76.5 weight % Al 2 O 3 balance SiO 2 is pressed into a compact with a density of at least 1 g/cc and sintered in oxygen producing an optically translucent theoretically dense body of mullite.
Inventors
- 👤 Svante Prochazka
- 👤 Frederic J. Klug
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-01 12:08
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/01; C04B35/16; C04B35/18
Claims Analysis
Total Claims: 7
Claim 1
Independent Claim
228 words
A process for producing a polycrystalline mullite body optically translucent in the visible wave length which comprises providing an amorphous shapeless mixed oxide powder consisting essentially of from about 74 weight % to about 76.5 weight % Al 2 O 3 balance SiO 2 with a surface area ranging from about 100 square meters per gram to about 400 square meters per gram and a bulk density ranging from about 0.2 g/cc to about 0.3 g/cc containing a significant amount of water, calcining said powder at a temperature ranging from about 490° C. to about 1100° C. to remove water and any organic material therefrom leaving no significant amount thereof producing an amorphous shapeless mixed oxide powder consisting essentially of from about 74 weight % to about 76.5 weight % Al 2 O 3 balance SiO 2 , said calcining having no significant effect on the oxide composition or morphology of said powder, said calcined powder being pressable at about room temperature into a compact having a minimum density of 1.0 g/cc, pressing said calcined powder into a compact having a minimum density of 1.0 g/cc, and sintering said compact in an atmosphere of oxygen at a temperature ranging from about 1700° C. to about 1850° C. producing a sintered body of theoretical density based on the density of 3.16 g/cc±0.01 or 3.17 g/cc±0.01 for said mullite body.
Claim 2
Dependent Claim
228 words
A process for producing a polycrystalline mullite body optically translucent in the visible wave length which comprises providing an amorphous shapeless mixed oxide powder consisting essentially of from about 74 weight % to about 76.5 weight % Al 2 O 3 balance SiO 2 with a surface area ranging from about 100 square meters per gram to about 400 square meters per gram and a bulk density ranging from about 0.2 g/cc to about 0.3 g/cc containing a significant amount of water, calcining said powder at a temperature ranging from about 490° C. to about 1100° C. to remove water and any organic material therefrom leaving no significant amount thereof producing an amorphous shapeless mixed oxide powder consisting essentially of from about 74 weight % to about 76.5 weight % Al 2 O 3 balance SiO 2 , said calcining having no significant effect on the oxide composition or morphology of said powder, said calcined powder being pressable at about room temperature into a compact having a minimum density of 1.0 g/cc, pressing said calcined powder into a compact having a minimum density of 1.0 g/cc, and sintering said compact in an atmosphere of oxygen at a temperature ranging from about 1700° C. to about 1850° C. producing a sintered body of theoretical density based on the density of 3.16 g/cc±0.01 or 3.17 g/cc±0.01 for said mullite body.
Claim 3
Dependent Claim
35 words
A process according to claim 1 wherein said compact is prefired in oxygen or in a vacuum ranging from about 0.05 torr to about 1.0 torr at a temperature ranging up to about 1650° C.
Claim 4
Dependent Claim
22 words
A process to claim 1 wherein said Al 2 O 3 ranges from about 74.5 weight % to about 75.5 weight %.
Claim 5
Dependent Claim
49 words
A process according to claim 1 wherein said compact is prefired to impart strength thereto in air, argon, helium, nitrogen, oxygen and mixtures thereof as well as a partial vacuum at a temperature ranging up to about 1500° C., said prefiring having no significant deleterious effect on said compact.
Claim 6
Dependent Claim
222 words
A process for producing a polycrystalline mullite body optically translucent in the visible wave length which comprises providing an amorphous shapeless mixed oxide powder consisting esssentially of from about 74.5 weight % to about 75.5 weight % Al 2 O 3 balance SiO 2 with a surface area ranging from about 200 square meters per gram to about 300 square meters per gram and a bulk density ranging from about 0.2 g/cc to about 0.3 g/cc containing a significant amount of water, calcining said powder at a temperature ranging from about 500° C. to 700° C. to remove water and any organic material therefrom producing an amorphous shapeless mixed oxide powder consisting essentially of from about 74.5 weight % to about 75.5 weight % Al 2 O 3 balance SiO 2 , said calcining having no significant effect on the oxide composition or morphology of said powder, said calcined powder being pressable at about room temperature into a compact having a minimum density of 1.0 g/cc, pressing said calcined powder into a compact having a minimum density of 1.0 g/cc, and sintering said compact in an atmosphere of oxygen at a temperature ranging from about 1700° C. to about 1850° C. producing a sintered body of theoretical density based on the density of 3.16 g/cc±0.01 or 3.17 g/cc±0.01 for said mullite body.
Claim 7
Dependent Claim
222 words
A process for producing a polycrystalline mullite body optically translucent in the visible wave length which comprises providing an amorphous shapeless mixed oxide powder consisting esssentially of from about 74.5 weight % to about 75.5 weight % Al 2 O 3 balance SiO 2 with a surface area ranging from about 200 square meters per gram to about 300 square meters per gram and a bulk density ranging from about 0.2 g/cc to about 0.3 g/cc containing a significant amount of water, calcining said powder at a temperature ranging from about 500° C. to 700° C. to remove water and any organic material therefrom producing an amorphous shapeless mixed oxide powder consisting essentially of from about 74.5 weight % to about 75.5 weight % Al 2 O 3 balance SiO 2 , said calcining having no significant effect on the oxide composition or morphology of said powder, said calcined powder being pressable at about room temperature into a compact having a minimum density of 1.0 g/cc, pressing said calcined powder into a compact having a minimum density of 1.0 g/cc, and sintering said compact in an atmosphere of oxygen at a temperature ranging from about 1700° C. to about 1850° C. producing a sintered body of theoretical density based on the density of 3.16 g/cc±0.01 or 3.17 g/cc±0.01 for said mullite body.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1986-11-28 | 1987-05-30 | 1987-11-29 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1990-11-28 | 1991-05-30 | 1991-11-29 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1994-11-28 | 1995-05-30 | 1995-11-29 | $7700.00 | Window Closed / Lapsed |