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Porous inorganic support material coated with an organic stationary phase, for use in chromatography, and process for its preparation

Assignee: Akzo NV
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Filing: 1981-06-29
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Granted: 1983-11-15
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Expires: 2001-06-29
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Abstract

Abstract The invention relates to support material usable as such in chromatography or as a starting material which, upon linkage to it of compounds containing ionic groups, ligands or biomacromolecules, can be used as ion exchanger, as a medium in affinity chromatography or in enzymatic reactions and consists of porous, inorganic silanized particles onto which there is covalently bonded an organic, stationary phase built up of (co)polymerized vinyl monomers containing amide groups, said inorganic particles having been silanized with an organo silane.

Inventors

  • 👤 Jan A. J. Schutijser

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-27 10:39
CPC Classifications
B; B01; B01J; B01J20/00; B01J20/281; B01J20/286; B01J20/22; B01J20/26; B01J20/261; B01J20/264; B01J20/265; B01J20/267; B01J20/28; B01J20/28054; B01J20/28057; B01J20/28078; B01J20/289; B01J20/30; B01J20/3092; B01J20/32; B01J20/3202; B01J20/3204; B01J20/3214; B01J20/3217; B01J20/3219; B01J20/3231; B01J20/3242; B01J20/3244; B01J20/3246; B01J20/3257; B01J20/3263; B01J20/3268; B01J20/327; B01J20/3276; B01J20/328; B01J20/3282; C; C08; C08F; C08F292/00; B01J2220/00; B01J2220/50; B01J2220/54; B01J2220/58; Y; Y10; Y10T; Y10T428/00; Y10T428/29; Y10T428/2982; Y10T428/2991; Y10T428/2993; Y10T428/2995; Y10T428/31504; Y10T428/31652; Y10T428/31663

Claims Analysis

Total Claims: 18
Claim 1
Independent Claim 275 words
A support material, usable as such in chromatography or as a starting material which, upon linkage to it of compounds containing ionic groups, ligands or biomacromolecules, can be used as ion exchanger, as a medium in affinity chromatography or in enzymatic reactions, consisting of porous, inorganic silanized particles onto which there is covalently bonded an organic, stationary phase built up of (co)polymerized vinyl monomers and containing amide groups, characterized in that (a) a hydroxyl-containing inorganic material has been silanized with an organo silane of the formula I ##STR12## wherein n=1-5; R 1 is halogen or alkoxy (1-10 C); R 2 and R 3 are each halogen, alkoxy (1-10 C), alkyl (1-3 C) or aryl (6-10 C), the halogen and alkoxy group in R 1 , R 2 and R 3 being capable of forming an --O--Si-bond between the silane and the inorganic material through its surface hydroxyl groups; and R 4 is amino, substituted amino, mercapto, an ester group or glycidoxy; and (B) the organic stationary phase is a crosslinked (co)polymer obtained by addition polymerization and built up of 0.1 to 140 μmoles of vinyl monomers per m 2 inorganic surface of the support material, said (co)polymer containing at least 0.1 μmoles amide groups per m 2 inorganic surface of the support material, and said vinyl monomers consisting wholly or partly of bifunctional vinyl monomers containing amide groups and having the formula II ##STR13## wherein R 5 and R 6 each are hydrogen or an organic group having up to 18 carbon atoms; R 7 is hydrogen or an organic group up to 20 carbon atoms; and m is an integer from 1 to 20.
Claim 2
Dependent Claim 275 words
A support material, usable as such in chromatography or as a starting material which, upon linkage to it of compounds containing ionic groups, ligands or biomacromolecules, can be used as ion exchanger, as a medium in affinity chromatography or in enzymatic reactions, consisting of porous, inorganic silanized particles onto which there is covalently bonded an organic, stationary phase built up of (co)polymerized vinyl monomers and containing amide groups, characterized in that (a) a hydroxyl-containing inorganic material has been silanized with an organo silane of the formula I ##STR12## wherein n=1-5; R 1 is halogen or alkoxy (1-10 C); R 2 and R 3 are each halogen, alkoxy (1-10 C), alkyl (1-3 C) or aryl (6-10 C), the halogen and alkoxy group in R 1 , R 2 and R 3 being capable of forming an --O--Si-bond between the silane and the inorganic material through its surface hydroxyl groups; and R 4 is amino, substituted amino, mercapto, an ester group or glycidoxy; and (B) the organic stationary phase is a crosslinked (co)polymer obtained by addition polymerization and built up of 0.1 to 140 μmoles of vinyl monomers per m 2 inorganic surface of the support material, said (co)polymer containing at least 0.1 μmoles amide groups per m 2 inorganic surface of the support material, and said vinyl monomers consisting wholly or partly of bifunctional vinyl monomers containing amide groups and having the formula II ##STR13## wherein R 5 and R 6 each are hydrogen or an organic group having up to 18 carbon atoms; R 7 is hydrogen or an organic group up to 20 carbon atoms; and m is an integer from 1 to 20.
Claim 3
Dependent Claim 46 words
A support material according to claim 1, characterized in that R 5 and R 6 each are hydrogen, an alkyl or cyclo-alkyl group up to 6 carbon atoms or an aryl group up to 10 carbon atoms; and m is an integer from 1 to 10.
Claim 4
Dependent Claim 26 words
A support material according to claim 2, characterized in that R 5 is hydrogen; R 6 is hydrogen or methyl; R 7 is hydrogen; and m=1.
Claim 5
Dependent Claim 32 words
A support material according to any one of claims 1, 2 or 3, characterized in that said vinyl monomers consist of at least 5 mol% of bifunctional vinyl monomers of formula II.
Claim 6
Dependent Claim 96 words
A support material according to claim 4, characterized in that the amide groups have been obtained partly by bringing into reaction (a) a spacer molecule, a ligand, a biomacromolecule, or a compound containing an ionic group, each having a reactive group and one or more amide groups, with a reactive group of a vinyl monomer or the crosslinked (co)polymer; or (b) a spacer molecule, a ligand, a biomacromolecule or a compound containing an ionic group, each having one or more amino and/or carboxyl groups, with one or more carboxyl and/or amino groups in the crosslinked (co)polymer.
Claim 7
Dependent Claim 29 words
A support material according to claim 5 characterized in that the (co)polymer contains 5 to 25 μmoles of amide groups per m 2 inorganic surface of the support material.
Claim 8
Dependent Claim 131 words
A support material according to claim 6, characterized in that the comonomer for obtaining the crosslinked copolymer is chosen from one or more vinyl monomers having a functional group and having the formula III ##STR14## wherein R 8 is H or CH 3 ; R 9 is --CH 2 NH 2 , ##STR15## X is halogen; R 10 = alkyl up to 10 carbon atoms, or glycidoxy; R 11 represents a functional group, which is linked to the carbonyl group and has the meaning of a hydroxyl group or one of the following groups ##STR16## wherein R 12 has the same meaning as R 11 and p represents an integer from 1 to 10, and the molecular weight of the vinyl comonomer having a functional group is not higher than 1000.
Claim 9
Dependent Claim 15 words
A support material according to claim 7 wherein, in formula III, R 9 is ##STR17##
Claim 10
Dependent Claim 19 words
A support material according to claim 7 wherein, in formula III, when R 9 is ##STR18## X is Br.
Claim 11
Dependent Claim 24 words
A support material according to claim 7 wherein, in formula III, when R 9 is --CH 2 OR 10 , R 10 is methyl.
Claim 12
Dependent Claim 26 words
A support material according to claim 7 wherein the vinyl comonomer having a functional group has a molecular weight in the range of 70 to 400.
Claim 13
Dependent Claim 45 words
A support material according to claim 7 wherein, in formula III, when R 9 is ##STR19## R 11 is linked to the carbonyl group via a spacer group, and the molecular weight of the vinyl comonomer having a functional group is not higher than 1000.
Claim 14
Dependent Claim 26 words
A support material according to claim 12 wherein the vinyl comonomer having a functional group has a molecular weight in the range of 70 to 400.
Claim 15
Dependent Claim 12 words
A support material according to claim 1 wherein, in formula I, n=3.
Claim 16
Dependent Claim 15 words
A support material according to claim 1, wherein, in formula I, R 4 is glycidoxy.
Claim 17
Dependent Claim 31 words
A support material according to claim 1, wherein in (B) the copolymer is built up of 5 to 25 μmoles of vinyl monomers per m 2 inorganic surface of support material.
Claim 18
Dependent Claim 23 words
A support material according to claim 1 wherein in the organo silane of formula I, R 4 is a ω-amino-alkyl (1-3C) - amino.

References Cited (Backward Citations)

US3984349A Cited
US3983299A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-11-14 1987-05-16 1987-11-15 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-11-14 1991-05-16 1991-11-15 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-11-14 1995-05-16 1995-11-15 $7700.00 Window Closed / Lapsed

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