US4405378A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Extraction of sucrose
Assignee: Honeywell UOP LLC
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Filing: 1981-09-28
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Granted: 1983-09-20
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Expires: 2001-09-28
Abstract
Abstract Sucrose which is found in molasses such as beet molasses or cane molasses may be selectively extracted therefrom by passing an aqueous solution of the molasses over an adsorbent comprising activated carbon powder bound with a binder material comprising a water permeable organic polymer. The sucrose will be selectively adsorbed thereon and separated from the mineral salts and betaine in the molasses. The sucrose is then removed from the adsorbent by treatment with a desorbent material comprising a water and methanol mixture.
Inventors
- 👤 Santi Kulprathipanja
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-30 07:22
CPC Classifications
C; C13; C13B; C13B20/00; C13B20/14; C13B20/148
Claims Analysis
Total Claims: 13
Claim 1
Independent Claim
131 words
A process for separating sucrose from an aqueous solution containing sucrose and at least one of the compounds selected from the group consisting of betaine and a mineral salt, which process comprises: (a) contacting said solution, at adsorption conditions, with an adsorbent comprising activated carbon powder bound with a binder material consisting essentially of a water permeable organic polymer selected from the group consisting of a cellulose nitrate, a cellulose ester and a mixture of a cellulose nitrate and cellulose ester, thereby selectively adsorbing said sucrose thereon; and (b) separating the solution from contact with said adsorbent, wherein the solution still contains said at least one of the compounds selected from the group consisting of betaine and a mineral salt; and thereafter recovering said sucrose by desorption thereof from said adsorbent.
Claim 2
Dependent Claim
131 words
A process for separating sucrose from an aqueous solution containing sucrose and at least one of the compounds selected from the group consisting of betaine and a mineral salt, which process comprises: (a) contacting said solution, at adsorption conditions, with an adsorbent comprising activated carbon powder bound with a binder material consisting essentially of a water permeable organic polymer selected from the group consisting of a cellulose nitrate, a cellulose ester and a mixture of a cellulose nitrate and cellulose ester, thereby selectively adsorbing said sucrose thereon; and (b) separating the solution from contact with said adsorbent, wherein the solution still contains said at least one of the compounds selected from the group consisting of betaine and a mineral salt; and thereafter recovering said sucrose by desorption thereof from said adsorbent.
Claim 3
Dependent Claim
42 words
The process as set forth in claim 1 in which said adsorption conditions include a temperature in the range of from about 20° C. to about 200° C. and a pressure in the range of from about atmospheric to about 500 psig.
Claim 4
Dependent Claim
21 words
The process as set forth in claim 2 is further characterized in that said process is effected in the liquid phase.
Claim 5
Dependent Claim
26 words
The process as set forth in claim 1 in which said sucrose is recovered from said adsorbent by desorption with a mixture of water and methanol.
Claim 6
Dependent Claim
22 words
The process as set forth in claim 4 wherein the methanol and water are mixed in a volume ratio of about 1.0:1.0.
Claim 7
Dependent Claim
15 words
The process as set forth in claim 1 in which said aqueous solution is molasses.
Claim 8
Dependent Claim
148 words
A process for separating sucrose from an aqueous solution of sucrose and at least one of the compounds selected from the group consisting of betaine and a mineral salt, which process comprises the steps of: (a) contacting said sugar source, at adsorption conditions to selectively adsorb said sucrose, with an adsorbent comprising activated carbon bound with a binder material consisting essentially of a water permeable organic polymer selected from the group consisting of a cellulose nitrate, a cellulose ester and a mixture of said cellulose nitrate and cellulose ester; (b) removing from the adsorbent a raffinate stream comprising at least one of the compounds selected from the group consisting of a mineral salt and betaine; (c) contacting said adsorbent at desorption conditions with a desorbent material to effect the desorption of said sucrose from said adsorbent; and (d) removing from said adsorbent an extraction stream comprising said sucrose.
Claim 9
Dependent Claim
148 words
A process for separating sucrose from an aqueous solution of sucrose and at least one of the compounds selected from the group consisting of betaine and a mineral salt, which process comprises the steps of: (a) contacting said sugar source, at adsorption conditions to selectively adsorb said sucrose, with an adsorbent comprising activated carbon bound with a binder material consisting essentially of a water permeable organic polymer selected from the group consisting of a cellulose nitrate, a cellulose ester and a mixture of said cellulose nitrate and cellulose ester; (b) removing from the adsorbent a raffinate stream comprising at least one of the compounds selected from the group consisting of a mineral salt and betaine; (c) contacting said adsorbent at desorption conditions with a desorbent material to effect the desorption of said sucrose from said adsorbent; and (d) removing from said adsorbent an extraction stream comprising said sucrose.
Claim 10
Dependent Claim
49 words
The process as set forth in claim 7 in which said adsorption and desorption conditions include a temperature in the range of from about 20° C. to about 200° C. and a pressure in the range of from about atmospheric to about 500 psig to ensure a liquid phase.
Claim 11
Dependent Claim
20 words
The process as set forth in claim 7 in which said desorbent material is a mixture of water and methanol.
Claim 12
Dependent Claim
22 words
The process as set forth in claim 9 wherein the methanol and water are mixed in a volume ratio of about 1.0:1.0.
Claim 13
Dependent Claim
15 words
The process as set forth in claim 7 in which said aqueous solution is molasses.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1986-09-19 | 1987-03-21 | 1987-09-20 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1990-09-19 | 1991-03-21 | 1991-09-20 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1994-09-19 | 1995-03-21 | 1995-09-20 | $7700.00 | Window Closed / Lapsed |