Patent US4403490A successfully refreshed from Google Patents.
US4403490A
Expired / Lapsed
US
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Metal forming lubricant and method of use thereof
Assignee: E M Corp
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Filing: 1981-06-24
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Granted: 1983-09-13
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Expires: 2001-06-24
Abstract
Abstract The present invention relates to a lubricant for use in the drawing and ironing of black plate steel during the manufacture of enclosed containers such as cans. In particular, the lubricant is applied to that portion of the black plate steel which ultimately becomes the outside surface of the can body. The lubricant comprises an aqueous solution of an active component, such as a major portion of molybdenum disulfide, together with minor amounts of waxes and other materials. In performing the method of the present invention, a lubricant system is employed. The lubricant system comprises a dual lubricant coating. The first, or outside, coating is applied to that portion of the black plate steel which ultimately becomes the outside surface of the can body. The outside coating is applied, such as by spraying or gravure or offset printing, at a rate of about 25 to about 200 milligrams per squre foot of steel surface. This coating is dried, as through the use of a heat source, such as infrared heat or hot air. A second, or inside, coating is applied to that portion of the black plate steel which ultimately becomes the inside surface of the can body. The inside coating may also be applied to the surface of the black plate steel in a manner similar to that used for the application of the outside coating. After the can body is produced, the outside and inside lubricants must be totally removed. Such removal may be achieved by washing the can bodies in an alkaline solution (pH about 7.5 to 11.5) having a temperature of about 140° to about 160° F.
Inventors
- 👤 Donald J. Sargent
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-30 23:36
CPC Classifications
C; C10; C10M; C10M173/00; C10M101/00; C10M101/02; C10M101/04; C10M103/00; C10M103/06; C10M105/00; C10M105/08; C10M105/22; C10M105/24; C10M105/32; C10M105/40; C10M105/56; C10M105/58; C10M105/60; C10M105/62; C10M107/00; C10M107/02; C10M107/20; C10M107/30; C10M107/32; C10M107/34; C10M107/38; C10M107/50; C10M173/02; C10M2201/00; C10M2201/02; C10M2201/06; C10M2201/062; C10M2201/065; C10M2201/0653; C10M2201/066; C10M2201/0663; C10M2205/00; C10M2205/02; C10M2205/0206; C10M2205/14; C10M2205/16; C10M2207/00; C10M2207/10; C10M2207/12; C10M2207/125; C10M2207/126; C10M2207/18; C10M2207/20; C10M2207/28; C10M2207/287; C10M2207/289; C10M2207/40; C10M2209/00; C10M2209/02; C10M2209/08; C10M2209/086; C10M2209/10; C10M2209/101; C10M2209/103; C10M2209/104; C10M2215/00; C10M2215/02; C10M2215/04; C10M2215/042; C10M2215/22; C10M2215/225; C10M2215/226; C10M2229/00; C10M2229/02; C10M2229/04; C10M2229/041; C10M2229/05; C10N; C10N2010/00; C10N2010/02; C10N2040/00; C10N2040/20; C10N2040/24; C10N2040/242; C10N2040/243; C10N2040/244; C10N2040/245; C10N2040/246
Claims Analysis
Total Claims: 13
Claim 1
Independent Claim
89 words
A composition for use as a lubricant in metal forming operations using black plate steel comprising: 2.0 to 10.0 percent emulsifiable microcrystalline wax, 3.5 to 11.75 percent refined microcrystalline wax, 0.2 to 1.0 percent unsaturated fatty acid, 0.75 to 3.5 percent nonylphenoxypolyethoxy ethanol, 0.4 to 1.75 percent amines, 24.0 to 32.0 percent of a compound comprising an anion selected from Group VIb of the Periodic Table and a cation selected from Group VIa of the Periodic Table, 8.5 to 11.5 percent synthetic wax emulsion and the remainder distilled water.
Claim 2
Dependent Claim
89 words
A composition for use as a lubricant in metal forming operations using black plate steel comprising: 2.0 to 10.0 percent emulsifiable microcrystalline wax, 3.5 to 11.75 percent refined microcrystalline wax, 0.2 to 1.0 percent unsaturated fatty acid, 0.75 to 3.5 percent nonylphenoxypolyethoxy ethanol, 0.4 to 1.75 percent amines, 24.0 to 32.0 percent of a compound comprising an anion selected from Group VIb of the Periodic Table and a cation selected from Group VIa of the Periodic Table, 8.5 to 11.5 percent synthetic wax emulsion and the remainder distilled water.
Claim 3
Dependent Claim
27 words
The composition of claim 1, wherein the said Group VIa/Group VIb compound is selected from the group comprising molybdenum disulfide, molybdenum diselenide, tungsten disulfide and tungsten diselenide.
Claim 4
Dependent Claim
12 words
The composition of claim 1 further including 0 to 0.25 percent surfactant.
Claim 5
Dependent Claim
13 words
The composition of claim 1 further including 0 to 0.02 percent silicone antifoam.
Claim 6
Dependent Claim
19 words
The composition of claim 2 further including 0 to 0.025 percent surfactant and 0 to 0.02 percent silicone antifoam.
Claim 7
Dependent Claim
223 words
In a method of forming two piece cans from black plate steel in which a blank is produced from the black plate steel and the blank is subjected to drawing and ironing operations to produce an elongated can body, the improvement comprising the additional steps of: a. prior to the drawing operation, coating the portion of the black plate steel which ultimately becomes the exterior of the can body with a first coating lubricant, said first coating lubricant comprising 2.0 to 10.0 percent emulsifiable microcrystalline wax, 3.5 to 11.75 percent refined microcrystalline wax, 0.2 to 1.0 percent unsaturated fatty acid, 0.75 to 3.5 percent nonylphenoxypolyethoxy ethanol, 0.4 to 1.75 percent amines, 24.0 to 32.0 percent of a compound comprising an anion selected from Group VIb of the Periodic Table and a cation selected from Group VIa of the Periodic Table, 8.5 to 11.5 percent synthetic wax emulsion and the remainder distilled water; b. drying the first coating lubricant; c. coating the portion of the black plate steel which ultimately becomes the interior of the can body with a second coating lubricant, said second coating lubricant comprising 5.0 to 20.0 percent synthetic wax emulsion and the remainder distilled water; and d. after the ironing operation, removing said first and second coating lubricants by washing the elongated, enclosed can body in a slightly alkaline solution.
Claim 8
Dependent Claim
223 words
In a method of forming two piece cans from black plate steel in which a blank is produced from the black plate steel and the blank is subjected to drawing and ironing operations to produce an elongated can body, the improvement comprising the additional steps of: a. prior to the drawing operation, coating the portion of the black plate steel which ultimately becomes the exterior of the can body with a first coating lubricant, said first coating lubricant comprising 2.0 to 10.0 percent emulsifiable microcrystalline wax, 3.5 to 11.75 percent refined microcrystalline wax, 0.2 to 1.0 percent unsaturated fatty acid, 0.75 to 3.5 percent nonylphenoxypolyethoxy ethanol, 0.4 to 1.75 percent amines, 24.0 to 32.0 percent of a compound comprising an anion selected from Group VIb of the Periodic Table and a cation selected from Group VIa of the Periodic Table, 8.5 to 11.5 percent synthetic wax emulsion and the remainder distilled water; b. drying the first coating lubricant; c. coating the portion of the black plate steel which ultimately becomes the interior of the can body with a second coating lubricant, said second coating lubricant comprising 5.0 to 20.0 percent synthetic wax emulsion and the remainder distilled water; and d. after the ironing operation, removing said first and second coating lubricants by washing the elongated, enclosed can body in a slightly alkaline solution.
Claim 9
Dependent Claim
225 words
In a method of forming two piece cans from black plate steel in which a blank is produced from the black plate steel and the blank is subjected to drawing and ironing operations to produce an elongated can body, the improvement comprising the additional steps of: a. prior to the drawing operation, coating the portion of the black plate steel which ultimately becomes the exterior of the can body with a first coating lubricant, said first coating lubricant comprising 2.0 to 10.0 percent emulsifiable microcrystalline wax, 3.5 to 11.75 percent refined microcrystalline wax, 0.2 to 1.0 percent unsaturated fatty acid, 0.75 to 3.5 percent nonylphenoxypolyethoxy ethanol, 0.4 to 1.75 percent amines, 24.0 to 32.0 percent of a compound comprising an anion selected from Group VIb of the Periodic Table and a cation selected from Group VIa of the Periodic Table, 8.5 to 11.5 percent synthetic wax emulsion and the remainder distilled water; b. coating the portion of the black plate steel which ultimately becomes the interior of the can body with a second coating lubricant, said second coating lubricant comprising 5.0 to 20.0 percent synthetic wax emulsion and the remainder distilled water; c. drying the first and second coating lubricants; and d. after the ironing operation, removing the first and second coating lubricants by washing the elongated, enclosed can body in a slightly alkaline solution.
Claim 10
Dependent Claim
225 words
In a method of forming two piece cans from black plate steel in which a blank is produced from the black plate steel and the blank is subjected to drawing and ironing operations to produce an elongated can body, the improvement comprising the additional steps of: a. prior to the drawing operation, coating the portion of the black plate steel which ultimately becomes the exterior of the can body with a first coating lubricant, said first coating lubricant comprising 2.0 to 10.0 percent emulsifiable microcrystalline wax, 3.5 to 11.75 percent refined microcrystalline wax, 0.2 to 1.0 percent unsaturated fatty acid, 0.75 to 3.5 percent nonylphenoxypolyethoxy ethanol, 0.4 to 1.75 percent amines, 24.0 to 32.0 percent of a compound comprising an anion selected from Group VIb of the Periodic Table and a cation selected from Group VIa of the Periodic Table, 8.5 to 11.5 percent synthetic wax emulsion and the remainder distilled water; b. coating the portion of the black plate steel which ultimately becomes the interior of the can body with a second coating lubricant, said second coating lubricant comprising 5.0 to 20.0 percent synthetic wax emulsion and the remainder distilled water; c. drying the first and second coating lubricants; and d. after the ironing operation, removing the first and second coating lubricants by washing the elongated, enclosed can body in a slightly alkaline solution.
Claim 11
Dependent Claim
28 words
The method of claim 6 or 7 wherein the said Group VIa/VIb compound is selected from the group comprising molybdenum disulfide, molybdenum diselenide, tungsten disulfide and tungsten diselenide.
Claim 12
Dependent Claim
25 words
The method of claim 8 wherein the said first coating lubricant further includes 0 to 0.25 percent surfactant and 0 to 0.02 percent silicone antifoam.
Claim 13
Independent Claim
26 words
The method of claims 6 or 7 where said first coating lubricant further includes 0 to 0.25 percent surfactant and 0 to 0.02 percent silicone antifoam.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1986-09-12 | 1987-03-14 | 1987-09-13 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1990-09-12 | 1991-03-14 | 1991-09-13 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1994-09-12 | 1995-03-14 | 1995-09-13 | $7700.00 | Window Closed / Lapsed |