Patent US4401643A successfully refreshed from Google Patents.
US4401643A
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Preparation of finely divided barium ferrite of high coercivity
Assignee: BASF SE
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Filing: 1981-10-20
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Granted: 1983-08-30
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Expires: 2001-10-20
Abstract
Abstract A process for the preparation of barium ferrite of the formula BaFe 12 O 19 by reacting an aqueous solution or suspension of a barium salt and an aqueous solution of an iron(III) salt with an aqueous sodium carbonate solution, removing the solvent, heating the dry salt mixture to below the melting point of the sodium salt present, but to not less than 680° C., and isolating the resulting finely divided, platelet-like barium ferrite from the barium ferrite/sodium salt mixture by leaching with water.
Inventors
- 👤 Hartmut Hibst
- 👤 Helmut Jakusch
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-01 18:58
CPC Classifications
C; C01; C01G; C01G49/00; C01G49/0018; C01G49/0036; G; G11; G11B; G11B5/00; G11B5/62; G11B5/68; G11B5/70; G11B5/706; G11B5/70626; C01P; C01P2004/00; C01P2004/20; C01P2004/60; C01P2004/62; C01P2006/00; C01P2006/12; C01P2006/42
Claims Analysis
Total Claims: 4
Claim 1
Independent Claim
145 words
A process for the preparation of barium ferrite of the formula BaFe 12 Fe 19 which comprises: (a) mixing an aqueous solution of a barium compound selected from the group consisting of barium chloride, barium sulfate and barium carbonate with an aqueous solution or an iron(III) compound selected from the group consisting of iron(III) chloride and iron(III) sulfate; (b) reacting the mixture formed in step (a) with an aqueous sodium carbonate solution; (c) completely dehydrating the resulting mixture from step (b) which consists essentially of sparingly soluble barium compound and iron(III) carbonate in an aqueous sodium salt solution; (d) heating the dry salt mixture from step (c) at a temperature above 680° C. but below the melting point of the sodium salt present; and (e) leaching the resulting product with water to dissolve the sodium salt and to isolate the finely divided, platelet-like barium ferrite.
Claim 2
Dependent Claim
145 words
A process for the preparation of barium ferrite of the formula BaFe 12 Fe 19 which comprises: (a) mixing an aqueous solution of a barium compound selected from the group consisting of barium chloride, barium sulfate and barium carbonate with an aqueous solution or an iron(III) compound selected from the group consisting of iron(III) chloride and iron(III) sulfate; (b) reacting the mixture formed in step (a) with an aqueous sodium carbonate solution; (c) completely dehydrating the resulting mixture from step (b) which consists essentially of sparingly soluble barium compound and iron(III) carbonate in an aqueous sodium salt solution; (d) heating the dry salt mixture from step (c) at a temperature above 680° C. but below the melting point of the sodium salt present; and (e) leaching the resulting product with water to dissolve the sodium salt and to isolate the finely divided, platelet-like barium ferrite.
Claim 3
Dependent Claim
34 words
The process of claim 1, wherein barium chloride and iron(III) chloride are employed, so that sodium chloride is formed as the sodium salt component, and heating is effected at from 680° to 800° C.
Claim 4
Dependent Claim
37 words
The process of claim 1, wherein BaCO 3 or BaSO 4 and iron(III) sulfate are employed, so that sodium sulfate is formed as the sodium salt component, and heating is effected at from 680° to 880° C.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1986-08-29 | 1987-02-28 | 1987-08-30 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1990-08-29 | 1991-02-28 | 1991-08-30 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1994-08-29 | 1995-02-28 | 1995-08-30 | $7700.00 | Window Closed / Lapsed |