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Preparation of finely divided barium ferrite of high coercivity

Assignee: BASF SE
•
Filing: 1981-10-20
•
Granted: 1983-08-30
•
Expires: 2001-10-20
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Abstract

Abstract A process for the preparation of barium ferrite of the formula BaFe 12 O 19 by reacting an aqueous solution or suspension of a barium salt and an aqueous solution of an iron(III) salt with an aqueous sodium carbonate solution, removing the solvent, heating the dry salt mixture to below the melting point of the sodium salt present, but to not less than 680° C., and isolating the resulting finely divided, platelet-like barium ferrite from the barium ferrite/sodium salt mixture by leaching with water.

Inventors

  • 👤 Hartmut Hibst
  • 👤 Helmut Jakusch

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-01 18:58
CPC Classifications
C; C01; C01G; C01G49/00; C01G49/0018; C01G49/0036; G; G11; G11B; G11B5/00; G11B5/62; G11B5/68; G11B5/70; G11B5/706; G11B5/70626; C01P; C01P2004/00; C01P2004/20; C01P2004/60; C01P2004/62; C01P2006/00; C01P2006/12; C01P2006/42

Claims Analysis

Total Claims: 4
Claim 1
Independent Claim 145 words
A process for the preparation of barium ferrite of the formula BaFe 12 Fe 19 which comprises: (a) mixing an aqueous solution of a barium compound selected from the group consisting of barium chloride, barium sulfate and barium carbonate with an aqueous solution or an iron(III) compound selected from the group consisting of iron(III) chloride and iron(III) sulfate; (b) reacting the mixture formed in step (a) with an aqueous sodium carbonate solution; (c) completely dehydrating the resulting mixture from step (b) which consists essentially of sparingly soluble barium compound and iron(III) carbonate in an aqueous sodium salt solution; (d) heating the dry salt mixture from step (c) at a temperature above 680° C. but below the melting point of the sodium salt present; and (e) leaching the resulting product with water to dissolve the sodium salt and to isolate the finely divided, platelet-like barium ferrite.
Claim 2
Dependent Claim 145 words
A process for the preparation of barium ferrite of the formula BaFe 12 Fe 19 which comprises: (a) mixing an aqueous solution of a barium compound selected from the group consisting of barium chloride, barium sulfate and barium carbonate with an aqueous solution or an iron(III) compound selected from the group consisting of iron(III) chloride and iron(III) sulfate; (b) reacting the mixture formed in step (a) with an aqueous sodium carbonate solution; (c) completely dehydrating the resulting mixture from step (b) which consists essentially of sparingly soluble barium compound and iron(III) carbonate in an aqueous sodium salt solution; (d) heating the dry salt mixture from step (c) at a temperature above 680° C. but below the melting point of the sodium salt present; and (e) leaching the resulting product with water to dissolve the sodium salt and to isolate the finely divided, platelet-like barium ferrite.
Claim 3
Dependent Claim 34 words
The process of claim 1, wherein barium chloride and iron(III) chloride are employed, so that sodium chloride is formed as the sodium salt component, and heating is effected at from 680° to 800° C.
Claim 4
Dependent Claim 37 words
The process of claim 1, wherein BaCO 3 or BaSO 4 and iron(III) sulfate are employed, so that sodium sulfate is formed as the sodium salt component, and heating is effected at from 680° to 880° C.

References Cited (Backward Citations)

US3113109A Cited
US3582266A Cited
US3634254A Cited
GB1317088A Cited
US3793443A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-08-29 1987-02-28 1987-08-30 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-08-29 1991-02-28 1991-08-30 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-08-29 1995-02-28 1995-08-30 $7700.00 Window Closed / Lapsed

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