US4399167A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Metal coating of abrasive particles
Assignee: Individual
•
Filing: 1981-02-12
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Granted: 1983-08-16
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Expires: 2001-02-12
Abstract
Abstract The invention provides a method of metal coating diamond or cubic boron nitride particles, the metal being capable of forming a chemical bond with the particles, including the steps of providing a mass of metal for the coating in powdered form in contact with the particles, heat treating the metal powder and the particles at a temperature below the melting point of the metal to deposit a layer of metal on the particles, and recovering the particles as discrete, metal coated particles, the heat treatment taking place in a non-oxidizing atmosphere and being chosen to allow chemical bond formation between the particles and the coating.
Inventors
- 👤 Noel J. Pipkin
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-28 21:13
CPC Classifications
C; C04; C04B; C04B41/00; C04B41/009; C04B20/00; C04B20/10; C04B20/1055; C04B41/45; C04B41/4584; C04B41/50; C04B41/51; C04B41/5133; C04B41/80; C04B41/81; C04B41/85; C04B41/88; C09; C09K; C09K3/00; C09K3/14; C09K3/1436; C09K3/1445
Claims Analysis
Total Claims: 11
Claim 1
Independent Claim
206 words
A method of metal coating diamond or cubic boron nitride particles, the metal being selected from the group consisting of titanium, manganese, chromium, vanadium, tungsten, molybdenum and niobium and being capable of forming a chemical bond with the particles, including the steps of providing a mass of metal for the coating in powdered form, of particle size in the range 125 to 37 microns and without having been subjected to an oxidation treatment, in contact with the particles so as to form a mixture consisting essentially of metal powder and the diamond or cubic boron nitride particles, with the metal powder present in a greater volume than the particles and with the particles being substantially uniformly distributed through the mass of metal powder, heat treating the metal powder and the particles in a non-oxidizing atmosphere at a temperature below the melting point of the metal by elevating the temperature of the powdered metal and the particles and maintaining the elevated temperature for a period of time sufficient to produce a loosely sintered mass and to allow the metal to deposit onto the particles and chemically bond thereto, and thereafter breaking up the loosely sintered mass and separating the metal-coated abrasive particles from the remaining metal particles.
Claim 2
Independent Claim
206 words
A method of metal coating diamond or cubic boron nitride particles, the metal being selected from the group consisting of titanium, manganese, chromium, vanadium, tungsten, molybdenum and niobium and being capable of forming a chemical bond with the particles, including the steps of providing a mass of metal for the coating in powdered form, of particle size in the range 125 to 37 microns and without having been subjected to an oxidation treatment, in contact with the particles so as to form a mixture consisting essentially of metal powder and the diamond or cubic boron nitride particles, with the metal powder present in a greater volume than the particles and with the particles being substantially uniformly distributed through the mass of metal powder, heat treating the metal powder and the particles in a non-oxidizing atmosphere at a temperature below the melting point of the metal by elevating the temperature of the powdered metal and the particles and maintaining the elevated temperature for a period of time sufficient to produce a loosely sintered mass and to allow the metal to deposit onto the particles and chemically bond thereto, and thereafter breaking up the loosely sintered mass and separating the metal-coated abrasive particles from the remaining metal particles.
Claim 3
Independent Claim
158 words
A method of coating diamond particles with titanium including the steps of providing a mass of titanium in powdered form of particle size in the range 125 to 37 microns in contact with the particles so as to form a mixture consisting essentially of titanium powder and the diamond or cubic boron nitride particles, with the metal powder present in a greater volume than the particles and with the particles being substantially uniformly distributed through the mass of metal powder, heat treating the mixture of titanium and diamond particles at a temperature below the melting point of titanium by elevating the temperature of the powdered titanium and the particles and maintaining the elevated temperature for a period of time sufficient to produce a loosely sintered mass and to allow the titanium to deposit onto the particles and chemically bond thereto, and thereafter breaking up the loosely sintered mass and separating the titanium-coated particles from the remaining titanium particles.
Claim 4
Independent Claim
158 words
A method of coating diamond particles with titanium including the steps of providing a mass of titanium in powdered form of particle size in the range 125 to 37 microns in contact with the particles so as to form a mixture consisting essentially of titanium powder and the diamond or cubic boron nitride particles, with the metal powder present in a greater volume than the particles and with the particles being substantially uniformly distributed through the mass of metal powder, heat treating the mixture of titanium and diamond particles at a temperature below the melting point of titanium by elevating the temperature of the powdered titanium and the particles and maintaining the elevated temperature for a period of time sufficient to produce a loosely sintered mass and to allow the titanium to deposit onto the particles and chemically bond thereto, and thereafter breaking up the loosely sintered mass and separating the titanium-coated particles from the remaining titanium particles.
Claim 5
Independent Claim
160 words
A method of metal coating abrasive particles of diamond or cubic boron nitride comprising: forming a mixture of the particles with a mass of powdered metal selected from the group consisting of titanium, manganese, chromium, vanadium, tungsten, molybdenum and niobium of particle size smaller than the abrasive particle size, such that the mixture consists essentially of the powdered metal and the abrasive particles, with the metal powder present in a greater volume than the particles and such that the abrasive particles are substantially uniformly distributed through the mass of metal powder; heating the mixture in a non-oxidising atmosphere to an elevated temperature below the melting point of the metal and sufficient to produce a loosely sintered mass and maintaining the elevated temperature for a period of time sufficient to allow the metal to deposit onto the particles and chemically bond thereto; and thereafter breaking up the loosely sintered mass and separating the metal-coated abrasive particles from the remaining metal particles.
Claim 6
Independent Claim
160 words
A method of metal coating abrasive particles of diamond or cubic boron nitride comprising: forming a mixture of the particles with a mass of powdered metal selected from the group consisting of titanium, manganese, chromium, vanadium, tungsten, molybdenum and niobium of particle size smaller than the abrasive particle size, such that the mixture consists essentially of the powdered metal and the abrasive particles, with the metal powder present in a greater volume than the particles and such that the abrasive particles are substantially uniformly distributed through the mass of metal powder; heating the mixture in a non-oxidising atmosphere to an elevated temperature below the melting point of the metal and sufficient to produce a loosely sintered mass and maintaining the elevated temperature for a period of time sufficient to allow the metal to deposit onto the particles and chemically bond thereto; and thereafter breaking up the loosely sintered mass and separating the metal-coated abrasive particles from the remaining metal particles.
Claim 7
Independent Claim
23 words
A method according to any one of claims 1, 2 or 3 wherein the temperature of heat treatment does not exceed 1000° C.
Claim 8
Independent Claim
26 words
A method according to any one of claims 1, 2 or 3 wherein the elevated temperature is maintained for a period of less than 60 minutes.
Claim 9
Independent Claim
25 words
A method according to any one of claims 1, 2 or 3 wherein the elevated temperature is maintained for a period of about 30 minutes.
Claim 10
Independent Claim
28 words
A method according to any one of claims 1, 2 or 3 wherein the non-oxidising atmosphere is an inert gas or vacuum of 10 -4 Torr or higher.
Claim 11
Independent Claim
27 words
A method according to any one of claims 1, 2 or 3 wherein the metal powder has a particle size in the range 88 to 74 microns.
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1986-08-15 | 1987-02-14 | 1987-08-16 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1990-08-15 | 1991-02-14 | 1991-08-16 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1994-08-15 | 1995-02-14 | 1995-08-16 | $7700.00 | Window Closed / Lapsed |