Patent US4384150A successfully refreshed from Google Patents.
US4384150A
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US
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Method of making either a softener for rubber mixtures or a furnace fuel oil
Assignee: Individual
•
Filing: 1981-08-20
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Granted: 1983-05-17
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Expires: 2001-08-20
Abstract
Abstract A method of making either a softener for rubber mixtures or a furnace fuel oil comprises the steps of heating a hydrocarbonaceous solvent and introducing thereinto waste from vulcanized or nonvulcanized rubbers under intensive stirring. Then the waste is thermally decomposed at a pressure of 5·10 2 to 25.10 5 n/m 2 , the hydrocarbonaceous solvent continuously circulating through the reaction mixture. The end product is separated from the formed suspension by distillation at a temperature of 200° to 560° C. and at a pressure of 10 to 2·10 5 n/m 2 in the presence of an inert gaseous agent.
Inventors
- 👤 Genrikh D. Lyakhevich
- 👤 Alexandr E. Sokolovsky
- 👤 Vasily G. Suzansky
- 👤 Vulf P. Kovalerchik
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-09 03:57
CPC Classifications
C; C10; C10G; C10G1/00; C10G1/10; C08; C08L; C08L21/00
Claims Analysis
Total Claims: 6
Claim 1
Independent Claim
214 words
A method of making either a softener for rubber mixtures or a furnace fuel oil, comprising the steps of: a. heating to a temperature of from 150° to 600° C. a hydrocarbonaceous solvent selected from the group consisting of oil fractions having boiling temperatures of 40° to 120° C., 50° to 250° C., 250° to 400° C. and 200° to 500° C., coke-chemical fractions having boiling temperatures of 320° to 535° C., and furnace fuel oils produced according to the presently claimed method; b. adding vulcanized or, olefinically unsaturated nonvulcanized waste rubber to said heated hydrocarbonaceous solvent under intensive stirring, wherein said waste rubber is added to said hydrocarbonaceous solvent in a ratio of 1:1 to 1:100 parts by mass; c. thermally decomposing said waste rubber at a pressure of 5·10 2 to 25·10 5 n/m 2 and at a temperature of 150° to 485° C. for 1 to 300 seconds, said hydrocarbonaceous solvent continuously circulating through the reaction mixture at a rate of 1 to 30 l/hr per 1 kg of the waste rubber; and d. separating the end product from the formed suspension by distillation at a temperature of 200° to 560° C. and at a pressure of 10 to 2·10 5 n/m 2 in the presence of an inert gaseous agent.
Claim 2
Dependent Claim
31 words
A method as claimed in claim 1, wherein used as the inert gaseous agent are nitrogen, steam, stack gases, methane, ethane, propane, hydrocarbonaceous C 3 -C 6 fraction or mixtures thereof.
Claim 3
Dependent Claim
35 words
A method as claimed in claim 1, wherein in the course of the distillation the inert gaseous agent is continuously fed at a rate of 0.01 to 90 l/hr per 1 kg of the suspension.
Claim 4
Dependent Claim
43 words
A method as claimed in claim 1, wherein in the course of making the furnace fuel oil the distillation process is carried out at a temperature of 250° to 560° C. and at a pressure of 10 to 1·10 5 n/m 2 .
Claim 5
Dependent Claim
33 words
A method as claimed in claim 4, wherein in the course of the thermal decomposition of said waste said hydrocarbonaceous solvent contains from 0.1 to 100% by mass of aromatic hydrocarbons and resins.
Claim 6
Dependent Claim
80 words
A method as claimed in claim 1, wherein in the course of making the softener for rubber mixtures the thermal decomposition of said waste is carried out at a temperature of 200° to 400° C. and at a pressure of 1·10 5 to 4·10 5 n/m 2 , and in the distillation process the temperature is maintained within the range of 200° to 400° C. and the pressure, within the range of 1·10 3 to 2·10 5 n/m 2 .
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1986-05-16 | 1986-11-15 | 1987-05-17 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1990-05-16 | 1990-11-15 | 1991-05-17 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1994-05-16 | 1994-11-15 | 1995-05-17 | $7700.00 | Window Closed / Lapsed |