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US4376652A Expired / Lapsed US ⏱️ 0.0 years remaining

High density high strength Si3 N4 ceramics prepared by pressureless sintering of amorphous Si3 N4 powder and Ti

Assignee: Clinical Product Development Ltd
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Filing: 1979-01-08
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Granted: 1983-03-15
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Expires: 1999-01-08
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Abstract

Abstract High purity fine particle size amorphous Si 3 N 4 powder compacts may be pressureless sintered to high density by the addition of from 100 to 1000 parts per million Ti to the powder prior to compaction.

Inventors

  • 👤 Sergej-Tomislav Buljan

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-31 10:26
CPC Classifications
C; C04; C04B; C04B35/00; C04B35/515; C04B35/58; C04B35/584

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 38 words
A powder mixture consisting essentially of amorphous Si 3 N 4 powder of average particle size below about 3 microns characterized in that the Si 3 N 4 powder contains about 100 to 1000 parts per million Ti.
Claim 2
Dependent Claim 38 words
A powder mixture consisting essentially of amorphous Si 3 N 4 powder of average particle size below about 3 microns characterized in that the Si 3 N 4 powder contains about 100 to 1000 parts per million Ti.
Claim 3
Dependent Claim 36 words
The powder mixture of claim 1 in which the Si 3 N 4 , powder consists of up to 5 weight percent crystalline Si 3 N 4 , remainder substantially amorphous Si 3 N 4 .
Claim 4
Dependent Claim 54 words
The powder mixture of claim 1 additionally containing up to 25 weight percent of at least one additive selected from the group consisting of MgO, CrN, Y 2 O 3 , HfO 2 , ZrO 2 , ZrN, La 2 O 3 , CeO 2 , SiO 2 and Al 2 O 3 .
Claim 5
Dependent Claim 12 words
A powder compact of the powder of claims 1, 2 or 3.
Claim 6
Dependent Claim 13 words
The powder compact of claim 4 in which a volatilizable additive is present.
Claim 7
Dependent Claim 19 words
A polycrystalline body of Si 3 N 4 obtained by the pressureless sintering of the compact of claim 4.

References Cited (Backward Citations)

US4097293A Cited
US4025351A Cited
JPS49128915A Cited
US4145224A Cited
US4117095A Cited
US4073845A Cited
US4043381A Cited
US4102698A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-03-14 1986-09-13 1987-03-15 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-03-14 1990-09-13 1991-03-15 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-03-14 1994-09-13 1995-03-15 $7700.00 Window Closed / Lapsed

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