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US4371691A Expired / Lapsed US ⏱️ 0.0 years remaining

Preparation of polycarbonate from specific crude bisphenols

Assignee: Bayer AG
•
Filing: 1980-07-09
•
Granted: 1983-02-01
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Expires: 2000-07-09
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Abstract

Abstract This disclosure relates to the processes for producing polycarbonates from specific crude bisphenols. The bisphenols are characterized in that immediately after their preparation they are subjected to (i) separation, of excess phenols and low-boiling substances, by means of an evaporator, and (ii) removal of monophenols by desorption. The invention also relates to high-molecular weight aromatic polycarbonates made of crude bisphenols and their use in a variety of applications.

Inventors

  • 👤 Gerhard Friedhofen
  • 👤 Volker Serini
  • 👤 Rainer Neumann
  • 👤 Dieter Freitag
  • 👤 Hans-Helmut Schwarz

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-28 10:11
CPC Classifications
C; C08; C08G; C08G64/00; C08G64/20; C08G64/22; C08G64/24; C07; C07C; C07C37/00; C07C37/11; C07C37/20; C07C37/68; C07C37/70; C07C37/74; C08G64/04; C08G64/06; C08L; C08L69/00

Claims Analysis

Total Claims: 7
Claim 1
Independent Claim 92 words
In the process for the preparation of a thermoplastic, aromatic, high-molecular weight polycarbonate from at least one crude bisphenol, the improvement comprising: (i) separating said at least one crude bisphenol, immediately after its preparation, from excess of at least one phenol and low boiling substance, in an evaporator at a temperature between 100° and 300° C., and under a pressure of between 0.05 and 1000 millibars, and (ii) subjecting said crude bisphenol to desorption using an inert gas to attain a presence therein of monophenols of less than 2.5 percent by weight.
Claim 2
Dependent Claim 92 words
In the process for the preparation of a thermoplastic, aromatic, high-molecular weight polycarbonate from at least one crude bisphenol, the improvement comprising: (i) separating said at least one crude bisphenol, immediately after its preparation, from excess of at least one phenol and low boiling substance, in an evaporator at a temperature between 100° and 300° C., and under a pressure of between 0.05 and 1000 millibars, and (ii) subjecting said crude bisphenol to desorption using an inert gas to attain a presence therein of monophenols of less than 2.5 percent by weight.
Claim 3
Dependent Claim 15 words
The process according to claim 1 wherein said temperature is between 150° and 250° C.
Claim 4
Dependent Claim 15 words
The process according to claim 1 wherein said pressure is between 0.5 and 500 millibars.
Claim 5
Dependent Claim 19 words
The process according to claim 1 wherein said at least one crude bisphenol has at least 2 alkyl substituents.
Claim 6
Dependent Claim 19 words
The process according to claim 1 wherein said at least one crude bisphenol has at least 4 alkyl substituents.
Claim 7
Dependent Claim 19 words
The process in accordance with claim 1 wherein said presence of monophenols is less than 0.5 percent by weight.

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1986-01-31 1986-08-02 1987-02-01 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1990-01-31 1990-08-02 1991-02-01 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1994-01-31 1994-08-02 1995-02-01 $7700.00 Window Closed / Lapsed

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