Patent US4366191A successfully refreshed from Google Patents.
US4366191A
Expired / Lapsed
US
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Method of increasing the strength of carbon and graphite members
Assignee: SGL Carbon SE
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Filing: 1978-01-19
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Granted: 1982-12-28
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Expires: 1998-01-19
Abstract
Abstract Increasing the strength and improving other properties of porous carbon or graphite bodies by immersing the porous body in a mixture containing 35-70% hardenable resin and 30 to 65% volatile solvent to impregnate pores. The impregnated porous body is heated to 120 DEG to 180 DEG C. to harden the resin. Carbonization of the body is effected by heating in an inert atmosphere at a rate of at least 3 K/hr to 800 DEG -1300 DEG C. Improved strength bodies are obtained with a single impregnation and single carbonizing step.
Inventors
- 👤 Guido Gistinger
- 👤 Manfred Schmid
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-31 15:31
CPC Classifications
C; C04; C04B; C04B41/00; C04B41/009; C04B35/00; C04B35/515; C04B35/52; C04B35/521; C04B41/45; C04B41/46; C04B41/48; C04B41/4811; C04B41/50; C04B41/5001
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
167 words
Method of increasing the strength of a porous carbon or graphite body formed from a mixture of granular carbon-containing substances with a carbonizable binder and heating in the absence of air to carbonize the binder which comprises subjecting said body to a single resin impregnation and carbonization by (a) immersing the porous body in a mixture in which 35 to 70% by weight of a hardenable resin containing an aldehyde, selected from the group consisting of phenol-formaldehyde resins, furan resins and melamine resins is admixed with 30 to 65% by weight of a volatile liquid, organic solvent and in the absence of colloidal graphite, to impregnate the pores of the porous body with said mixture; (b) Heating the impregnated porous body to a temperature of 120° to 180° C. to effect hardening the resin in said pores; and (c) carbonizing the impregnating medium by heating in an inert or reducing atmosphere at a rate of at least 3 K/hr to a temperature of 800° to 1300° C.
Claim 2
Dependent Claim
167 words
Method of increasing the strength of a porous carbon or graphite body formed from a mixture of granular carbon-containing substances with a carbonizable binder and heating in the absence of air to carbonize the binder which comprises subjecting said body to a single resin impregnation and carbonization by (a) immersing the porous body in a mixture in which 35 to 70% by weight of a hardenable resin containing an aldehyde, selected from the group consisting of phenol-formaldehyde resins, furan resins and melamine resins is admixed with 30 to 65% by weight of a volatile liquid, organic solvent and in the absence of colloidal graphite, to impregnate the pores of the porous body with said mixture; (b) Heating the impregnated porous body to a temperature of 120° to 180° C. to effect hardening the resin in said pores; and (c) carbonizing the impregnating medium by heating in an inert or reducing atmosphere at a rate of at least 3 K/hr to a temperature of 800° to 1300° C.
Claim 3
Dependent Claim
20 words
Method according to claim 1, wherein the volatile solvent is selected from the group consisting of alcohols, ethers and ketones.
Claim 4
Dependent Claim
22 words
Method according to claim 1, wherein there is 45 to 55% by weight hardenable resin and 45 to 55% by weight solvent.
Claim 5
Dependent Claim
12 words
Method according to claim 1, wherein the phenol-formaldehyde resin is a novolak.
Claim 6
Dependent Claim
12 words
Method according to claim 3, wherein the phenol-formaldehyde resin is a novolak.
Claim 7
Dependent Claim
19 words
Method according to claim 1, wherein carbonizing is effected by heating at a rate of at least 4 K/hr.
Claim 8
Dependent Claim
19 words
Method according to claim 3 wherein carbonizing is effected by heating at a rate of at least 4 K/hr.
Claim 9
Dependent Claim
19 words
Method according to claim 4, wherein carbonizing is effected by heating at a rate of at least 4 K/hr.
References Cited (Backward Citations)
GB992085A
Cited
US3462289A
Cited
US3810780A
Cited
US3917884A
Cited
FR2276913A1
Cited
US4100322A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1985-12-27 | 1986-06-28 | 1986-12-28 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1989-12-27 | 1990-06-28 | 1990-12-28 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1993-12-27 | 1994-06-28 | 1994-12-28 | $7700.00 | Window Closed / Lapsed |