Patent US4366138A successfully refreshed from Google Patents.
US4366138A
Expired / Lapsed
US
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Carbon black useful for pigment for black lacquers
Assignee: Evonik Operations GmbH
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Filing: 1981-06-01
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Granted: 1982-12-28
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Expires: 2001-06-01
Abstract
Abstract An oxidized carbon black (gas black) is prepared within the MCC (medium color channel black) area showing primary particle sizes of an average diameter of 16 to 18 nm and a content of volatiles of at least 15% which, as secondary characteristics, has a specific surface area (BET) of 300 to 420 m2/g, an oil absorption (stiff paste) conducted on carbon black powder of 430 to 560 g/100 g, an oil absorption (stiff paste) conducted on carbon black beads of 370 to 450 g/100 g, a pH value of 2 to 5, a nigrometer index of 68 to 72 and a maximum content of volatiles of 25%. The carbon black is used as a pigment in high jet black lacquers.
Inventors
- 👤 Edith Eisenmenger
- 👤 Richard Engel
- 👤 Gerhard Kuhner
- 👤 Reinhold Reck
- 👤 Hans Schaefer
- 👤 Manfred Voll
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-24 05:58
CPC Classifications
C; C09; C09C; C09C1/00; C09C1/44; C09C1/48; C09C1/56; C09C1/565; C01; C01P; C01P2004/00; C01P2004/60; C01P2004/64; C01P2006/00; C01P2006/12; C01P2006/19
Claims Analysis
Total Claims: 5
Claim 1
Independent Claim
169 words
An oxidized channel type carbon black within the MCC, medium color channel black, area comprising finely divided primary particles with an average diameter of 16 to 18 nm a content of volatiles of at least 15% and at maximum of 25% and having the following secondary characteristics: ______________________________________
Specific surface area (BET)
300-420 m.sup.2 /g
Oil absorption (stiff paste)
conducted on carbon black
powder 430-560 g/100 g
pH value 2-5
Nigrometer index 68-72
______________________________________ said black having been produced from gas carbon black by burning a carrier gas loaded with oil to produce a gas carbon black having a nigrometer index of 68 to 73 corresponding to a mean particle size in the range of 16 to 18 nm and the following secondary characteristics: ______________________________________
Specific surface area (BET)
185-240 m.sup.2 /g
Volatiles 4.5-7.5%
Oil absorption conducted
on carbon black powder
640-740 g/100 g
pH 3-5
______________________________________ and thereafter subjecting said black to oxidation as an after treatment at a temperature not exceeding a maximal temperature of 300° C.
Claim 2
Dependent Claim
169 words
An oxidized channel type carbon black within the MCC, medium color channel black, area comprising finely divided primary particles with an average diameter of 16 to 18 nm a content of volatiles of at least 15% and at maximum of 25% and having the following secondary characteristics: ______________________________________
Specific surface area (BET)
300-420 m.sup.2 /g
Oil absorption (stiff paste)
conducted on carbon black
powder 430-560 g/100 g
pH value 2-5
Nigrometer index 68-72
______________________________________ said black having been produced from gas carbon black by burning a carrier gas loaded with oil to produce a gas carbon black having a nigrometer index of 68 to 73 corresponding to a mean particle size in the range of 16 to 18 nm and the following secondary characteristics: ______________________________________
Specific surface area (BET)
185-240 m.sup.2 /g
Volatiles 4.5-7.5%
Oil absorption conducted
on carbon black powder
640-740 g/100 g
pH 3-5
______________________________________ and thereafter subjecting said black to oxidation as an after treatment at a temperature not exceeding a maximal temperature of 300° C.
Claim 3
Dependent Claim
24 words
A carbon black as defined in claim 1, wherein the mean primary particle diameter is 17 nm and the content of volatiles is 17%.
Claim 4
Dependent Claim
29 words
The carbon black of claim 1, wherein the after treatment is carried out by heating in the presence of nitrogen oxide at a temperature of up to 300° C.
Claim 5
Dependent Claim
21 words
The carbon black of claim 1, wherein the after treatment is carried out by heating in the presence of nitric acid.
References Cited (Backward Citations)
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Cited
US2707273A
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US3365637A
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US3398009A
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US3383232A
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US3595618A
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US3978019A
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USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1985-12-27 | 1986-06-28 | 1986-12-28 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1989-12-27 | 1990-06-28 | 1990-12-28 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1993-12-27 | 1994-06-28 | 1994-12-28 | $7700.00 | Window Closed / Lapsed |