Patent US4357188A successfully refreshed from Google Patents.
US4357188A
Expired / Lapsed
US
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Method for manufacturing cigarette filters
Assignee: Mitsubishi Chemical Corp
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Filing: 1980-10-17
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Granted: 1982-11-02
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Expires: 2000-10-17
Abstract
Abstract A method for manufacturing cigarette filters which have a well-stabilized shape in which acetate fibrous tows impregnated with carboxylic acid ester of polyol are formed into a predetermined shape, uniformly impregnated with water, and irradiated with microwave energy. Water is used during the application of microwave energy to enhance the absorption of microwave energy and hence heating of the filter. This causes the carboxylic acid ester of polyol to very rapidly disperse causing it to permeate into the acetate fiber to rapidly complete the stabilization and solidification of the filter.
Inventors
- 👤 Naoki Mochida
- 👤 Kazuhiko Morifuji
- 👤 Takashi Sakai
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-09 08:48
CPC Classifications
D; D04; D04H; D04H1/00; D04H1/40; D04H1/54; A; A24; A24D; A24D3/00; A24D3/02; A24D3/0204; A24D3/0212; A24D3/022; B; B01; B01D; B01D39/00; B01D39/14; B01D39/16; B01D39/18; B29; B29C; B29C35/00; B29C35/02; B29C35/08; B29C35/10; B29C70/00; B29C70/04; B29C70/28; B29C70/40; B29C70/50; B29C70/52; B29C70/521; B29C35/0805; B29C2035/0855; B29K; B29K2067/00; B29K2067/06; B29K2105/00; B29K2105/06; B29K2105/08; B29K2105/10; B29K2105/101; B29K2105/25; B29K2201/00; B29K2503/00; B29L; B29L2031/00; B29L2031/06
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
57 words
A method for producing fibrous rod articles having a desired configuration stabilization comprising the steps of: forming into fibrous rods cellulose esters fibers impregnated with at least one carboxylic acid ester of polyol; uniformly impregnating said cellulose ester fibers with water; and irradiating the fibrous rods with microwave energy to heat said water to a predetermined temperature.
Claim 2
Independent Claim
57 words
A method for producing fibrous rod articles having a desired configuration stabilization comprising the steps of: forming into fibrous rods cellulose esters fibers impregnated with at least one carboxylic acid ester of polyol; uniformly impregnating said cellulose ester fibers with water; and irradiating the fibrous rods with microwave energy to heat said water to a predetermined temperature.
Claim 3
Dependent Claim
29 words
The method as defined in claim 1 wherein the amount of the carboxylic acid ester of polyol contained in the cellulose ester fibers is 4 to 8% by weight.
Claim 4
Dependent Claim
27 words
The method as defined in claim 1 wherein the carboxylic acid ester of polyol is selected from the group consisting of triethylene glycol diacetate and glycerol triacetate.
Claim 5
Dependent Claim
25 words
The method as defined in claim 1 wherein the amount of water contained in the fibrous rods is 1 to 100% of the fiber weight.
Claim 6
Dependent Claim
25 words
The method as defined in claim 4 wherein the amount of water contained in the fibrous rods is 4 to 40% of the fiber weight.
Claim 7
Dependent Claim
30 words
The method as defined in claim 4 wherein the amount of water contained in the cellulose ester fibers before formation of said fibrous rods is 1 to 100% by weight.
Claim 8
Dependent Claim
27 words
The method as defined in claim 4 wherein said step of impregnating said fibrous rods with water comprises supplying water in vapor form to said fibrous rods.
Claim 9
Independent Claim
22 words
The method as defined in any of claims 1, 4, 5, 6 or 7 wherein said cellulose ester fiber comprises cellulose diacetate.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1985-11-01 | 1986-05-03 | 1986-11-02 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1989-11-01 | 1990-05-03 | 1990-11-02 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1993-11-01 | 1994-05-03 | 1994-11-02 | $7700.00 | Window Closed / Lapsed |