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US4353715A Expired / Lapsed US ⏱️ 0.0 years remaining

Apparatus for and process of removal of solvent vapors

Assignee: Kovalus Separation Solutions LLC
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Filing: 1980-12-16
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Granted: 1982-10-12
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Expires: 2000-12-16
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Abstract

Abstract A process for and a system of removing volatile vapor solvents, particularly from paint-spray booths and paint dryers, and recovering such solvents, which process comprises: intimately contacting the solvent-laden air with a multiphase scrubbing media, particularly a water stream containing an oil-in-water emulsion or a surfactant or a powdered activated carbon, to capture and to dissolve the solvent vapor in the dispersed phase of the scrubbing media in a gas scrubber; removing the solvent-enriched scrubbing media and concentrating the solvent-enriched scrubbing media employing an ultrafiltration device; stripping the solvent from the concentrated solvent-enriched scrubbing media from the ultrafiltration device to remove and recover the solvent, while recycling the scrubbing media for further contact with fresh solvent-laden air; and recycling the water carrier as a permeate for reuse in contacting the solvent-laden air.

Inventors

  • 👤 Leon Mir
  • 👤 Joseph Zahka

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-09 04:36
CPC Classifications
B; B01; B01D; B01D53/00; B01D53/14; B01D53/1493; B01D47/00; B01D47/06; B01D53/1425; B01D53/1487; B05; B05B; B05B14/00; B05B14/40; B05B14/49; Y; Y02; Y02A; Y02A50/00; Y02A50/20; Y02P; Y02P70/00; Y02P70/10

Claims Analysis

Total Claims: 11
Claim 1
Independent Claim 262 words
A process for the removal of a volatile organic solvent from a solvent-laden air stream, which process comprises: (a) intimately contacting and scrubbing the solvent-laden air stream with an aqueous, multiple-phase scrubbing media to provide a solvent-lean air stream and a solvent-rich scrubbing media, the scrubbing media comprising a surfactant-dispersed, activated carbon or molecular-sieve particles, which particles adsorb the solvent from the solvent-lean air stream, to form a solvent-rich scrubbing media; (b) discharging the solvent-lean air stream; (c) concentrating the solvent-rich scrubbing media in a low-pressure ultrafiltration-membrane unit having a feed zone and a permeate zone separated by a membrane which permits the passage of water, but retards the passage of the dispersed activated carbon or molecular-sieve particles of the scrubbing media, to provide a concentrated, solvent-rich scrubbing media in the feed zone and permeate water which passes through the membrane into the permeate zone; (d) heating the concentrated, solvent-rich scrubbing media to a temperature to remove the solvent from the activated carbon or molecular-sieve particles of the concentrated, solvent-rich scrubbing media, to form a solvent vapor and a concentrated, solvent-lean scrubbing media; (e) recovering the solvent vapor; and (f) continuously recycling the concentrated, solvent-lean scrubbing media and the permeate water from the permeate zone for use in the contacting and scrubbing of the solvent-lean air stream, to reconstitute a scrubbing media for use in the contacting and scrubbing steps, whereby the volatile organic solvent is condensed, a solvent-lean air stream is discharged and the multiple-phase scrubbing media is continuously recycled and reused in removing the solvent from the solvent-laden air stream.
Claim 2
Dependent Claim 262 words
A process for the removal of a volatile organic solvent from a solvent-laden air stream, which process comprises: (a) intimately contacting and scrubbing the solvent-laden air stream with an aqueous, multiple-phase scrubbing media to provide a solvent-lean air stream and a solvent-rich scrubbing media, the scrubbing media comprising a surfactant-dispersed, activated carbon or molecular-sieve particles, which particles adsorb the solvent from the solvent-lean air stream, to form a solvent-rich scrubbing media; (b) discharging the solvent-lean air stream; (c) concentrating the solvent-rich scrubbing media in a low-pressure ultrafiltration-membrane unit having a feed zone and a permeate zone separated by a membrane which permits the passage of water, but retards the passage of the dispersed activated carbon or molecular-sieve particles of the scrubbing media, to provide a concentrated, solvent-rich scrubbing media in the feed zone and permeate water which passes through the membrane into the permeate zone; (d) heating the concentrated, solvent-rich scrubbing media to a temperature to remove the solvent from the activated carbon or molecular-sieve particles of the concentrated, solvent-rich scrubbing media, to form a solvent vapor and a concentrated, solvent-lean scrubbing media; (e) recovering the solvent vapor; and (f) continuously recycling the concentrated, solvent-lean scrubbing media and the permeate water from the permeate zone for use in the contacting and scrubbing of the solvent-lean air stream, to reconstitute a scrubbing media for use in the contacting and scrubbing steps, whereby the volatile organic solvent is condensed, a solvent-lean air stream is discharged and the multiple-phase scrubbing media is continuously recycled and reused in removing the solvent from the solvent-laden air stream.
Claim 3
Dependent Claim 21 words
The process of claim 1 wherein the volatile solvent comprises acetone, methylethyl ketone, toluene, xylene, benzene, ethyl acetate and mixtures thereof.
Claim 4
Dependent Claim 18 words
The process of claim 1 wherein the solvent-laden air stream is derived from a paint-spray booth or oven.
Claim 5
Dependent Claim 36 words
The process of claim 1 which includes introducing water or make-up scrubbing media to the scrubbing media to make up for loss of water or scrubbing media, prior to contacting and scrubbing the solvent-laden air stream.
Claim 6
Dependent Claim 31 words
The process of claim 1 which includes reconstituting the scrubbing media by admixing the recycled permeate water and the recycled, concentrated, solvent-lean scrubbing media, prior to the contacting and scrubbing steps.
Claim 7
Dependent Claim 31 words
The process of claim 1 wherein the multiple-phase scrubbing media used in the contacting and scrubbing steps comprises from about 0.5% to 5% by weight of activated carbon or molecular-sieve particles.
Claim 8
Dependent Claim 27 words
The process of claim 1 wherein the concentrated, solvent-rich scrubbing media comprises from about 15% to 40% by weight of the solvent-adsorbed activated carbon or molecular-sieve particles.
Claim 9
Dependent Claim 13 words
The process of claim 1 wherein recovering the solvent comprises condensing the solvent.
Claim 10
Dependent Claim 21 words
The process of claim 1 wherein the surfactant in the dispersed scrubbing media comprises from about 0.5% to 20% by weight.
Claim 11
Dependent Claim 26 words
The process of claim 1 wherein the concentrated, solvent-rich scrubbing media in the feed zone contains from 15% to 40% by weight of activated carbon particles.

References Cited (Backward Citations)

US2823763A Cited
US3068627A Cited
US4257783A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1985-10-11 1986-04-12 1986-10-12 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1989-10-11 1990-04-12 1990-10-12 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1993-10-11 1994-04-12 1994-10-12 $7700.00 Window Closed / Lapsed

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