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US4347144A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for the purification of effluent

Assignee: Hoechst AG
•
Filing: 1981-11-06
•
Granted: 1982-08-31
•
Expires: 2001-11-06
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Abstract

Abstract Effluent containing organic impurities which are difficult to degrade is purified by oxidation in the aqueous phase at temperatures of 100° to 310° C. and under elevated pressure. This is effected by initially treating the effluent in a first stage with gases containing oxygen, but without the addition of catalysts, until the C.O.D. value has been reduced by 50 to 98%. The effluent which has received preliminary treatment in this way is subsequently treated, in a second stage, with an oxidizing agent stronger than oxygen, in the liquid phase and at the same, or at a higher, temperature, until the C.O.D. value has fallen to approximately 0 g/l.

Inventors

  • 👤 Kurt Bodenbenner
  • 👤 Helmut Perkow
  • 👤 Helmut Vollmuller

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 06:24
CPC Classifications
C; C02; C02F; C02F1/00; C02F1/72; C02F11/00; C02F11/06; C02F11/08

Claims Analysis

Total Claims: 6
Claim 1
Independent Claim 111 words
A process for the purification of effluent containing organic impurities which are difficult to degrade, by oxidation in an aqueous phase at temperatures of 100° to 310° C. and under elevated pressure, the effluent being initially treated in a first stage with gases containing oxygen, but without addition of catalysts, until the C.O.D. value has been reduced by 50 to 98%, which comprises subjecting the effluent which has received preliminary treatment in this way, subsequently, in a second stage, to treatment with an oxidizing agent stronger than oxygen, in the liquid phase and at the same, or at a higher, temperature, until the C.O.D. value has fallen to approximately 0 g/l.
Claim 2
Dependent Claim 111 words
A process for the purification of effluent containing organic impurities which are difficult to degrade, by oxidation in an aqueous phase at temperatures of 100° to 310° C. and under elevated pressure, the effluent being initially treated in a first stage with gases containing oxygen, but without addition of catalysts, until the C.O.D. value has been reduced by 50 to 98%, which comprises subjecting the effluent which has received preliminary treatment in this way, subsequently, in a second stage, to treatment with an oxidizing agent stronger than oxygen, in the liquid phase and at the same, or at a higher, temperature, until the C.O.D. value has fallen to approximately 0 g/l.
Claim 3
Dependent Claim 23 words
A process as claimed in claim 1, wherein nitric acid or a nitrate are used as the oxidizing agent in the second stage.
Claim 4
Dependent Claim 36 words
A process as claimed in claim 2, wherein 0.02 to 0.05 mole of nitric acid or nitrates per g of C.O.D. in the effluent leaving the first stage, are employed for oxidation in the second stage.
Claim 5
Dependent Claim 28 words
A process as claimed in claim 1, wherein the effluent containing the organic impurities which are difficult to degrade, originates from the manufacture of secondary products of cellulose.
Claim 6
Dependent Claim 20 words
A process as claimed in claim 1, wherein the effluent employed also contains chlorides in addition to the organic impurities.

References Cited (Backward Citations)

US2903425A Cited
US4012321A Cited
US4000068A Cited
US4246104A Cited
GB2034684A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1985-08-30 1986-03-01 1986-08-31 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1989-08-30 1990-03-01 1990-08-31 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1993-08-30 1994-03-01 1994-08-31 $7700.00 Window Closed / Lapsed

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