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US4246104A Expired / Lapsed US ⏱️ 0.0 years remaining

Pressure-hydrolytic treatment of effluent

Assignee: Bayer AG
•
Filing: 1979-04-30
•
Granted: 1981-01-20
•
Expires: 1999-04-30
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Abstract

Abstract A process for the chemical treatment of an effluent containing at least one organic compound selected from the group consisting of an organometallic compound and an organic compound containing at least one of phosphorus, nitrogen and halogen, comprising treating the effluent hydrolytically for about 20 to 200 minutes at a temperature above about 100° C. under a pressure above about 2 bars and a pH of about 1 to 14. Advantageously, a catalyst comprising activated carbon or kieselguhr is added to the effluent before the hydrolytic treatment and the hydrolytic treatment is carried out in the presence of ammonia or a primary or secondary amine. The organic compound may be an acid ester, a dye, or quaternary ammonium compound, a cyanide, a nitrile, a cyanate, an isocyanate, hydrazine, an organic derivative of hydrazine, an azo compound or an organometallic compound and the effluent may be aftertreated as with hypochlorite or H 2 O 2 .

Inventors

  • 👤 Friedrich Schmidt
  • 👤 Kurt Mack
  • 👤 Hans-Rolf Furtwangler

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 16:05
CPC Classifications
C; C02; C02F; C02F1/00; C02F1/72; C02F1/725; C02F1/02; C02F1/025; Y; Y10; Y10S; Y10S210/00; Y10S210/902; Y10S210/906

Claims Analysis

Total Claims: 9
Claim 1
Independent Claim 61 words
A process for the chemical treatment of an effluent containing organic phosphoric ester acids, comprising treating the effluent hydrolytically for about 20 to 200 minutes at a temperature above about 100° C. under a pressure above about 2 bars and at a pH of about 1 to 14, and thereafter treating the effluent with hydrochlorite or H 2 O 2 .
Claim 2
Dependent Claim 61 words
A process for the chemical treatment of an effluent containing organic phosphoric ester acids, comprising treating the effluent hydrolytically for about 20 to 200 minutes at a temperature above about 100° C. under a pressure above about 2 bars and at a pH of about 1 to 14, and thereafter treating the effluent with hydrochlorite or H 2 O 2 .
Claim 3
Dependent Claim 31 words
A process as claimed in claim 1, wherein effluent contains an organohalogen compound and the hydrolytic treatment is carried out in the presence of ammonia or a primary or secondary amine.
Claim 4
Dependent Claim 34 words
A process as claimed in claim 2, wherein about 1 to 20 kg of nitrogen, in the form of ammonia, amine or precursor thereof, are present per cubic meter of effluent to be treated.
Claim 5
Dependent Claim 24 words
A process as claimed in claim 1, wherein a catalyst comprising activated carbon or kieselguhr is added to the effluent before the hydrolytic treatment.
Claim 6
Dependent Claim 25 words
A process as claimed in claim 4, wherein about 100 to 10000 g of catalyst is added per cubic meter of effluent to be treated.
Claim 7
Dependent Claim 88 words
A process as claimed in claim 5, wherein about 2 to 10 kg of nitrogen, in the form of ammonia, amine or precursor thereof, are present per cubic meter of effluent to be treated, and the effluent is treated for about 100 to 150 minutes at about 170° to 210° C. under a pressure of about 20 to 30 bars and a pH of about 9 to 14, and the effluent is aftertreated with about 10 to 1000 g/l of hypochlorite or H 2 O 2 . PG,16
Claim 8
Dependent Claim 25 words
A process as claimed in claim 1, wherein the effluent is treated hydrolytically at about 170° to 210° C. in an autoclave under spontaneous pressure.
Claim 9
Dependent Claim 19 words
A process as claimed in claim 1, wherein the effluent is neutralized by the addition of acids or alkalis.

References Cited (Backward Citations)

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US3607738A Cited
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US3586625A Cited
US3817862A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-01-20 1984-07-21 1985-01-20 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-01-20 1988-07-21 1989-01-20 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-01-20 1992-07-21 1993-01-20 $7700.00 Window Closed / Lapsed

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