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US4347101A Expired / Lapsed US ⏱️ 0.0 years remaining

Process for producing newsprint

Assignee: WR Grace and Co
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Filing: 1980-11-24
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Granted: 1982-08-31
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Expires: 2000-11-24
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Abstract

Abstract A high quality newsprint pulp can be produced from wood or vegetable fibers by thermomechanically pulping one portion of these fibers and thermochemically pulping the remaining portion. After combining these pulps the result is a pulp which has a GE brightness of 55 to 60, an opacity of 93 to 96 percent, and a relatively high tear strength. A pulp useful for making low strength papers can be produced by solely thermomechanically pulping fiber and directly using this pulp to make such products.

Inventors

  • 👤 Eduardo J. Villavicencio

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-02 20:41
CPC Classifications
D; D21; D21B; D21B1/00; D21B1/04; D21B1/12; D21C; D21C3/00; D21C3/22; D21H; D21H11/00; D21H11/10

Claims Analysis

Total Claims: 13
Claim 1
Independent Claim 363 words
A method for producing a high quality newsprint pulp from wood or vegetable fibrous material comprising: (a) providing a quantity of said fibrous material in a form suitable for input into a digester; (b) (i) conveying at least forty percent by weight of said quantity of fibrous material to a thermochemical digester and contacting said fibrous material with an alkaline cooking liquor whereby lignin is removed from said fibrous material and said fibrous components; (ii) after digesting said fiber for from 0.1 to 1 hour at 140° C. to 190° C., refining the digested fiber at above 100° C.; (iii) rapidly reducing the pressure on said digested and refined fibers to approximately ambient pressure and washing and screening said fiber to remove pulping chemicals and dirt and other foreign fragments therefrom; and (iv) contacting said washed and screened fibers with a bleachant for a time sufficient to raise the GE brightness of said fibers to greater than about 60; (c) (i) conveying the remainder of said quantity of fibrous material to a thermomechanical digester which consists of a first section and a second section, said sections being separated by a refiner; (ii) contacting said fibrous material within the first section, of said thermomechanical digester with steam at a pressure greater than about 2 kg/sq. cm and mechanically working said fiber in said section of the digester to partially reduce said fibrous material to its fiber components; (iii) conveying the fibrous material from the first section of said digester to a refiner and refining said fibrous material; (iv) contacting the refined fiber in a second section of said thermomechanical digester with steam at a pressure of less than about 2 kg/cm 2 , whereby said fibrous material is substantially reduced to its fiber components; (v) refining the digested fiber and rapidly reducing the pressure on the digested fiber to approximately ambient pressure; and (vi) refining said digested and elevated pressure refined fibers at ambient pressure; and washing and screening the refined fibers to remove dirt and large fiber fragments therefrom; (d) intermixing the bleached fiber from thermochemical digestion with the fiber from thermomechanical digestion; and; (e) producing a newsprint paper from such intermixed fibers.
Claim 2
Independent Claim 363 words
A method for producing a high quality newsprint pulp from wood or vegetable fibrous material comprising: (a) providing a quantity of said fibrous material in a form suitable for input into a digester; (b) (i) conveying at least forty percent by weight of said quantity of fibrous material to a thermochemical digester and contacting said fibrous material with an alkaline cooking liquor whereby lignin is removed from said fibrous material and said fibrous components; (ii) after digesting said fiber for from 0.1 to 1 hour at 140° C. to 190° C., refining the digested fiber at above 100° C.; (iii) rapidly reducing the pressure on said digested and refined fibers to approximately ambient pressure and washing and screening said fiber to remove pulping chemicals and dirt and other foreign fragments therefrom; and (iv) contacting said washed and screened fibers with a bleachant for a time sufficient to raise the GE brightness of said fibers to greater than about 60; (c) (i) conveying the remainder of said quantity of fibrous material to a thermomechanical digester which consists of a first section and a second section, said sections being separated by a refiner; (ii) contacting said fibrous material within the first section, of said thermomechanical digester with steam at a pressure greater than about 2 kg/sq. cm and mechanically working said fiber in said section of the digester to partially reduce said fibrous material to its fiber components; (iii) conveying the fibrous material from the first section of said digester to a refiner and refining said fibrous material; (iv) contacting the refined fiber in a second section of said thermomechanical digester with steam at a pressure of less than about 2 kg/cm 2 , whereby said fibrous material is substantially reduced to its fiber components; (v) refining the digested fiber and rapidly reducing the pressure on the digested fiber to approximately ambient pressure; and (vi) refining said digested and elevated pressure refined fibers at ambient pressure; and washing and screening the refined fibers to remove dirt and large fiber fragments therefrom; (d) intermixing the bleached fiber from thermochemical digestion with the fiber from thermomechanical digestion; and; (e) producing a newsprint paper from such intermixed fibers.
Claim 3
Dependent Claim 106 words
A method for producing a high quality newsprint pulp as in claim 1, wherein the thermomechanical digester consists of two interconnected tubular chambers with screw means within each tubular chamber to convey fibers from the input end to the exit end of each tubular chamber, the interconnection including a pulp refiner; the temperature in the first tubular chamber and in the second tubular chamber being about 120° C. to 140° C.; the pressure in said first chamber being reduced in said refiner to the pressure level of said second tubular chamber, the energy from the reduction in pressure in the refiner aiding to open fiber bundles.
Claim 4
Dependent Claim 37 words
A method for producing a high quality newsprint pulp as in claim 1, wherein the thermochemical digester consists of two interconnected tubular chambers with the pressure in each chamber being maintained in excess of 2 kg/sq cm.
Claim 5
Dependent Claim 54 words
A method for producing a high quality newsprint pulp as in claim 1, wherein said alkaline cooking liquor is selected from a sodium hydroxide liquor, a sodium hydroxide-sodium sulfite liquor, a sodium hydroxide-sodium bisulfite liquor, and a kraft liquor consisting of sodium hydroxide and sodium sulfide having a sulfidity of at least 30 percent.
Claim 6
Dependent Claim 32 words
A method for producing a high quality newsprint pulp as in claim 4, wherein said alkaline cooking liquor consists of an aqueous solution of sodium hydroxide having a Ph of about 14.
Claim 7
Dependent Claim 36 words
A method for producing a high quality newsprint pulp as in claim 4, wherein said alkaline cooking liquor consists of an aqueous solution of sodium hydroxide and sodium sulfite in a molar ratio of about 1:3.
Claim 8
Dependent Claim 27 words
A method of producing a high quality newsprint pulp as in claim 1, wherein said bleachant is selected from the group consisting of oxidizing and reducing bleachants.
Claim 9
Dependent Claim 19 words
A method for producing a high quality newsprint pulp as in claim 7, wherein said bleachant is hydrogen peroxide.
Claim 10
Dependent Claim 19 words
A method for producing a high quality newsprint pulp as in claim 7, wherein said bleachant is sodium peroxide.
Claim 11
Dependent Claim 20 words
A method for producing a high quality newsprint pulp as in claim 7, wherein said bleachant is an alkaline hypochlorite.
Claim 12
Dependent Claim 19 words
A method for producing a high quality newsprint pulp as in claim 7, wherein said fibrous material is bagasse.
Claim 13
Dependent Claim 20 words
A method for producing a high quality newsprint pulp as in claim 7, wherein said fibrous material is wood chips.

References Cited (Backward Citations)

US2862813A Cited
US2913362A Cited
US3238088A Cited
US3773610A Cited
US4152197A Cited
US4235665A Cited
US4260452A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1985-08-30 1986-03-01 1986-08-31 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1989-08-30 1990-03-01 1990-08-31 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1993-08-30 1994-03-01 1994-08-31 $7700.00 Window Closed / Lapsed

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