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Patent US4340512A successfully refreshed from Google Patents.
US4340512A
Expired / Lapsed
US
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Method of providing a universal coating for fluorescent lamps
Assignee: Philips North America LLC
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Filing: 1979-10-01
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Granted: 1982-07-20
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Expires: 1999-10-01
Abstract
Abstract A method of preparing phosphor suspensions for coating fluorescent lamps wherein the temporary organic binder is an association compound of purified carboxy methyl cellulose and polyethylene oxide in such proportions as to avoid the gelation caused by ionizable phosphors releasing multivalent cations.
Inventors
- 👤 Willy P. Schreurs
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-03 16:29
CPC Classifications
H; H01; H01J; H01J61/00; H01J61/02; H01J61/38; H01J61/42; H01J61/46; C; C08; C08K; C08K3/00; C08K3/02; C08L; C08L1/00; C08L1/08; C08L1/26; C08L1/28; C08L1/286; C08L71/00; C08L71/02; C09; C09D; C09D101/00; C09D101/08; C09D101/26; C09D101/28; C09D101/286; C09K; C09K11/00; C09K11/02
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
220 words
A method for preparing a universal water-base suspension for coating the interior surface of fluorescent lamps, said method comprising: (a) preparing a temporary binder solution of polyoxyethylene in water at concentrations ranging from 1.5 to 2.5 weight by volume percent and removing the contaminating particulates of silica and Ca CO 3 by centrifuging; (b) preparing a temporary binder solution of sodium carboxymethyl cellulose in water at concentrations ranging from 1.2 to 2.5 weight by volume percent; (c) mixing said temporary binder solutions and removing the contaminating cations by an ion exchange process; (d) neutralizing said purified temporary binder solution with ammonia to a pH 7.0 to 7.5 and adding between 0.01 and 0.02 weight by volume percent of bactericide; (e) preparing an inorganic binder suspension of submicron size Al 2 O 3 in water solution of low molecular weight polyacrylic acid neutralized to a pH 9.0 to 9.5 with monethanolamine, said suspension containing 0.5 to 1.5 weight by volume percent polyacrylic acid and 5 to 15 weight by volume percent of Al 2 O 3 ; and (f) mixing said temporary binder solution and inorganic binder suspension with phosphors and defoamer in such proportions as to contain a ratio of 0.5 to 1.5 weight percent of dry binder to phosphor and 0.02 to 0.1 weight percent of defoamer to phosphor.
Claim 2
Independent Claim
220 words
A method for preparing a universal water-base suspension for coating the interior surface of fluorescent lamps, said method comprising: (a) preparing a temporary binder solution of polyoxyethylene in water at concentrations ranging from 1.5 to 2.5 weight by volume percent and removing the contaminating particulates of silica and Ca CO 3 by centrifuging; (b) preparing a temporary binder solution of sodium carboxymethyl cellulose in water at concentrations ranging from 1.2 to 2.5 weight by volume percent; (c) mixing said temporary binder solutions and removing the contaminating cations by an ion exchange process; (d) neutralizing said purified temporary binder solution with ammonia to a pH 7.0 to 7.5 and adding between 0.01 and 0.02 weight by volume percent of bactericide; (e) preparing an inorganic binder suspension of submicron size Al 2 O 3 in water solution of low molecular weight polyacrylic acid neutralized to a pH 9.0 to 9.5 with monethanolamine, said suspension containing 0.5 to 1.5 weight by volume percent polyacrylic acid and 5 to 15 weight by volume percent of Al 2 O 3 ; and (f) mixing said temporary binder solution and inorganic binder suspension with phosphors and defoamer in such proportions as to contain a ratio of 0.5 to 1.5 weight percent of dry binder to phosphor and 0.02 to 0.1 weight percent of defoamer to phosphor.
Claim 3
Independent Claim
222 words
A method for preparing a universal water-base suspension for coating the interior surface of fluorescent lamps, said method comprising: (a) preparing a temporary binder solution of polyoxyethylene in water at concentrations ranging from 1.2 to 2.5 and preferably 2 weight by volume percent and removing the contaminating particulates of silica and Ca CO 3 by centrifuging; (b) preparing a temporary binder solution of sodium carboxymethyl cellulose in water at concentrations ranging from 1.2 to 2.5 and preferably 1.5 weight by volume percent; (c) mixing said temporary binder solutions and removing the contaminating cations by an ion exchange process; (d) neutralizing said purified temporary binder solution with ammonia to a pH 7.0 to 7.5 and adding between 0.01 and 0.02 weight by volume percent of bactericide; (e) preparing an inorganic binder suspension of submicron size Al 2 O 3 in water solution of low molecular weight polyacrylic acid neutralized to a pH 9.0 to 9.5 with monethanolamine, said suspension containing 0.5 to 1.5 and preferably 1.0 weight percent polyacrylic acid and 5 to 15 and preferably 10 weight by volume percent of Al 2 O 3 ; and (f) mixing said temporary binder solution and inorganic binder suspension with phosphors and defoamer in such proportions as to contain a ratio of 0.5 to 1.5 of dry binder and 0.02 to 0.08 of defoamer.
Claim 4
Independent Claim
222 words
A method for preparing a universal water-base suspension for coating the interior surface of fluorescent lamps, said method comprising: (a) preparing a temporary binder solution of polyoxyethylene in water at concentrations ranging from 1.2 to 2.5 and preferably 2 weight by volume percent and removing the contaminating particulates of silica and Ca CO 3 by centrifuging; (b) preparing a temporary binder solution of sodium carboxymethyl cellulose in water at concentrations ranging from 1.2 to 2.5 and preferably 1.5 weight by volume percent; (c) mixing said temporary binder solutions and removing the contaminating cations by an ion exchange process; (d) neutralizing said purified temporary binder solution with ammonia to a pH 7.0 to 7.5 and adding between 0.01 and 0.02 weight by volume percent of bactericide; (e) preparing an inorganic binder suspension of submicron size Al 2 O 3 in water solution of low molecular weight polyacrylic acid neutralized to a pH 9.0 to 9.5 with monethanolamine, said suspension containing 0.5 to 1.5 and preferably 1.0 weight percent polyacrylic acid and 5 to 15 and preferably 10 weight by volume percent of Al 2 O 3 ; and (f) mixing said temporary binder solution and inorganic binder suspension with phosphors and defoamer in such proportions as to contain a ratio of 0.5 to 1.5 of dry binder and 0.02 to 0.08 of defoamer.
Claim 5
Dependent Claim
39 words
A water-base phosphor suspension for coating the interior surface of fluorescent lamps prepared by the method specified in claim 1 or 2 and containing carboxymethyl cellulose and polyoxyethylene in ratios ranging between 80 to 20 and 50 to 50.
Claim 6
Dependent Claim
20 words
A water-base phosphor suspension according to claim 3 wherein the ratio of carboxymethyl cellulose to polyoxyethylene is 60 to 40.
Claim 7
Dependent Claim
48 words
The method as described in claim 2 wherein: said step of mixing said temporary binder solution in inorganic binder suspension with phosphors and defoamers is in such proportions as to contain a ratio of substantially 0.6 weight percent of dry binder and substantially 0.05 weight percent of defoamer.
Claim 8
Dependent Claim
48 words
The suspension as described in claim 3 wherein: said step of mixing said temporary binder solution in inorganic binder suspension with phosphors and defoamers is in such proportions as to contain a ratio of substantially 0.6 weight percent of dry binder and substantially 0.05 weight percent of defoamer.
Claim 9
Dependent Claim
48 words
The suspension as described in claim 4 wherein: said step of mixing said temporary binder solution in inorganic binder suspension with phosphors and defoamers is in such proportions as to contain a ratio of substantially 0.6 weight percent of dry binder and substantially 0.05 weight percent of defoamer.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1985-07-19 | 1986-01-18 | 1986-07-20 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1989-07-19 | 1990-01-18 | 1990-07-20 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1993-07-19 | 1994-01-18 | 1994-07-20 | $7700.00 | Window Closed / Lapsed |