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US4325842A
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Process for preparing a supported molybdenum carbide composition
Assignee: Shell USA Inc
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Filing: 1980-12-08
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Granted: 1982-04-20
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Expires: 2000-12-08
Abstract
Abstract A process for preparing a supported molybdenum carbide composition which comprises impregnating a porous support with a solution of hexamolybdenum dodecachloride, drying the impregnated support and then heating in a carbiding atmosphere at a temperature of about 650°-750° C.
Inventors
- 👤 Lynn H. Slaugh
- 👤 Ronald J. Hoxmeier
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-05 05:14
CPC Classifications
B; B01; B01J; B01J27/00; B01J27/20; B01J27/22; C; C07; C07C; C07C4/00; C07C4/08; C07C4/12; C07C4/14; C07C4/18; C07C2527/00; C07C2527/20; C07C2527/22; Y; Y02; Y02P; Y02P20/00; Y02P20/50; Y02P20/52; Y10; Y10S; Y10S502/00; Y10S502/506
Claims Analysis
Total Claims: 8
Claim 1
Independent Claim
126 words
A process for preparing a supported molybdenum carbide composition which comprises impregnating a porous, inert support with a solution of (H 3 O) 2 Mo 6 Cl 14 .2H 2 O dissolved in an organic solvent, heating the impregnated support under non-oxidizing conditions in order to remove the solvent and subsequently heating the impregnated support to a temperature ranging from about 650° C. to about 750° C. in a carbidng gas mixture which comprises hydrogen in a concentration ranging from about 1 to about 20 percent by volume, a carbiding component selected from the group consisting of lower alkane, lower alkene, carbon monoxide and mixtures thereof in a concentration ranging from about 0.5 to about 5 percent by volume and the balance being a noble gas.
Claim 2
Dependent Claim
126 words
A process for preparing a supported molybdenum carbide composition which comprises impregnating a porous, inert support with a solution of (H 3 O) 2 Mo 6 Cl 14 .2H 2 O dissolved in an organic solvent, heating the impregnated support under non-oxidizing conditions in order to remove the solvent and subsequently heating the impregnated support to a temperature ranging from about 650° C. to about 750° C. in a carbidng gas mixture which comprises hydrogen in a concentration ranging from about 1 to about 20 percent by volume, a carbiding component selected from the group consisting of lower alkane, lower alkene, carbon monoxide and mixtures thereof in a concentration ranging from about 0.5 to about 5 percent by volume and the balance being a noble gas.
Claim 3
Dependent Claim
13 words
The process of claim 1 wherein the solvent is a polar organic solvent.
Claim 4
Dependent Claim
12 words
The process of claim 2 wherein the solvent is an oxygenated solvent.
Claim 5
Dependent Claim
19 words
The process of claim 3 wherein the solvent is selected from the group consisting of alcohols, ethers and ketones.
Claim 6
Dependent Claim
23 words
The process of claim 4 wherein the solvent is a lower alcohol having a carbon number ranging from about 1 to about 6.
Claim 7
Dependent Claim
23 words
The process of claim 1 wherein the alkane and/or alkene is selected from the group consisting of methane, ethane, propane, ethylene, and propylene.
Claim 8
Dependent Claim
10 words
The process of claim 6 wherein the alkane is methane.
References Cited (Backward Citations)
US4073866A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1985-04-19 | 1985-10-19 | 1986-04-20 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1989-04-19 | 1989-10-19 | 1990-04-20 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1993-04-19 | 1993-10-19 | 1994-04-20 | $7700.00 | Window Closed / Lapsed |