Claims Analysis
Total Claims: 31
Claim 1
Independent Claim
178 words
In a process for the encapsulation of a liquid hydrophobic substance by interfacial polycondensation comprising in a first stage, dispersing, in an aqueous phase, an organic phase consisting essentially of the liquid hydrophobic substance to be encapsulated and at least one hydrophobic reagent having two or three functional groups selected from the groups consisting of carboxylic acid chloride, sulfonyl acid chloride, isocyanate and mixtures thereof; and then, in a second stage, causing the polycondensation of the hydrophobic reagent with at least one di- or tri-functional amine as a hydrophilic reagent, said liquid hydrophobic substance being inert to said hydrophobic reagent and the polycondensation product thereof: the improvement wherein, prior to said hydrophobic reagent being brought into contact with said di- or tri-functional amine, said di- or tri-functional amine in the aqueous phase has its amine functions rendered unreactive by salification with hydrohalic acid and, in the second stage, the polycondensation is started by liberating the amine functions through the addition, to the aqueous phase, of an equivalent amount of an inorganic base which is stronger than the amine.
Claim 2
Dependent Claim
178 words
In a process for the encapsulation of a liquid hydrophobic substance by interfacial polycondensation comprising in a first stage, dispersing, in an aqueous phase, an organic phase consisting essentially of the liquid hydrophobic substance to be encapsulated and at least one hydrophobic reagent having two or three functional groups selected from the groups consisting of carboxylic acid chloride, sulfonyl acid chloride, isocyanate and mixtures thereof; and then, in a second stage, causing the polycondensation of the hydrophobic reagent with at least one di- or tri-functional amine as a hydrophilic reagent, said liquid hydrophobic substance being inert to said hydrophobic reagent and the polycondensation product thereof: the improvement wherein, prior to said hydrophobic reagent being brought into contact with said di- or tri-functional amine, said di- or tri-functional amine in the aqueous phase has its amine functions rendered unreactive by salification with hydrohalic acid and, in the second stage, the polycondensation is started by liberating the amine functions through the addition, to the aqueous phase, of an equivalent amount of an inorganic base which is stronger than the amine.
Claim 3
Dependent Claim
15 words
Process according to claim 1, wherein said liquid hydrophobic substance is a pure organic compound.
Claim 4
Dependent Claim
17 words
Process according to claim 1, wherein said liquid hydrophobic substance is a solution in an organic solvent.
Claim 5
Dependent Claim
19 words
Process according to claim 1, wherein said liquid hydrophobic substance is a dispersion or suspension in an organic solvent.
Claim 6
Dependent Claim
17 words
Process according to claim 1, wherein said hydrophobic reagent is a di- or tri- functional acid chloride.
Claim 7
Dependent Claim
15 words
Process according to claim 5, wherein said hydrophobic reagent is a chloride of a diacid.
Claim 8
Dependent Claim
23 words
Process according to claim 6, wherein said hydrophobic reagent is a chloride of an aliphatic diacid containing from 2 to 36 carbon atoms.
Claim 9
Dependent Claim
16 words
Process according to claim 7, wherein said hydrophobic reagent is a chloride of a linear diacid.
Claim 10
Dependent Claim
12 words
Process according to claim 8, wherein said hydrophobic reagent is sebacoyl chloride.
Claim 11
Dependent Claim
16 words
Process according to claim 6, wherein said hydrophobic reagent is a chloride of an aromatic diacid.
Claim 12
Dependent Claim
16 words
Process according to claim 1 wherein said hydrophobic reagent is a di- or tri- functional isocyanate.
Claim 13
Dependent Claim
12 words
Process according to claim 11, wherein said hydrophobic reagent is a diisocyanate.
Claim 14
Dependent Claim
12 words
Process according to claim 11, wherein said hydrophobic reagent is a triisocyanate.
Claim 15
Dependent Claim
15 words
Process according to claim 11, wherein two separate polyisocyanates are used as the hydrophobic reagents.
Claim 16
Dependent Claim
30 words
Process according to claim 1, wherein at least one di- or tri-functional acid chloride and at least one di- or tri- functional isocyanate are used simultaneously as the hydrophobic reagents.
Claim 17
Dependent Claim
12 words
Process according to claim 1, wherein said hydrophilic reagent is a diamine.
Claim 18
Dependent Claim
12 words
Process according to claim 1, wherein said hydrophilic reagent is a triamine.
Claim 19
Dependent Claim
16 words
Process according to claim 1, wherein two separate polyfunctional amines are used as the hydrophilic reagents.
Claim 20
Dependent Claim
13 words
Process according to claim 1, wherein said hydrophilic reagent is an aliphatic amine.
Claim 21
Dependent Claim
18 words
Process according to claim 19, wherein said amine functions have been rendered unreactive by salification with hydrochloric acid.
Claim 22
Dependent Claim
17 words
Process according to claim 1, wherein said liquid hydrophobic substance contains an active ingredient for plant health.
Claim 23
Dependent Claim
15 words
Process according to claim 21, wherein that active ingredient for plant health is an insecticide.
Claim 24
Dependent Claim
11 words
Process according to claim 22, wherein that the insecticide is parathion-methyl.
Claim 25
Dependent Claim
10 words
Process according to claim 22, wherein that insecticide is Chlormephos.
Claim 26
Dependent Claim
15 words
Process according to claim 21, wherein that active ingredient for plant health is a herbicide.
Claim 27
Dependent Claim
10 words
Process according to claim 25, wherein said herbicide is Isoproturon.
Claim 28
Dependent Claim
15 words
Process according to claim 1 wherein said hydrophobic reagent comprises 5-50% of said organic phase.
Claim 29
Dependent Claim
31 words
Process according to claim 27 wherein said dispersing of said organic phase in said aqueous phase is effected by stirring sufficiently vigorous to form droplets of 1 micron to 100 microns.
Claim 30
Dependent Claim
20 words
Process according to claim 28 wherein said polycondensation is effected over about 1-5 hours at 0° C. to ambient temperature.
Claim 31
Dependent Claim
28 words
Process according to claim 1 wherein said di- or tri-functional amine is already mixed into said aqueous phase and its amine functions rendered unreactive prior to said dispersing.