Patent US4308074A successfully refreshed from Google Patents.
US4308074A
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Precipitated silicic acid, method and compositions containing same
Assignee: Evonik Operations GmbH
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Filing: 1981-01-23
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Granted: 1981-12-29
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Expires: 2001-01-23
Abstract
Abstract Finely divided precipitated silicic acid is obtained by the method of the invention. Compositions containing the finely divided precipitated silicic acid as a filler distributed in an elastomer such as an organopolysiloxane are disclosed.
Inventors
- 👤 Peter Nauroth
- 👤 Heinz Esch
- 👤 Robert Kuhlmann
- 👤 Rudolf Bode
- 👤 Arthur Reisert
- 👤 Harald Buhler
- 👤 Gunter Turk
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 13:12
CPC Classifications
C; C01; C01B; C01B33/00; C01B33/113; C01B33/12; C01B33/18; C01B33/187; C01B33/193; B; B82; B82Y; B82Y30/00; C08; C08K; C08K3/00; C08K3/34; C08K3/36; C09; C09C; C09C1/00; C09C1/28; C09C1/30; C09C1/3081; C01P; C01P2004/00; C01P2004/60; C01P2004/64; C01P2006/00; C01P2006/10; C01P2006/11; C01P2006/12; C01P2006/19; C01P2006/40; C01P2006/80; C01P2006/82; C01P2006/90
Claims Analysis
Total Claims: 3
Claim 1
Independent Claim
197 words
A process for the production of hydrophobic silicic acid comprising treating precipitated silicic acid having the following properties: ______________________________________
BET surface acc. to DIN 66 131
m.sup.2 /g
150 ± 30
Average size of the primary
particles from EM pictures
nm 15-22
Loss after drying acc. to DIN
55 921 after 2 hours at 105° C.
% 2.5-3.5
Loss at red heat (related to the
substance dried for 2 hours at
105° C.) acc. to DIN 55 921
% 3 ± 0.5
pH value (in 5% aqueous dis-
persion) acc. to DIN 53 200 3.5-5.5
Conductivity (in 4% aqueous
dispersion) us <500
Tamped density of the
unaerated substance acc. to
g/l 60 ± 20
DIN 53 194
SO.sub.3 content (related to the
substance dried for 2 hours at
105° C.) % <0.3
Na.sub.2 O content (related to the
substance dried for 2 hours at
105° C.) % <0.3
______________________________________ with a hydrophobic agent in a ratio of 10:0.5 to 10:3 and agitating the precipitated silicic acid with hydrophobic agent, and tempering the product obtained for 60 to 180 minutes at a temperature of 200° C. to 400° C. and thereafter grinding to form a finely divided product.
Claim 2
Dependent Claim
197 words
A process for the production of hydrophobic silicic acid comprising treating precipitated silicic acid having the following properties: ______________________________________
BET surface acc. to DIN 66 131
m.sup.2 /g
150 ± 30
Average size of the primary
particles from EM pictures
nm 15-22
Loss after drying acc. to DIN
55 921 after 2 hours at 105° C.
% 2.5-3.5
Loss at red heat (related to the
substance dried for 2 hours at
105° C.) acc. to DIN 55 921
% 3 ± 0.5
pH value (in 5% aqueous dis-
persion) acc. to DIN 53 200 3.5-5.5
Conductivity (in 4% aqueous
dispersion) us <500
Tamped density of the
unaerated substance acc. to
g/l 60 ± 20
DIN 53 194
SO.sub.3 content (related to the
substance dried for 2 hours at
105° C.) % <0.3
Na.sub.2 O content (related to the
substance dried for 2 hours at
105° C.) % <0.3
______________________________________ with a hydrophobic agent in a ratio of 10:0.5 to 10:3 and agitating the precipitated silicic acid with hydrophobic agent, and tempering the product obtained for 60 to 180 minutes at a temperature of 200° C. to 400° C. and thereafter grinding to form a finely divided product.
Claim 3
Dependent Claim
21 words
The process as defined in claim 1 wherein the tempering is carried out for a period of 70 to 130 minutes.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1984-12-28 | 1985-06-29 | 1985-12-29 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1988-12-28 | 1989-06-29 | 1989-12-29 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1992-12-28 | 1993-06-29 | 1993-12-29 | $7700.00 | Window Closed / Lapsed |