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Precipitated silicic acid, method and compositions containing same

Assignee: Evonik Operations GmbH
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Filing: 1981-01-23
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Granted: 1981-12-29
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Expires: 2001-01-23
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Abstract

Abstract Finely divided precipitated silicic acid is obtained by the method of the invention. Compositions containing the finely divided precipitated silicic acid as a filler distributed in an elastomer such as an organopolysiloxane are disclosed.

Inventors

  • 👤 Peter Nauroth
  • 👤 Heinz Esch
  • 👤 Robert Kuhlmann
  • 👤 Rudolf Bode
  • 👤 Arthur Reisert
  • 👤 Harald Buhler
  • 👤 Gunter Turk

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-11-08 13:12
CPC Classifications
C; C01; C01B; C01B33/00; C01B33/113; C01B33/12; C01B33/18; C01B33/187; C01B33/193; B; B82; B82Y; B82Y30/00; C08; C08K; C08K3/00; C08K3/34; C08K3/36; C09; C09C; C09C1/00; C09C1/28; C09C1/30; C09C1/3081; C01P; C01P2004/00; C01P2004/60; C01P2004/64; C01P2006/00; C01P2006/10; C01P2006/11; C01P2006/12; C01P2006/19; C01P2006/40; C01P2006/80; C01P2006/82; C01P2006/90

Claims Analysis

Total Claims: 3
Claim 1
Independent Claim 197 words
A process for the production of hydrophobic silicic acid comprising treating precipitated silicic acid having the following properties: ______________________________________ BET surface acc. to DIN 66 131 m.sup.2 /g 150 ± 30 Average size of the primary particles from EM pictures nm 15-22 Loss after drying acc. to DIN 55 921 after 2 hours at 105° C. % 2.5-3.5 Loss at red heat (related to the substance dried for 2 hours at 105° C.) acc. to DIN 55 921 % 3 ± 0.5 pH value (in 5% aqueous dis- persion) acc. to DIN 53 200 3.5-5.5 Conductivity (in 4% aqueous dispersion) us <500 Tamped density of the unaerated substance acc. to g/l 60 ± 20 DIN 53 194 SO.sub.3 content (related to the substance dried for 2 hours at 105° C.) % <0.3 Na.sub.2 O content (related to the substance dried for 2 hours at 105° C.) % <0.3 ______________________________________ with a hydrophobic agent in a ratio of 10:0.5 to 10:3 and agitating the precipitated silicic acid with hydrophobic agent, and tempering the product obtained for 60 to 180 minutes at a temperature of 200° C. to 400° C. and thereafter grinding to form a finely divided product.
Claim 2
Dependent Claim 197 words
A process for the production of hydrophobic silicic acid comprising treating precipitated silicic acid having the following properties: ______________________________________ BET surface acc. to DIN 66 131 m.sup.2 /g 150 ± 30 Average size of the primary particles from EM pictures nm 15-22 Loss after drying acc. to DIN 55 921 after 2 hours at 105° C. % 2.5-3.5 Loss at red heat (related to the substance dried for 2 hours at 105° C.) acc. to DIN 55 921 % 3 ± 0.5 pH value (in 5% aqueous dis- persion) acc. to DIN 53 200 3.5-5.5 Conductivity (in 4% aqueous dispersion) us <500 Tamped density of the unaerated substance acc. to g/l 60 ± 20 DIN 53 194 SO.sub.3 content (related to the substance dried for 2 hours at 105° C.) % <0.3 Na.sub.2 O content (related to the substance dried for 2 hours at 105° C.) % <0.3 ______________________________________ with a hydrophobic agent in a ratio of 10:0.5 to 10:3 and agitating the precipitated silicic acid with hydrophobic agent, and tempering the product obtained for 60 to 180 minutes at a temperature of 200° C. to 400° C. and thereafter grinding to form a finely divided product.
Claim 3
Dependent Claim 21 words
The process as defined in claim 1 wherein the tempering is carried out for a period of 70 to 130 minutes.

References Cited (Backward Citations)

US3132961A Cited
US3677784A Cited
US3649588A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-12-28 1985-06-29 1985-12-29 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-12-28 1989-06-29 1989-12-29 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-12-28 1993-06-29 1993-12-29 $7700.00 Window Closed / Lapsed

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