Patent US4302166A successfully refreshed from Google Patents.
US4302166A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Droplet forming apparatus for use in producing uniform particles
Assignee: Coulter Electronics Inc
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Filing: 1979-03-15
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Granted: 1981-11-24
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Expires: 1999-03-15
Abstract
Abstract Uniform particles are produced by introducing a laminar stream of a core liquid into a laminar flowing body of an immiscible sheath liquid. The core liquid or the sheath liquid, or both liquids, can contain one or more materials dispersed (dissolved or suspended) in them from which the uniform particles are formed. The two liquids and the dispersed material are expelled from a nozzle to form a liquid jet. The liquid jet is disturbed at a uniform, periodic rate to form liquid droplets which contain a uniform amount of the core liquid, the sheath liquid and the dispersed material. The droplets are collected and held in a catch liquid until the core and the sheath liquid in each droplet have diffused into the catch liquid leaving the uniform particles formed from the dispersed materials. There can be more than one sheath liquid which can also contain one or more materials dispersed in it.
Inventors
- 👤 Mack J. Fulwyler
- 👤 C. William Hatcher
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 09:48
CPC Classifications
B; B01; B01J; B01J13/00; B01J13/02; B01J13/04; Y; Y10; Y10S; Y10S376/00; Y10S376/916
Claims Analysis
Total Claims: 6
Claim 1
Independent Claim
218 words
A droplet forming apparatus for producing uniformly sized solid particles from dispersed material in at least one of a core and sheath liquids which are immiscible with each other and supplied to the apparatus from a source of said liquids, said apparatus comprising: means for connecting the source of core liquid to the apparatus; means for connecting the source of sheath liquid to the apparatus; means for forming a moving body of at least one sheath liquid for laminar movement through the apparatus; means for introducing said core liquid as a laminar stream into said moving body at a selected location along the path of movement of the moving body through the apparatus; means for producing a liquid jet from said moving body after said introduction of said core liquid; disturbance means for periodically disturbing said liquid jet to separate said liquid jet including said core and said sheath liquids into unconnected uniform droplets containing a uniform amount of said disbursed material, said core liquid and said sheath liquid; and means to collect said formed droplets in a catch liquid in which said sheath liquid and said core liquid are each soluble, whereby said sheath liquid and said core liquid are dissolved therein to render the material dispersed in said core liquid into said uniformily sized solid particles.
Claim 2
Dependent Claim
218 words
A droplet forming apparatus for producing uniformly sized solid particles from dispersed material in at least one of a core and sheath liquids which are immiscible with each other and supplied to the apparatus from a source of said liquids, said apparatus comprising: means for connecting the source of core liquid to the apparatus; means for connecting the source of sheath liquid to the apparatus; means for forming a moving body of at least one sheath liquid for laminar movement through the apparatus; means for introducing said core liquid as a laminar stream into said moving body at a selected location along the path of movement of the moving body through the apparatus; means for producing a liquid jet from said moving body after said introduction of said core liquid; disturbance means for periodically disturbing said liquid jet to separate said liquid jet including said core and said sheath liquids into unconnected uniform droplets containing a uniform amount of said disbursed material, said core liquid and said sheath liquid; and means to collect said formed droplets in a catch liquid in which said sheath liquid and said core liquid are each soluble, whereby said sheath liquid and said core liquid are dissolved therein to render the material dispersed in said core liquid into said uniformily sized solid particles.
Claim 3
Dependent Claim
29 words
An apparatus according to claim 1 wherein said disturbance means includes: means for uniformly and periodically disturbing said liquid jet at a constant rate in a transverse direction thereto.
Claim 4
Dependent Claim
29 words
An apparatus according to claim 1 wherein said means for introducing includes: means for introducing said core liquid substantially into the center of said moving body of sheath liquid.
Claim 5
Dependent Claim
30 words
An apparatus according to claim 1 wherein said means for introducing includes: means for introducing said core liquid substantially coaxial with the axis of said moving body of sheath liquid.
Claim 6
Dependent Claim
20 words
An apparatus according to claim 1 further including: charging means for applying like-repelling charges to each of said uniform droplets.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1984-11-23 | 1985-05-25 | 1985-11-24 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1988-11-23 | 1989-05-25 | 1989-11-24 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1992-11-23 | 1993-05-25 | 1993-11-24 | $7700.00 | Window Closed / Lapsed |