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US4299593A Expired / Lapsed US ⏱️ 0.0 years remaining

Method and apparatus for detecting and measuring a gas

Assignee: Dow Chemical Co
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Filing: 1979-04-20
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Granted: 1981-11-10
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Expires: 1999-04-20
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Abstract

Abstract A technique is described for continuously detecting or measuring a gas such as hydrogen cyanide in a gas stream. The gas stream is passed in counterflow relationship with a well defined stream of gas absorbing reagent liquid in an absorption cell through which the reagent flows under gravity feed. The exposed reagent is passed through a heater in which the color of the reagent is developed. The reagent is passed through the heater at a constant regulated flow rate with a flow controller operative between the absorption cell and the heater to provide a consistent color development. A stable and consistent detection and measurement of the amount of hydrogen cyanide in the gas stream is obtained.

Inventors

  • 👤 Robert B. Dopp

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-29 17:10
CPC Classifications
G; G01; G01N; G01N21/00; G01N21/75; G01N21/77; G01N21/78; G01N21/783; Y; Y10; Y10T; Y10T436/00; Y10T436/17; Y10T436/172307

Claims Analysis

Total Claims: 2
Claim 1
Independent Claim 205 words
In a method for measuring the amount of hydrogen cyanide in a gas stream by utilizing a hydrogen cyanide absorbing reagent liquid, which upon exposure to and absorption of hydrogen cyanide, undergoes a color change upon passage of the exposed reagent liquid through a heater for subsequent analysis of the reagent liquid in a color detector, the improvement comprising the steps of: passing the stream of gas in counter flow relationship with a flow of hydrogen cyanide absorbing reagent liquid for exposure to and absorption by the latter of hydrogen cyanide while feeding the reagent liquid under gravity in a well defined stream; controlling the flow rate of said exposed reagent liquid at a point subsequent to its exposure to hydrogen cyanide and prior to the entry of the reagent to the heater with a predetermined head of the reagent liquid above said heater by optically sensing the reagent liquid at a predetermined level above said heater; and varying the flow of said reagent liquid at a place above said heater to maintain a meniscus of the reagent liquid at said predetermined level thereby establishing through said heater a substantially constant flow rate for a consistent measurement of the color of said exposed reagent liquid.
Claim 2
Dependent Claim 205 words
In a method for measuring the amount of hydrogen cyanide in a gas stream by utilizing a hydrogen cyanide absorbing reagent liquid, which upon exposure to and absorption of hydrogen cyanide, undergoes a color change upon passage of the exposed reagent liquid through a heater for subsequent analysis of the reagent liquid in a color detector, the improvement comprising the steps of: passing the stream of gas in counter flow relationship with a flow of hydrogen cyanide absorbing reagent liquid for exposure to and absorption by the latter of hydrogen cyanide while feeding the reagent liquid under gravity in a well defined stream; controlling the flow rate of said exposed reagent liquid at a point subsequent to its exposure to hydrogen cyanide and prior to the entry of the reagent to the heater with a predetermined head of the reagent liquid above said heater by optically sensing the reagent liquid at a predetermined level above said heater; and varying the flow of said reagent liquid at a place above said heater to maintain a meniscus of the reagent liquid at said predetermined level thereby establishing through said heater a substantially constant flow rate for a consistent measurement of the color of said exposed reagent liquid.

References Cited (Backward Citations)

US2116999A Cited
US2356530A Cited
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USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-11-09 1985-05-11 1985-11-10 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-11-09 1989-05-11 1989-11-10 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-11-09 1993-05-11 1993-11-10 $7700.00 Window Closed / Lapsed

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