US4299593A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Method and apparatus for detecting and measuring a gas
Assignee: Dow Chemical Co
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Filing: 1979-04-20
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Granted: 1981-11-10
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Expires: 1999-04-20
Abstract
Abstract A technique is described for continuously detecting or measuring a gas such as hydrogen cyanide in a gas stream. The gas stream is passed in counterflow relationship with a well defined stream of gas absorbing reagent liquid in an absorption cell through which the reagent flows under gravity feed. The exposed reagent is passed through a heater in which the color of the reagent is developed. The reagent is passed through the heater at a constant regulated flow rate with a flow controller operative between the absorption cell and the heater to provide a consistent color development. A stable and consistent detection and measurement of the amount of hydrogen cyanide in the gas stream is obtained.
Inventors
- 👤 Robert B. Dopp
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-29 15:13
CPC Classifications
G; G01; G01N; G01N21/00; G01N21/75; G01N21/77; G01N21/78; G01N21/783; Y; Y10; Y10T; Y10T436/00; Y10T436/17; Y10T436/172307
Claims Analysis
Total Claims: 2
Claim 1
Independent Claim
205 words
In a method for measuring the amount of hydrogen cyanide in a gas stream by utilizing a hydrogen cyanide absorbing reagent liquid, which upon exposure to and absorption of hydrogen cyanide, undergoes a color change upon passage of the exposed reagent liquid through a heater for subsequent analysis of the reagent liquid in a color detector, the improvement comprising the steps of: passing the stream of gas in counter flow relationship with a flow of hydrogen cyanide absorbing reagent liquid for exposure to and absorption by the latter of hydrogen cyanide while feeding the reagent liquid under gravity in a well defined stream; controlling the flow rate of said exposed reagent liquid at a point subsequent to its exposure to hydrogen cyanide and prior to the entry of the reagent to the heater with a predetermined head of the reagent liquid above said heater by optically sensing the reagent liquid at a predetermined level above said heater; and varying the flow of said reagent liquid at a place above said heater to maintain a meniscus of the reagent liquid at said predetermined level thereby establishing through said heater a substantially constant flow rate for a consistent measurement of the color of said exposed reagent liquid.
Claim 2
Dependent Claim
205 words
In a method for measuring the amount of hydrogen cyanide in a gas stream by utilizing a hydrogen cyanide absorbing reagent liquid, which upon exposure to and absorption of hydrogen cyanide, undergoes a color change upon passage of the exposed reagent liquid through a heater for subsequent analysis of the reagent liquid in a color detector, the improvement comprising the steps of: passing the stream of gas in counter flow relationship with a flow of hydrogen cyanide absorbing reagent liquid for exposure to and absorption by the latter of hydrogen cyanide while feeding the reagent liquid under gravity in a well defined stream; controlling the flow rate of said exposed reagent liquid at a point subsequent to its exposure to hydrogen cyanide and prior to the entry of the reagent to the heater with a predetermined head of the reagent liquid above said heater by optically sensing the reagent liquid at a predetermined level above said heater; and varying the flow of said reagent liquid at a place above said heater to maintain a meniscus of the reagent liquid at said predetermined level thereby establishing through said heater a substantially constant flow rate for a consistent measurement of the color of said exposed reagent liquid.
References Cited (Backward Citations)
US2116999A
Cited
US2356530A
Cited
US2534229A
Cited
US2728639A
Cited
US2829032A
Cited
GB834816A
Cited
US3028224A
Cited
US3666419A
Cited
US3708265A
Cited
US4079293A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1984-11-09 | 1985-05-11 | 1985-11-10 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1988-11-09 | 1989-05-11 | 1989-11-10 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1992-11-09 | 1993-05-11 | 1993-11-10 | $7700.00 | Window Closed / Lapsed |