Patent US4285735A successfully refreshed from Google Patents.
US4285735A
Expired / Lapsed
US
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Fructose polymer mixture
Assignee: Individual
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Filing: 1980-03-10
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Granted: 1981-08-25
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Expires: 2000-03-10
Abstract
Abstract A process for making a fructose polymer mixture containing chiefly inulin and inulides with minor amounts of impurities is based on the finding that inulin is in a soluble metastable state at room temperature as it exists in the dahlia tuber. Novel steps in the process are the separation, without the use of heat or adding water, of the water soluble from the ground dahlia tuber within about 10 minutes after grinding, followed by separation by coagulation of protein color and flavor bodies by heating at the boiling temperature from 3 to 10 minutes. No chemical defecating agent, such as lime water is used or required. The resulting clear extract is concentrated to 40% to 70% solids. Dry product is recovered by crystallizing the concentrated extract at 1° to 15° C. The product differs from inulin in that the product, in addition to inulin, also contains inulides, protein, color, flavor bodies, and minerals.
Inventors
- 👤 William A. Mitchell
- 👤 Charles E. Mitchell
- 👤 Pat R. Mitchell
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-09 16:34
CPC Classifications
C; C08; C08B; C08B37/00; C08B37/0006; C08B37/0051
Claims Analysis
Total Claims: 11
Claim 1
Independent Claim
54 words
The process for extracting a fructose polymer mixture dispersion from dahlia tubers without adding water or heating, comprising grinding scrubbed dahlia tubers at temperatures of 2° to 40° C. to about a 10 mesh particle size; and then separating the water solubles from the insoluble fibrous material within no longer than about ten minutes.
Claim 2
Dependent Claim
54 words
The process for extracting a fructose polymer mixture dispersion from dahlia tubers without adding water or heating, comprising grinding scrubbed dahlia tubers at temperatures of 2° to 40° C. to about a 10 mesh particle size; and then separating the water solubles from the insoluble fibrous material within no longer than about ten minutes.
Claim 3
Dependent Claim
22 words
The process of claim 1 wherein the separation of the water solubles from the insoluble material is accomplished by pressing or centrifuging.
Claim 4
Dependent Claim
76 words
The process for separating most of the protein, color and flavor bodies as well as some carbohydrates and minerals from the water soluble extract of claim 1 comprising boiling said water soluble extract for 3 to 10 minutes, separating by decanting or centrifuging from the resulting coagulated protein mixture, a clear soluble extract containing chiefly inulin and inulides; and then concentrating the clarified extract to 40% to 70% solids by evaporation under atmospheric or reduced pressures.
Claim 5
Dependent Claim
17 words
A 40% to 70% concentrated slurry of fructose polymer mixture prepared by the process of claim 3.
Claim 6
Dependent Claim
57 words
The process for making crystalline fructose polymer mixtures in which the concentrated fructose polymer mixture of claim 3 is cooled to 1° to 15° C., seeded with inulin crystals and allowed to crystallize for about 12 hours, then removal of mother liquors by centrifugation followed by drying the crystalline fructose polymer mixture between 35° and 70° C.
Claim 7
Dependent Claim
12 words
The dry fructose polymer mixture prepared by the process of claim 5.
Claim 8
Dependent Claim
164 words
The process for preparing a crystalline fructose polymer mixture comprising: (a) directly grinding scrubbed dahlia tubers at a temperature from 2° to 40° C., so as to obtain a 10 mesh particle size, said grinding being carried out without the addition of water; (b) separating the water solubles from the insoluble fibrous material resulting from step (a) within about 10 minutes of the grinding; (c) boiling the extract for 3 to 10 minutes whereby protein, color and flavor bodies are coagulated; (d) separating the coagulated matter to produce a clarified extract; (e) concentrating the clarified extract by evaporation to 40% to 70% solids under atmospheric or reduced pressures; (f) seeding the concentrated extract with inulin crystals; (g) cooling the seeded extract to 1° to 15° C. and maintaining the extract in said temperature range for approximately 12 hours; (h) separating the resulting mother liquor from the resulting fructose polymer mixture; and (i) drying the crystalline fructose polymer mixture at between 35° and 70° C.
Claim 9
Dependent Claim
164 words
The process for preparing a crystalline fructose polymer mixture comprising: (a) directly grinding scrubbed dahlia tubers at a temperature from 2° to 40° C., so as to obtain a 10 mesh particle size, said grinding being carried out without the addition of water; (b) separating the water solubles from the insoluble fibrous material resulting from step (a) within about 10 minutes of the grinding; (c) boiling the extract for 3 to 10 minutes whereby protein, color and flavor bodies are coagulated; (d) separating the coagulated matter to produce a clarified extract; (e) concentrating the clarified extract by evaporation to 40% to 70% solids under atmospheric or reduced pressures; (f) seeding the concentrated extract with inulin crystals; (g) cooling the seeded extract to 1° to 15° C. and maintaining the extract in said temperature range for approximately 12 hours; (h) separating the resulting mother liquor from the resulting fructose polymer mixture; and (i) drying the crystalline fructose polymer mixture at between 35° and 70° C.
Claim 10
Dependent Claim
17 words
The process of claim 7 wherein the separation of step (b) is accomplished by pressing or centrifuging.
Claim 11
Dependent Claim
17 words
The process of claim 7 wherein the separation of step (d) is accomplished by decantation or centrifugation.
References Cited (Backward Citations)
US2834694A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1984-08-24 | 1985-02-23 | 1985-08-25 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1988-08-24 | 1989-02-23 | 1989-08-25 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1992-08-24 | 1993-02-23 | 1993-08-25 | $7700.00 | Window Closed / Lapsed |