US4282034A
Expired / Lapsed
US
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Amorphous metal structures and method
Assignee: Wisconsin Alumni Research Foundation
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Filing: 1978-11-13
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Granted: 1981-08-04
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Expires: 1998-11-13
Abstract
Abstract Bulk shapes and solid structures of amorphous metals formed of micron sized particles produced by droplet emulsion technique whereby undercooled droplets are solidified in the amorphous state with a stabilizing coating on the surfaces thereof, the shapes and solid structures being formed by dispersing the stabilizing coating and bringing the particles into intimate metal to metal contact for atomic bonding, without raising the temperature to crystallization temperature.
Inventors
- 👤 Jeffery S. Smith
- 👤 John H. Perepezko
- 👤 Don H. Rasmussen
- 👤 Carl R. Loper, Jr.
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-10-24 23:20
CPC Classifications
B; B22; B22F; B22F3/00; B22F3/006; B22F9/00; B22F9/002; B22F9/02; B22F9/06
Claims Analysis
Total Claims: 5
Claim 1
Independent Claim
156 words
In the method of producing amorphous metal structures from amorphous metal particles produced by (a) emulsifying the metal as droplets in a molten state in an inert carrier fluid, (b) reacting the molten metal while in the emulsified state in the fluid to form a reaction product on the surface of the metal droplets which stabilizes the metal droplets in the emulsion, (c) cooling the emulsion whereby the metal droplets solidify as particles of undercooled metal in the amorphous state, and (d) separating the undercooled amorphous metal particles, the improvement comprising: (1) compressing the particles while deforming the particles to apply shear and compressive forces to said particles to expose the amorphous metal interior of the reaction product on the surface of the particles while at a temperature below recrystallization temperature of the metal to avoid recrystallization, whereby the exposed amorphous metal of the particles interbond with each other to form a solid amorphous metal structure.
Claim 2
Dependent Claim
156 words
In the method of producing amorphous metal structures from amorphous metal particles produced by (a) emulsifying the metal as droplets in a molten state in an inert carrier fluid, (b) reacting the molten metal while in the emulsified state in the fluid to form a reaction product on the surface of the metal droplets which stabilizes the metal droplets in the emulsion, (c) cooling the emulsion whereby the metal droplets solidify as particles of undercooled metal in the amorphous state, and (d) separating the undercooled amorphous metal particles, the improvement comprising: (1) compressing the particles while deforming the particles to apply shear and compressive forces to said particles to expose the amorphous metal interior of the reaction product on the surface of the particles while at a temperature below recrystallization temperature of the metal to avoid recrystallization, whereby the exposed amorphous metal of the particles interbond with each other to form a solid amorphous metal structure.
Claim 3
Dependent Claim
23 words
The method as claimed in claim 1 in which the reaction product on the surface of the metal particles is a metal oxide.
Claim 4
Dependent Claim
28 words
The method as claimed in claim 1 in which the particles are in the form of micro-sized spherical particles having a diameter within the range of 1-200 μm.
Claim 5
Dependent Claim
8 words
A product of the process of claim 1.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1984-08-03 | 1985-02-02 | 1985-08-04 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1988-08-03 | 1989-02-02 | 1989-08-04 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1992-08-03 | 1993-02-02 | 1993-08-04 | $7700.00 | Window Closed / Lapsed |