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US4276229A
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Process for preparing carbamate compounds
Assignee: Rhone Poulenc Nederland BV
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Filing: 1980-03-25
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Granted: 1981-06-30
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Expires: 2000-03-25
Abstract
Abstract This invention relates to an improved process for preparing carbamate compounds by reacting an active hydrogen-containing compound with an N-alkylcarbamoyl sulfonate salt in the presence of a base.
Inventors
- 👤 Young-Jin Lee
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-07 21:21
CPC Classifications
C; C07; C07C; C07C271/00; C07C271/06
Claims Analysis
Total Claims: 9
Claim 1
Independent Claim
102 words
A process for preparing a compound of the formula: ##STR5## which comprises reacting a compound of the formula: ##STR6## with an active hydrogen containing compound containing an organic radical, in the presence of a base, wherein: M is an alkali metal or ammonium ion; R is a C 1 -C 8 alkyl or phenyl group; and, R' is an organic radical from the active hydrogen containing compound, and wherein said active hydrogen containing compound is selected from the group consisting of an aliphatic alcohol, an aromatic aliphatic alcohol, a phenolic compound, a thiol compound, a secondary or primary amine, or an oxime.
Claim 2
Dependent Claim
102 words
A process for preparing a compound of the formula: ##STR5## which comprises reacting a compound of the formula: ##STR6## with an active hydrogen containing compound containing an organic radical, in the presence of a base, wherein: M is an alkali metal or ammonium ion; R is a C 1 -C 8 alkyl or phenyl group; and, R' is an organic radical from the active hydrogen containing compound, and wherein said active hydrogen containing compound is selected from the group consisting of an aliphatic alcohol, an aromatic aliphatic alcohol, a phenolic compound, a thiol compound, a secondary or primary amine, or an oxime.
Claim 3
Dependent Claim
14 words
A process according to claim 1 wherein said base is an alkali metal hydroxide.
Claim 4
Dependent Claim
28 words
A process according to claim 1 wherein said reaction is conducted in a solvent selected from the group consisting of water, toluene, methylene chloride, chloroform and mixtures thereof.
Claim 5
Dependent Claim
11 words
A process according to claim 3 wherein said solvent is water.
Claim 6
Dependent Claim
12 words
A process according to claim 1 wherein R' is a methyl group.
Claim 7
Dependent Claim
30 words
A process according to claim 1 wherein an alkali or ammonium salt of N-methylcarbamoyl sulfonate is reacted with 1-naphthol in the presence of an alkali base to prepare 1-naphthyl-N-methyl carbamate.
Claim 8
Dependent Claim
35 words
A process according to claim 1 wherein an alkali or ammonium salt of N-methylcarbamoylsulfonate is reacted with 2-methyl 2-(methylthio) propionaldehyde oxime in the presence of an alkali metal base to prepare 2-methyl-2(methylthio) propionaldehyde-)-(methyl carbamoyl) oxime.
Claim 9
Dependent Claim
33 words
A process according to claim 1 wherein an alkali or ammonium salt of N-methylcarbamoyl sulfonate is reacted with methomyl oxime in the presence of an alkali metal base to prepare methyl N-[(methylcarbamoyl)oxy] thioacetimidate.
References Cited (Backward Citations)
US3847988A
Cited
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1984-06-29 | 1984-12-29 | 1985-06-30 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1988-06-29 | 1988-12-29 | 1989-06-30 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1992-06-29 | 1992-12-29 | 1993-06-30 | $7700.00 | Window Closed / Lapsed |