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US4256469A Expired / Lapsed US ⏱️ 0.0 years remaining

Repressurization technique for pressure swing adsorption

Assignee: Bergwerksverband GmbH
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Filing: 1978-11-06
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Granted: 1981-03-17
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Expires: 1998-11-06
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Abstract

Abstract In a pressure swing adsorption process, the adsorbent being for example a carbon molecular sieve, the usual initial surge of an undesired component, e.g., O2 in a nitrogen stream, from the outlet of a freshly repressurized adsorber, is reduced or eliminated by conducting repressurization in a stage-wise manner with the final part of the repressurization being conducted substantially more slowly than the initial stage of repressurization.

Inventors

  • 👤 Paul Leitgeb

Bibliographic Details

Application Number —
Jurisdiction US
Data Source google_patents
Last Synchronized 2026-10-24 21:36
CPC Classifications
B; B01; B01D; B01D53/00; B01D53/02; B01D53/04; B01D53/047; B01D53/0476; B01D53/0473; B01D2253/00; B01D2253/10; B01D2253/116; B01D2253/25; B01D2256/00; B01D2256/10; B01D2257/00; B01D2257/10; B01D2257/104; B01D2257/50; B01D2257/504; B01D2257/80; B01D2259/00; B01D2259/40; B01D2259/40011; B01D2259/40013; B01D2259/40015; B01D2259/40028; B01D2259/4003; B01D2259/40035; B01D2259/40037; B01D2259/40058; B01D2259/40066; B01D2259/402; B01D53/26; B01D53/261; Y; Y02; Y02C; Y02C20/00; Y02C20/40

Claims Analysis

Total Claims: 18
Claim 1
Independent Claim 164 words
In a pressure swing adsorption process for the separation of a gaseous mixture comprising conducting the gaseous mixture under pressure over a carbon molecular sieve adsorbent in a pressurized adsorber having an inlet and an outlet, said adsorbent being capable of adsorbing at least one component selectively over the other components; discharging from said outlet a gaseous stream enriched in one or more other components; lowering the pressure above the adsorbent for regenerating purposes wit liberation of a gaseous stream enriched in at least the one component; repressurizing the adsorber; and repeating the cycle thereover, the improvement which comprises conducting said repressurizing in at least two stages, wherein the pressure buildup in the first stage or stages to an intermediate pressure is effected relatively rapidly, and the pressure buildup in the last stage to the final adsorption pressure is conducted substantially more gradually, said improvement resulting in the diminution of a surge of undesired component in the initial stream discharged from the repressurized bed.
Claim 2
Dependent Claim 164 words
In a pressure swing adsorption process for the separation of a gaseous mixture comprising conducting the gaseous mixture under pressure over a carbon molecular sieve adsorbent in a pressurized adsorber having an inlet and an outlet, said adsorbent being capable of adsorbing at least one component selectively over the other components; discharging from said outlet a gaseous stream enriched in one or more other components; lowering the pressure above the adsorbent for regenerating purposes wit liberation of a gaseous stream enriched in at least the one component; repressurizing the adsorber; and repeating the cycle thereover, the improvement which comprises conducting said repressurizing in at least two stages, wherein the pressure buildup in the first stage or stages to an intermediate pressure is effected relatively rapidly, and the pressure buildup in the last stage to the final adsorption pressure is conducted substantially more gradually, said improvement resulting in the diminution of a surge of undesired component in the initial stream discharged from the repressurized bed.
Claim 3
Dependent Claim 28 words
A process according to claim 1, wherein the pressure buildup in the last stage is conducted with unseparated gaseous mixture passed in to the inlet of the adsorber.
Claim 4
Dependent Claim 33 words
A process according to claim 2, wherein during the pressure buildup in the last stage, a gaseous stream enriched in one or more other components is discharged from the outlet of the adsorber.
Claim 5
Dependent Claim 25 words
A process according to claim 3, wherein the end of the pressure buildup in the last stage coincides with the end of the adsorption cycle.
Claim 6
Dependent Claim 29 words
A process according to claim 2 comprising a three-stage pressure buildup, the pressure buildup in the second stage also being conducted by passing unseparated gaseous mixture into the adsorber.
Claim 7
Dependent Claim 45 words
A process according to claim 1, wherein a complete cycle is conducted in about 2 minutes, the pressure buildup in the first stages is conducted in 2 to 5 seconds, and the pressure buildup on the last stage is conducted in 20 to 30 seconds.
Claim 8
Dependent Claim 51 words
A process according to claim 1, wherein a complete cycle is conducted in about 2 minutes, the pressure buildup in the first stages is conducted in 2 to 5 seconds and the pressure buildup in the last stage is conducted in 20 seconds up to the end of the adsorption cycle.
Claim 9
Dependent Claim 22 words
A process according to claim 1, wherein the pressure ratio between the adsorption pressure and the desorption pressure is 4:1 to 8:1.
Claim 10
Dependent Claim 22 words
A process according to claim 1, wherein the pressure ratio between the adsorption pressure and the desorption pressure is 4:1 to 20:1.
Claim 11
Dependent Claim 23 words
A process according to claim 1, wherein the pressure ratio between the adsorption pressure and the desorption pressure is about 20:1 to 60:1.
Claim 12
Dependent Claim 79 words
A process according to claim 1, wherein in the first stage or stages the pressure is increased to 40 to 70% of the total adsorption pressure in 3 to 10% of the total time, and in the second stage the pressure is increased to 70 to 100% of the total adsorption pressure in 30 to 85% of the total time, and in the third stage the final adsorption pressure is achieved in 70 to 15% of the total time.
Claim 13
Dependent Claim 16 words
A process according to claim 11, wherein the total repressurization occurs in 5 to 60 seconds.
Claim 14
Dependent Claim 16 words
A process according to claim 12, wherein the total repressurization occurs in 30 to 60 seconds.
Claim 15
Dependent Claim 28 words
A process according to claim 1, wherein the gaseous mixture comprises air and wherein oxygen is preferentially adsorbed over the carbon molecular sieve adsorbent, thereby producing nitrogen-enriched gas.
Claim 16
Dependent Claim 22 words
A process according to claim 14, wherein the nitrogen enriched gas has a residual oxygen content of 0.1 to 5% by volume.
Claim 17
Dependent Claim 15 words
A process according to claim 1, wherein the adsorption pressure is 2 to 14 bars.
Claim 18
Dependent Claim 15 words
A process according to claim 16, wherein the adsorption pressure is 4 to 10 bars.

References Cited (Backward Citations)

US3176444A Cited
US3801513A Cited
US3738087A Cited
US3923477A Cited
US4011065A Cited
GB1480866A Cited

USPTO Annuity & Maintenance Windows

Annuity Stage Window Opens Payment Deadline Surcharge Period Until Estimated Fee Status
3.5 Years (Year 4) 1984-03-16 1984-09-15 1985-03-17 $2000.00 Window Closed / Lapsed
7.5 Years (Year 8) 1988-03-16 1988-09-15 1989-03-17 $3760.00 Window Closed / Lapsed
11.5 Years (Year 12) 1992-03-16 1992-09-15 1993-03-17 $7700.00 Window Closed / Lapsed

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