Patent US4248252A successfully refreshed from Google Patents.
US4248252A
Expired / Lapsed
US
⏱️ 0.0 years remaining
Continuous process for expanding tobacco
Assignee: Philip Morris USA Inc
•
Filing: 1978-06-02
•
Granted: 1981-02-03
•
Expires: 1998-06-02
Abstract
Abstract A continuous process of expanding tobacco with carbon dioxide and ammonia is disclosed which comprises contacting tobacco with concentrated ammonium hydroxide, mixing the ammonium hydroxide-treated tobacco with ground solid carbon dioxide, thereafter expanding the tobacco by means of heat and equilibrating the expanded tobacco until equilibrium moisture content is attained. Concentrated aqueous solutions of ammonium carbamate may be substituted for the ammonium hydroxide and solid carbon dioxide in the process. The tobacco may be expanded in an atmosphere of hot steam or gas, or by means of microwave or radiant heat energy. The process allows impregnation and expansion of tobacco to be effected without interruption on a production line.
Inventors
- 👤 Andrew T. Lendvay
- 👤 Billy M. Spann
Bibliographic Details
Application Number
—
Jurisdiction
US
Data Source
google_patents
Last Synchronized
2026-11-08 16:25
CPC Classifications
A; A24; A24B; A24B3/00; A24B3/18; A24B3/182
Claims Analysis
Total Claims: 7
Claim 1
Independent Claim
117 words
The continuous process of expanding tobacco comprising the steps of: a. contacting tobacco with concentrated ammonium hydroxide in an amount sufficient to introduce at least one percent by weight of ammonia; b. allowing the tobacco to remain in contact with the ammonium hydroxide for at least one minute; c. combining the ammonium hydroxide-treated tobacco with sufficient solid carbon dioxide in comminuted form to counteract the heat of reaction of the carbon dioxide, ammonia and tobacco moisture and to release enough carbon dioxide for absorption into the tobacco of between 2 and 8 percent by weight of carbon dioxide; d. thereafter expanding the tobacco by means of heat; and e. equilibrating the tobacco after it has been expanded.
Claim 2
Dependent Claim
117 words
The continuous process of expanding tobacco comprising the steps of: a. contacting tobacco with concentrated ammonium hydroxide in an amount sufficient to introduce at least one percent by weight of ammonia; b. allowing the tobacco to remain in contact with the ammonium hydroxide for at least one minute; c. combining the ammonium hydroxide-treated tobacco with sufficient solid carbon dioxide in comminuted form to counteract the heat of reaction of the carbon dioxide, ammonia and tobacco moisture and to release enough carbon dioxide for absorption into the tobacco of between 2 and 8 percent by weight of carbon dioxide; d. thereafter expanding the tobacco by means of heat; and e. equilibrating the tobacco after it has been expanded.
Claim 3
Dependent Claim
34 words
The process of claim 1, wherein the step of combining the blended tobacco with solid carbon dioxide is carried out using about twice the stoichiometric amount of solid carbon dioxide relative to ammonium hydroxide.
Claim 4
Dependent Claim
39 words
The process of claim 1, wherein the step of contacting tobacco with ammonium hydroxide is carried out until the amount of ammonia impregnated in the tobacco is between 2.5 and 10 percent based on the weight of the tobacco.
Claim 5
Dependent Claim
32 words
The process of claim 1, wherein the step of allowing the tobacco to remain in contact with the ammonium hydroxide is carried out while vibrating the tobacco on an enclosed vibratory conveyor.
Claim 6
Dependent Claim
30 words
The process of claim 1, wherein the step of expanding the tobacco is carried out by conveying the tobacco in a thin layer in proximity to a radiant heat source.
Claim 7
Dependent Claim
26 words
The process of claim 1, wherein the step of expanding the tobacco is carried out by conveying the tobacco in proximity to a microwave energy source.
References Cited (Backward Citations)
USPTO Annuity & Maintenance Windows
| Annuity Stage | Window Opens | Payment Deadline | Surcharge Period Until | Estimated Fee | Status |
|---|---|---|---|---|---|
| 3.5 Years (Year 4) | 1984-02-03 | 1984-08-04 | 1985-02-03 | $2000.00 | Window Closed / Lapsed |
| 7.5 Years (Year 8) | 1988-02-03 | 1988-08-04 | 1989-02-03 | $3760.00 | Window Closed / Lapsed |
| 11.5 Years (Year 12) | 1992-02-03 | 1992-08-04 | 1993-02-03 | $7700.00 | Window Closed / Lapsed |